JP2003201543A - Steel pipe excellent in workability and method for producing the same - Google Patents
Steel pipe excellent in workability and method for producing the sameInfo
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- JP2003201543A JP2003201543A JP2002218541A JP2002218541A JP2003201543A JP 2003201543 A JP2003201543 A JP 2003201543A JP 2002218541 A JP2002218541 A JP 2002218541A JP 2002218541 A JP2002218541 A JP 2002218541A JP 2003201543 A JP2003201543 A JP 2003201543A
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Abstract
(57)【要約】
【課題】 引張強さ:580MPa超えの高強度を有し、加工
性に優れた自動車構造部材用高強度鋼管およびその製造
方法を提案する。
【解決手段】 C:0.05〜0.30%、Si:0.01〜1.0 %、
Mn:1.0 〜4.0 %、Al:0.005 〜0.10%、S:0.003 %
以下を含有する組成の素材鋼管に、加熱および均熱処理
を施したのち、圧延終了温度:400 ℃以上 800℃未満、
累積縮径率:20%以上の絞り圧延を施して製品管とす
る。これにより、圧延ままで引張強さが580Mpa超え、降
伏比:70%以下を有し、150 〜300 ℃で10〜20min の熱
処理を施した後に、降伏応力が大きく上昇し、降伏比が
80%以上となる。なお、さらに、Cu、Ni、Cr、Mo、Nb、
Ti、Bのうちから選ばれた1種または2種以上および/
またはREM 、Caのうちから選ばれた1種または2種を含
有してもよい。PROBLEM TO BE SOLVED: To provide a high-strength steel pipe for an automobile structural member having a high tensile strength of more than 580 MPa and excellent workability, and a method for producing the same. SOLUTION: C: 0.05 to 0.30%, Si: 0.01 to 1.0%,
Mn: 1.0 to 4.0%, Al: 0.005 to 0.10%, S: 0.003%
After heating and soaking the raw steel pipe having the following composition, the rolling end temperature: 400 ° C or higher and lower than 800 ° C,
Cumulative diameter reduction: Reduced by 20% or more to produce product pipes. As a result, the as-rolled tensile strength exceeds 580 MPa, the yield ratio is 70% or less, and after a heat treatment at 150 to 300 ° C. for 10 to 20 min, the yield stress increases significantly, and the yield ratio increases.
80% or more. In addition, Cu, Ni, Cr, Mo, Nb,
One or more selected from Ti and B and / or
Alternatively, it may contain one or two selected from REM and Ca.
Description
【0001】[0001]
【発明の属する技術分野】本発明は、自動車構造部材用
鋼管に係り、とくに、自動車構造部材用として高強度で
かつ加工性に優れ、さらには低温短時間熱処理硬化性
(塗装焼付け硬化性)を有する鋼管に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a steel pipe for automobile structural members, and more particularly to a steel pipe for automobile structural members, which has high strength and excellent workability, and further has low temperature short time heat treatment hardenability (paint bake hardenability). The present invention relates to a steel pipe.
【0002】[0002]
【従来の技術】近年、地球環境の保全という観点から、
自動車車体の軽量化が強く要望されている。このような
自動車車体の軽量化要求に伴い、自動車構造用部材とし
て使用される鋼管にも、薄肉化・高強度化が要望されて
いる。鋼管は、自動車構造部材のうちでも懸架機構関係
の用途に向けられることが多い。懸架機構用部材として
用いられる鋼管は、単純な直管として使用される場合も
あるが、曲げ、 縮径、拡管等の成形を経て使用される場
合が多い。このため、鋼管の特性として、高強度に加え
て、加工性にも優れていることが要求される。2. Description of the Related Art In recent years, from the viewpoint of conservation of the global environment,
There is a strong demand for weight reduction of automobile bodies. Along with such demand for weight reduction of automobile bodies, steel pipes used as automobile structural members are also required to be thin and have high strength. Steel pipes are often used for suspension mechanism-related applications among automobile structural members. A steel pipe used as a member for a suspension mechanism may be used as a simple straight pipe, but is often used after being bent, reduced in diameter, or expanded. Therefore, the characteristics of the steel pipe are required to be excellent in workability in addition to high strength.
