CH219580A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH219580A CH219580A CH219580DA CH219580A CH 219580 A CH219580 A CH 219580A CH 219580D A CH219580D A CH 219580DA CH 219580 A CH219580 A CH 219580A
- Authority
- CH
- Switzerland
- Prior art keywords
- azo dye
- preparation
- dye
- sulfamino
- chloro
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 150000008049 diazo compounds Chemical class 0.000 claims 1
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 2
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical class [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
- C09B29/28—Amino naphthols
- C09B29/30—Amino naphtholsulfonic acid
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/34—Monoazo dyes prepared by diazotising and coupling from other coupling components
- C09B29/36—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
- C09B29/3604—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
- C09B29/3647—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms
- C09B29/3652—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles
- C09B29/366—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles containing hydroxy-1,2-diazoles, e.g. pyrazolone
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Azofarbstoifes. Gegenstand des vorliegenden Zusatz- .)atentes ist ein Verfahren zur Herstellung :ines Azofarbstoffes, welches dadurch ge- ;ennzeichnet ist, dass man die Diazoverbin- '.ung von 2-Amino-4'-isooctyldiphenyläther iit 1-(4-Chlor-3,6-dimethyl-l-sulfamino)-8- Yynaphthalin-3,6-disulfonsäure kuppelt.
<I>Beispiel:</I> 521,5 Gewichtsteile 1-(4-Chlor-3,6-di aethyl-1-sulfamino)-8-oxynaphthalin-3,6-di- ulfonsäure werden als Dinatriumsalz in Vasser gelöst. Nach Zugabe von überschüs- igem Natriumacetat lässt man .eine aus 97 Gewichtsteilen 2-Amino-4'-isooctyldi- henyläther erhaltene Diazolösung zulaufen. )ie Kupplung ist schnell beendet. Der Farb- toff wird abgesaugt und getrocknet.
Er stellt ein wasserlösliches, rotes Pulver dar, das Wolle in roten Tönen von sehr guter Wasch- und Walkeehtheit färbt.
Process for the production of an azo dye. The subject of the present additional.) Atentes is a process for the production of: an azo dye, which is characterized in that the diazo connection of 2-amino-4'-isooctyldiphenyl ether with 1- (4-chloro- 3,6-dimethyl-1-sulfamino) -8-yynaphthalene-3,6-disulfonic acid couples.
<I> Example: </I> 521.5 parts by weight of 1- (4-chloro-3,6-di-ethyl-1-sulfamino) -8-oxynaphthalene-3,6-di-sulfonic acid are dissolved as the disodium salt in water. After excess sodium acetate has been added, a diazo solution obtained from 97 parts by weight of 2-amino-4'-isooctyldihenyl ether is allowed to run in. ) The clutch is finished quickly. The dye is suctioned off and dried.
It is a water-soluble, red powder that dyes wool in red shades that are very easy to wash and loosen.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE219580X | 1938-12-07 | ||
| CH214175T | 1939-10-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH219580A true CH219580A (en) | 1942-02-15 |
Family
ID=25725552
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH219580D CH219580A (en) | 1938-12-07 | 1939-10-17 | Process for the preparation of an azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH219580A (en) |
-
1939
- 1939-10-17 CH CH219580D patent/CH219580A/en unknown
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