CH185145A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH185145A CH185145A CH185145DA CH185145A CH 185145 A CH185145 A CH 185145A CH 185145D A CH185145D A CH 185145DA CH 185145 A CH185145 A CH 185145A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- azo dye
- new azo
- new
- new dye
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title description 2
- 239000000975 dye Substances 0.000 claims description 7
- 239000000835 fiber Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 235000013311 vegetables Nutrition 0.000 claims description 2
- RJEMRACHOZYVGV-UHFFFAOYSA-N 4-[(4-chlorophenyl)diazenyl]-2-methoxy-5-methylaniline Chemical compound C1=C(N)C(OC)=CC(N=NC=2C=CC(Cl)=CC=2)=C1C RJEMRACHOZYVGV-UHFFFAOYSA-N 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- KPHCRJCYHWMMBI-UHFFFAOYSA-N benzo[a]fluoren-2-one Chemical compound C=1C(C=CC2=CC=C3C=4C=CC=CC4C=C3C21)=O KPHCRJCYHWMMBI-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B31/00—Disazo and polyazo dyes of the type A->B->C, A->B->C->D, or the like, prepared by diazotising and coupling
- C09B31/02—Disazo dyes
- C09B31/12—Disazo dyes from other coupling components "C"
- C09B31/14—Heterocyclic components
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B31/00—Disazo and polyazo dyes of the type A->B->C, A->B->C->D, or the like, prepared by diazotising and coupling
- C09B31/02—Disazo dyes
- C09B31/06—Disazo dyes from a coupling component "C" containing a directive hydroxyl group
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines neuen Azofarbstoffes. Es wurde gefunden, dass man einen neuen Farbstoff erhält, welcher der Formel
EMI0001.0003
entspricht, wenn man dianotiertes 4-Amirro- 5-methoxy - 2 - methyl-4'- chlor-1 . 1'- azobenzol mit 3-Oxy-1 .2-benzofluorenon kuppelt.
Der neue Farbstoff bildet ein schwarzes Pulver. Auf geeigneten Substraten, wie z. B. pflanzlichen Fasern, hergestellt, färbt er diese in echten schweren Tönen.
<I>Beispiel:</I> 27,5 Teile 4-Amirro-5-methoxy-2-methyl- 4'-chlor-1.1'-azobenzol werden wie üblich dianotiert und in eine Lösung von 24,6 Tei len des 3-Oxy-1. 2-benzofluorenons, 50 Teilen 30 o/oiger Natronlauge, 30 Teilen Soda und 2000 Teilen Wasser eingetragen. Der gebil- dete Farbstoff fällt sofort aus. Der schwarze Niederschlag wird filtriert und getrocknet.
Process for the production of a new azo dye. It has been found that a new dye is obtained which has the formula
EMI0001.0003
corresponds if one dianotated 4-Amirro-5-methoxy-2-methyl-4'-chloro-1. 1'-azobenzene couples with 3-oxy-1 .2-benzofluorenone.
The new dye forms a black powder. On suitable substrates, such as. B. vegetable fibers, he dyes them in real heavy tones.
<I> Example: </I> 27.5 parts of 4-amirro-5-methoxy-2-methyl-4'-chloro-1.1'-azobenzene are dianotized as usual and poured into a solution of 24.6 parts of the 3rd -Oxy-1. 2-benzofluorenone, 50 parts of 30% sodium hydroxide solution, 30 parts of soda and 2000 parts of water. The dye formed precipitates immediately. The black precipitate is filtered and dried.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH185145T | 1934-10-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH185145A true CH185145A (en) | 1936-07-15 |
Family
ID=4433507
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH185145D CH185145A (en) | 1934-10-13 | 1934-10-13 | Process for the production of a new azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH185145A (en) |
-
1934
- 1934-10-13 CH CH185145D patent/CH185145A/en unknown
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