【0003】自動車の懸架機構部品としては、例えば、
スタビライザーがある。スタビライザーは、自動車の旋
回時の乗り心地および走行安定性を向上する部品であ
り、重要保安部品として指定されている。したがって、
スタビライザーには十分な強度と耐久性を有することが
要求されている。従来から、自動車の懸架機構部品とし
てのスタビライザーは、熱延棒鋼または熱延線材を素材
として、該素材に熱間鍛造および熱間曲げ成形等により
所定の形状の成形品にしたのち、該成形品に焼入れ、焼
戻し処理を施す方法で製造されていた。しかしながら、
この方法では、複雑な工程と大掛かりな設備を必要とし
製造コストの高騰を招くとともに、加熱および焼入れ処
理中に変形が生じる場合があり矯正工程が必須となると
いう問題があった。また、加熱中の酸化にともなう肌荒
れ、脱炭の生成などにより耐疲労性が劣化するという問
題もあった。As a suspension mechanism part of an automobile, for example,
There is a stabilizer. The stabilizer is a component that improves riding comfort and traveling stability when the vehicle turns, and is designated as an important safety component. Therefore,
Stabilizers are required to have sufficient strength and durability. DESCRIPTION OF RELATED ART Conventionally, a stabilizer as a suspension mechanism part of an automobile uses a hot-rolled steel bar or a hot-rolled wire material as a raw material, and after hot-forging and hot-bending the raw material into a predetermined shaped article, the molded article is then formed. It was manufactured by a method of quenching and tempering. However,
This method has a problem in that a complicated process and large-scale equipment are required, the manufacturing cost rises, and deformation may occur during the heating and quenching processes, and the correction process is essential. There is also a problem that the fatigue resistance is deteriorated due to roughening of the skin due to oxidation during heating and generation of decarburization.
【0004】また、最近では、自動車車体の軽量化の要
求や、車体部品の生産効率の向上要求から、スタビライ
ザー等部品素材の中空化が検討されている。従来から、
種々の断面形状を有する中空部材を製造するには、鋼板
をプレス成形した部品同士を溶接代であるフランジ部で
スポット溶接する方法が採用されてきた。しかし、最近
ではこのような中空部材にも、衝突時に、より高い衝撃
吸収能を有することが求められるようになり、素材とし
て一層高強度化した鋼板が使用されるようになってき
た。そのため、従来のプレス成形を用いる方法では、成
形欠陥のない、また成形品の形状、寸法精度に優れた、
中空部材を製造することが困難になりつつある。[0004] Recently, hollowing of component materials such as stabilizers has been studied in response to demands for weight reduction of automobile bodies and demands for improvement in production efficiency of body components. Traditionally,
In order to manufacture hollow members having various cross-sectional shapes, a method has been adopted in which parts formed by press forming steel plates are spot-welded at a flange portion which is a welding allowance. However, recently, even such a hollow member has been required to have a higher impact absorbing capacity at the time of collision, and a steel plate having higher strength has been used as a material. Therefore, in the conventional method using press molding, there is no molding defect, and the shape and dimensional accuracy of the molded product are excellent.
It is becoming difficult to manufacture hollow members.
【0005】また、素材の中空化には、 鋼管を使用する
ことが考えられるが、部材の製造方法として従来の方法
をそのまま踏襲したのでは、 上記したような、矯正工程
を必要とすること、耐疲労性が劣化することといった問
題は依然として未解決のままとなる。
このような問題を解決するための新しい成形方法とし
て、最近、ハイドロフォーミングが注目されている。ハ
イドロフォーミングは、鋼管の内部に高圧液体を注入し
て所要形状の部材に成形する方法であり、鋼管の断面寸
法を拡管加工などにより変化させて、複雑な形状の部材
を一体成形でき、強度・剛性を高める機能を持つ優れた
成形法である。Further, it is conceivable to use a steel pipe for hollowing the material, but if the conventional method is used as it is as a method for manufacturing the member, the above-mentioned straightening step is required, Problems such as deterioration of fatigue resistance remain unsolved. Hydroforming has recently attracted attention as a new molding method for solving such problems. Hydroforming is a method of injecting a high-pressure liquid into the inside of a steel pipe and forming it into a member with the required shape.By changing the cross-sectional dimension of the steel pipe by expanding, etc., it is possible to integrally form a member with a complicated shape. This is an excellent molding method that has the function of increasing rigidity.
【0006】[0006]
【発明の解決しようとする課題】ハイドロフォーミング
に供される鋼管としては、ハイドロフォーミングに耐え
うる加工性を有することが必要なことから、C:0.02〜
0.1 質量%の低炭素鋼板を素材とした引張強さ:580MPa
以下の電縫鋼管が多用されていた。しかしながら、この
ような低強度の鋼管では、最近の自動車用部材の薄肉化
・高強度化の流れに対応できないため、ハイドロフォー
ミングに耐えうる加工性を有する高強度鋼管の開発が熱
望されていた。Since a steel pipe used for hydroforming needs to have workability capable of withstanding hydroforming, C: 0.02 to
Tensile strength made of 0.1% by mass low carbon steel plate: 580MPa
The following ERW pipes were frequently used. However, since such a low-strength steel pipe cannot cope with the recent trend toward thinning and high strength of automobile members, there has been earnest demand for development of a high-strength steel pipe having workability capable of withstanding hydroforming.
【0007】本発明は、上記した従来技術の問題を解決
し、引張強さ:580MPa超えの高強度を有し、加工性に優
れた自動車構造部材用高強度鋼管およびその製造方法を
提案することを目的とする。The present invention solves the above-mentioned problems of the prior art and proposes a high-strength steel pipe for automobile structural members having a high tensile strength: more than 580 MPa and excellent workability, and a method for producing the same. With the goal.
【0008】[0008]
【課題を解決するための手段】本発明者らは、上記した
課題を達成するため、歪発生の原因となる焼入れやオフ
ラインの熱処理を行うことなく、高強度と優れた加工性
を兼ね備えた鋼管を製造する方法について、鋭意研究し
た。その結果、特定範囲の組成を有する素材鋼管に、圧
延終了温度を400 ℃以上 800℃未満とする絞り圧延を行
い、圧延終了後空冷することにより、組織がマルテンサ
イトおよびフェライトあるいはさらに残留オーステナイ
トおよび/またはベイナイトの混合組織となり、オフラ
イン熱処理を行うことなく、高強度でかつ加工性に優れ
た製品管が得られることを見いだした。[Means for Solving the Problems] In order to achieve the above-mentioned objects, the present inventors have achieved a steel pipe having high strength and excellent workability without performing quenching or off-line heat treatment that causes strain. The method of manufacturing the was researched earnestly. As a result, a material steel pipe having a composition in a specific range is subjected to reduction rolling at a rolling end temperature of 400 ° C or higher and lower than 800 ° C, and air-cooled after the rolling, whereby the structure is martensite and ferrite or further retained austenite and / or It was also found that a product tube having a bainite mixed structure and having high strength and excellent workability can be obtained without performing off-line heat treatment.
【0009】本発明は、上記した知見に基づいて、 さら
に検討を加えて完成されたものである。すなわち、第1
の本発明は、質量%で、C:0.05〜0.30%、Si:0.01〜
2.0 %、Mn:1.0 〜4.0 %、Al:0.005 〜0.10%、S:
0.003 %以下を含有し、あるいはさらにCu:1%以下、
Ni:1%以下、Cr:0.05〜 1.0%、Mo:1%以下、Nb:
0.01〜 0.1%、Ti:0.01〜 0.1%、B:0.005 %以下の
うちから選ばれた1種または2種以上および/またはRE
M :0.02%以下、Ca:0.01%以下のうちから選ばれた1
種または2種を含有し、残部Feおよび不可避的不純物か
らなる組成を有し、引張強さが580Mpa超えで降伏比:70
%以下を有し、低温短時間熱処理を施したのちの降伏比
が80%以上となることを特徴とする加工性に優れる自動
車構造部材用高強度鋼管であり、また、 本発明では、組
織が、 マルテンサイト、 フェライトあるいはさらに残留
オーステナイトおよび/またはベイナイトを含む混合組
織であることが好ましい。The present invention has been completed by further studies based on the above findings. That is, the first
In the present invention, the mass% is C: 0.05 to 0.30%, Si: 0.01 to
2.0%, Mn: 1.0 to 4.0%, Al: 0.005 to 0.10%, S:
Contains 0.003% or less, or even Cu: 1% or less,
Ni: 1% or less, Cr: 0.05 to 1.0%, Mo: 1% or less, Nb:
0.01 to 0.1%, Ti: 0.01 to 0.1%, B: 0.005% or less and one or more selected from RE and / or RE
M: 0.02% or less, Ca: 0.01% or less selected 1
Type 1 or 2 type, with the composition consisting of balance Fe and unavoidable impurities, tensile strength above 580Mpa and yield ratio: 70
% Or less, the yield ratio after low-temperature short-time heat treatment is 80% or more, is a high-strength steel pipe for automobile structural members excellent in workability, and in the present invention, the structure , Martensite, ferrite, or a mixed structure containing retained austenite and / or bainite.
【0010】また、第2の本発明は、質量%で、C:0.
05〜0.30%、Si:0.01〜1.0 %、Mn:1.0 〜4.0 %、A
l:0.005 〜0.10%、S:0.003 %以下を含有し、ある
いはさらにCu:1%以下、Ni:1%以下、Cr:0.05〜
1.0%、Mo:1%以下、Nb:0.01〜 0.1%、Ti:0.01〜
0.1%、B:0.005 %以下のうちから選ばれた1種また
は2種以上および/またはREM :0.02%以下、Ca:0.01
%以下のうちから選ばれた1種または2種を含有し、好
ましくは残部Feおよび不可避的不純物からなる組成を有
する素材鋼管に、加熱および均熱処理を施したのち、圧
延終了温度:400 ℃以上 800℃未満、累積縮径率:20%
以上の絞り圧延を施して製品管とすることを特徴とする
加工性に優れた自動車構造部材用高強度鋼管の製造方法
である。なお、このようにして製造された製品管は、圧
延ままで引張強さが580Mpa超え、降伏比:70%以下を有
し、150 〜300 ℃で10〜20min の低温短時間熱処理を施
した後に、降伏応力が大きく上昇し、降伏比が80%以上
となる優れた低温短時間熱処理硬化性(塗装焼付け硬化
性)を有する。In the second aspect of the present invention, C: 0.
05 to 0.30%, Si: 0.01 to 1.0%, Mn: 1.0 to 4.0%, A
l: 0.005 to 0.10%, S: 0.003% or less, or further Cu: 1% or less, Ni: 1% or less, Cr: 0.05 to
1.0%, Mo: 1% or less, Nb: 0.01 to 0.1%, Ti: 0.01 to
0.1%, B: 0.005% or less, 1 or 2 or more selected, and / or REM: 0.02% or less, Ca: 0.01
% Or less, and preferably a raw steel tube having a composition consisting of the balance Fe and unavoidable impurities is heated and soaked, and then the rolling end temperature is 400 ℃ or more. Less than 800 ℃, cumulative reduction rate: 20%
A method for producing a high-strength steel pipe for automobile structural members, which is excellent in workability, characterized by performing the above-mentioned drawing rolling to obtain a product pipe. The product pipe manufactured in this way has an as-rolled tensile strength of more than 580 MPa and a yield ratio of 70% or less, and after being subjected to a low-temperature short-time heat treatment at 150 to 300 ° C for 10 to 20 min, It has an excellent low-temperature short-time heat treatment hardening property (paint bake hardening property) such that the yield stress is greatly increased and the yield ratio is 80% or more.
【0011】[0011]
【発明の実施の形態】本発明の自動車構造部材用高強度
鋼管は、引張強さTSが580 MPa 超えで、かつ降伏比Y
R(降伏強さYS/引張強さTS)が70%以下であり、
好ましくは限界拡管率が15%以上である、加工性に優れ
た高強度鋼管である。本発明の鋼管は、電縫鋼管、鍛接
鋼管等の溶接鋼管、あるいは継目無鋼管のいずれでもよ
く、その素材鋼管の製造方法には限定されない。BEST MODE FOR CARRYING OUT THE INVENTION The high-strength steel pipe for an automobile structural member according to the present invention has a tensile strength TS of more than 580 MPa and a yield ratio Y.
R (yield strength YS / tensile strength TS) is 70% or less,
A high-strength steel pipe having a limit expansion ratio of 15% or more and excellent in workability is preferable. The steel pipe of the present invention may be a welded steel pipe such as an electric resistance welded pipe, a forged steel pipe or the like, or a seamless steel pipe, and is not limited to the method for producing the raw material steel pipe.
【0012】なお、限界拡管率LBR (%)とは、 円形断
面自由バルジ変形させてバーストさせる自由バルジ試験
においてバーストしたときの試験体の最大外径dmax を
測定し、次式
LBR (%)={(dmax −d0 )/d0 }×100
(ここに、d0 :製品管(試験体)の外径)から算出さ
れた値である。The limit expansion rate LBR (%) is the maximum outer diameter d max of a test body when bursting in a free bulge test in which a free bulge is deformed in a circular cross section and bursted, and the following formula LBR (%) = {(D max −d 0 ) / d 0 } × 100 (where d 0 is the outer diameter of the product pipe (test body)).
【0013】さらに、本発明の自動車構造部材用高強度
鋼管は、低温短時間熱処理を施すことにより、降伏応力
が大きく上昇し、降伏比YRが80%以上となる特性を有
する。なお、本発明の自動車構造部材用高強度鋼管は、
歪量5%以下の予変形を施したのち、同様の低温短時間
熱処理を行っても同様の高降伏比が得られる。本発明で
いう「低温短時間熱処理」とは、150 〜300 ℃の温度で
10〜20min 保持する処理をいう。低温短時間熱処理の温
度が、150 ℃未満では大きな降伏応力の増加効果が得ら
れず、一方、300 ℃を超える温度では、引張強さが低下
するうえ、コスト高となる。また、低温短時間熱処理の
時間は、できるだけ短時間とすることが生産性、コスト
の面から好ましいが、10min 未満では十分な効果が得ら
れず、一方で20min を超えると、引張強さが低下する。Further, the high-strength steel pipe for automobile structural member of the present invention has a characteristic that the yield stress is greatly increased and the yield ratio YR is 80% or more when subjected to the heat treatment at a low temperature for a short time. The high-strength steel pipe for automobile structural members of the present invention,
The same high yield ratio can be obtained by performing a similar low temperature and short time heat treatment after performing a pre-deformation with a strain amount of 5% or less. The term "low-temperature short-time heat treatment" as used in the present invention means at a temperature of 150 to 300 ° C.
This is the process of holding for 10 to 20 minutes. If the temperature of the low-temperature short-time heat treatment is less than 150 ° C, a large effect of increasing the yield stress cannot be obtained. On the other hand, if the temperature exceeds 300 ° C, the tensile strength decreases and the cost increases. Also, it is preferable that the time of low temperature short time heat treatment is as short as possible from the viewpoint of productivity and cost, but if it is less than 10 min, a sufficient effect cannot be obtained, while if it exceeds 20 min, the tensile strength decreases. To do.
【0014】また、自動車用部材の場合、部品形状に成
形加工を施した後に、塗装、焼付け工程を経ることが多
い。塗装焼付け条件として、一般的には170 〜180 ℃で
20min 程度で行われる。本発明鋼管の場合は、従来のよ
うにQT(Quench-Temper )処理を施して強度や加工性
を確保する必要はなく、塗装焼付け時の熱を利用するこ
とにより所望の強度を確保することができる。また、上
記した低温短時間熱処理条件内であれば、加工性の低下
も少なく、加工性を保持したままで所望の強度を確保す
ることが可能となる。Further, in the case of automobile parts, after the parts are shaped, they are often painted and baked. Generally, the baking conditions are 170-180 ° C.
It takes about 20 minutes. In the case of the steel pipe of the present invention, it is not necessary to perform QT (Quench-Temper) treatment to secure the strength and workability as in the conventional case, but it is possible to secure the desired strength by utilizing the heat during baking of the coating. it can. Further, within the above-mentioned low-temperature short-time heat treatment condition, there is little deterioration in workability, and it becomes possible to secure desired strength while maintaining workability.
【0015】まず、本発明の自動車構造部材用高強度鋼
管の組成限定理由を説明する。以下、質量%は単に%と
記す。
C:0.05〜0.30%
Cは、基地中に固溶しあるいは他の元素と結合し炭化物
として析出し、鋼の強度増加に寄与する元素である。こ
のような効果を得るためには、0.05%以上の含有が必要
となる。一方、0.30%を超えて含有すると、溶接性が劣
化する。このため、本発明では、Cは0.05〜 0.30 %の
範囲に限定した。First, the reasons for limiting the composition of the high-strength steel pipe for automobile structural members of the present invention will be described. Hereinafter, mass% is simply referred to as%. C: 0.05 to 0.30% C is an element which forms a solid solution in the matrix or combines with other elements to precipitate as a carbide, which contributes to an increase in the strength of the steel. In order to obtain such effects, the content of 0.05% or more is required. On the other hand, if the content exceeds 0.30%, the weldability deteriorates. Therefore, in the present invention, C is limited to the range of 0.05 to 0.30%.
【0016】Si:0.01〜 2.0%
Siは、脱酸剤として作用するとともに、基地中に固溶し
鋼の強度を増加させる元素である。これらの効果は、0.
01%以上、好ましくは 0.10 %以上の含有で認められる
が、 2.0%を超える含有は延性を劣化させる。このた
め、Siは0.01〜 2.0%の範囲に限定した。なお、好まし
くは、0.01〜 1.0%である。Si: 0.01 to 2.0% Si is an element that acts as a deoxidizing agent and also forms a solid solution in the matrix to increase the strength of steel. These effects are 0.
It is recognized that the content is 01% or more, preferably 0.10% or more, but the content exceeding 2.0% deteriorates ductility. Therefore, Si is limited to the range of 0.01 to 2.0%. In addition, it is preferably 0.01 to 1.0%.
【0017】Mn:1.0 〜4.0 %
Mnは、鋼の強度を増加させ、また、焼入れ性を向上させ
圧延後の冷却時にマルテンサイト、残留オーステナイト
の形成を促進する作用を有する元素である。このような
効果は 1.0%以上の含有で認められるが、 4.0%を超え
る含有は延性を劣化させる。このため、Mnは 1.0〜 4.0
%の範囲に限定した。なお、好ましくは2.0 〜4.0 %で
ある。また、オフライン熱処理をせずに980MPa以上の高
強度を確保するためには、Mnは 2.5〜 4.0%の範囲とす
るのが好ましい。なお、より好ましくは、2.5 〜 3.0%
である。Mn: 1.0 to 4.0% Mn is an element having the functions of increasing the strength of steel, improving the hardenability, and promoting the formation of martensite and retained austenite during cooling after rolling. Such effects are recognized when the content is 1.0% or more, but the content exceeding 4.0% deteriorates ductility. Therefore, Mn is 1.0 to 4.0
It was limited to the range of%. The content is preferably 2.0 to 4.0%. Further, in order to secure high strength of 980 MPa or more without performing off-line heat treatment, it is preferable that Mn is in the range of 2.5 to 4.0%. More preferably, 2.5-3.0%
Is.
【0018】Al: 0.005〜0.10%
Alは、脱酸剤として作用することに加えて、結晶粒を微
細化する作用を有する元素である。この結晶粒微細化の
効果により、素材鋼管の組織を微細化し、本発明の効果
をより大きくする。このような効果は、0.005 %以上の
含有で認められるが、 0.10 %を超える含有は、酸化物
系介在物量を増加させ、清浄度を低下させる。このた
め、Alは 0.001〜0.10%の範囲に限定した。Al: 0.005 to 0.10% Al is an element which acts as a deoxidizing agent and, in addition, has an action of refining crystal grains. Due to the effect of refining the crystal grains, the structure of the material steel pipe is refined, and the effect of the present invention is further enhanced. Such an effect is recognized when the content is 0.005% or more, but the content exceeding 0.10% increases the amount of oxide inclusions and reduces the cleanliness. Therefore, Al is limited to the range of 0.001 to 0.10%.
【0019】S: 0.003%以下
Sは、鋼中で非金属介在物として存在し、この非金属介
在物を起点としてハイドロフォームなどの加工を行った
際に、鋼管が破断する場合がある。このため、Sはでき
るだけ低減することが耐破断性(ハイドロフォーミング
性)を改善するという観点から好ましい。しかし、0.00
3 %以下に低減すれば、耐破断性(ハイドロフォーミン
グ性)改善効果が現れる。このため、Sは0.003 %以下
に限定した。なお、好ましくは0.0010%以下である。S: 0.003% or less S is present as non-metallic inclusions in steel, and when a non-metallic inclusion is used as a starting point for processing a hydroform or the like, the steel pipe may break. Therefore, it is preferable to reduce S as much as possible from the viewpoint of improving the fracture resistance (hydroforming property). But 0.00
If it is reduced to 3% or less, the effect of improving the breakage resistance (hydroforming property) appears. Therefore, S is limited to 0.003% or less. The content is preferably 0.0010% or less.
【0020】上記した基本組成に加えて、下記に示す合
金元素を必要に応じ含有することが好ましい。
Cu:1%以下、Ni:1%以下、Cr:0.05〜 1.0%、Mo:
1%以下、Nb:0.01〜0.1%、Ti:0.01〜 0.1%、B:
0.005%以下のうちから選ばれた1種あるいは2種以
上、
Cu、Ni、Cr、Mo、Nb、Ti、Bは、いずれも強度を増加さ
せる元素であり、必要に応じ1種または2種以上含有で
きる。In addition to the above-mentioned basic composition, it is preferable to contain the following alloying elements as needed. Cu: 1% or less, Ni: 1% or less, Cr: 0.05 to 1.0%, Mo:
1% or less, Nb: 0.01 to 0.1%, Ti: 0.01 to 0.1%, B:
One or more selected from 0.005% or less, Cu, Ni, Cr, Mo, Nb, Ti, and B are all elements that increase the strength, and one or more selected if necessary. Can be included.
【0021】Cu、Ni、Moは、強度を増加させることに加
えてさらに、変態点を低下させ、組織を微細化する効果
を有している。このような効果は、Cu:0.1 %以上、N
i:0.1 %以上、Mo:0.1 %以上をそれぞれ含有するこ
とにより顕著となる。一方、Cuを1%を超えて多量に含
有すると熱間加工性が劣化する。また、Niは強度増加と
ともに靱性をも改善するが、1%を超えて多量に含有し
ても、効果が飽和し、含有量に見合う効果が期待できな
くなる。また、Moを1%を超えて多量に含有すると、溶
接性、延性が劣化するうえコスト高となる。このような
ことから、Cu:1%以下、Ni:1%以下、Mo:1%以下
とするのが好ましい。Cu, Ni and Mo have the effect of lowering the transformation point and refining the structure in addition to increasing the strength. Such effects are as follows: Cu: 0.1% or more, N
It becomes remarkable by containing i: 0.1% or more and Mo: 0.1% or more, respectively. On the other hand, if Cu is contained in a large amount exceeding 1%, hot workability deteriorates. Further, Ni improves not only the strength but also the toughness, but even if it is contained in a large amount over 1%, the effect is saturated and the effect commensurate with the content cannot be expected. Further, if Mo is contained in a large amount exceeding 1%, weldability and ductility are deteriorated and the cost becomes high. Therefore, Cu: 1% or less, Ni: 1% or less, Mo: 1% or less is preferable.
【0022】Crは、焼入れ性を向上させて、マルテンサ
イトを生成させやすくして、強度を増加させるととも
に、 耐食性を向上させる元素である。このような効果は
0.05%以上の含有で認められる。一方、1.0 %を超えて
含有すると、溶接性、延性が劣化する。このため、Crは
0.05〜 1.0%の範囲に限定することが好ましい。Nbは、
炭化物、窒化物、あるいは炭窒化物として析出し、鋼の
高強度化に寄与する元素である。とくに、高温に加熱さ
れる接合部を有する溶接鋼管では、接合時の加熱過程で
の粒の微細化や、冷却過程でのフェライトの析出核とし
て作用し、接合部の硬化を防止する効果を有する。この
ような効果は、0.01%以上の含有で認められる。一方、
0.1 %を超えて多量に添加すると、溶接性、靱性ともに
劣化する。このため、Nbは0.01〜0.1 %に限定すること
が好ましい。Cr is an element that improves hardenability, facilitates the formation of martensite, increases strength, and improves corrosion resistance. Such an effect
It is recognized when the content is 0.05% or more. On the other hand, if the content exceeds 1.0%, the weldability and ductility deteriorate. Therefore, Cr is
It is preferable to limit the range to 0.05 to 1.0%. Nb is
It is an element that precipitates as carbides, nitrides, or carbonitrides and contributes to the strengthening of steel. In particular, in a welded steel pipe having a joint that is heated to a high temperature, it has the effect of refining the grains in the heating process during joining and acting as ferrite precipitation nuclei in the cooling process, and preventing hardening of the joint. . Such an effect is recognized when the content is 0.01% or more. on the other hand,
If added in excess of 0.1%, both weldability and toughness will deteriorate. Therefore, Nb is preferably limited to 0.01 to 0.1%.
【0023】Tiは、Nbと同様に、炭化物、窒化物、ある
いは炭窒化物として析出し、高強度化に寄与する元素で
ある。本発明では、0.01%以上の含有を必要とするが、
0.1%を超えて多量に添加すると、溶接性、靱性とも劣
化する。このため、Tiは0.01〜0.1 %に限定することが
好ましい。Bは、焼入れ性の向上を介して強度を向上さ
せる元素である。このような効果は、0.0005%以上の含
有で顕著となる。一方、0.005 %を超えて多量に含有す
ると溶接性、靱性とも劣化する。このため、Bは0.005
%以下に限定するのが好ましい。Ti, like Nb, is an element that precipitates as carbides, nitrides, or carbonitrides and contributes to strengthening. In the present invention, it is necessary to contain 0.01% or more,
If added in excess of 0.1%, both weldability and toughness will deteriorate. Therefore, Ti is preferably limited to 0.01 to 0.1%. B is an element that improves strength by improving hardenability. Such an effect becomes remarkable when the content is 0.0005% or more. On the other hand, if the content exceeds 0.005% in a large amount, both weldability and toughness deteriorate. Therefore, B is 0.005
It is preferably limited to not more than%.
【0024】REM :0.02%以下、Ca:0.01%以下のうち
から選ばれた1種あるいは2種
REM ,Caは、いずれも硫化物、酸化物、または酸硫化物
として鋼中に存在して、介在物の形状を球状化して、鋼
の加工性を向上させる作用を有し、必要に応じ選択して
含有できる。また、REM ,Caはともに、接合部を有する
溶接鋼管の接合部の硬化を防止する作用を有する。この
ような効果は、REM :0.003 %以上、Ca:0.003 %以上
で顕著となる。REM: 0.02% or less, Ca: 0.01% or less One or two kinds of REM and Ca are present in the steel as sulfides, oxides, or oxysulfides. It has the effect of making the shape of inclusions spherical and improving the workability of steel, and can be selected and contained as necessary. Further, both REM and Ca have an action of preventing hardening of the joint of the welded steel pipe having the joint. Such an effect becomes remarkable when REM: 0.003% or more and Ca: 0.003% or more.
【0025】一方、REM が0.02%、あるいはCaが0.01%
を超えると介在物が多くなりすぎ清浄度が低下し延性が
劣化する。このため、REM :0.02%以下、Ca:0.01%以
下とすることが好ましい。上記した成分以外の残部はFe
および不可避的不純物である。不可避的不純物として
は、N:0.01%以下、O:0.01%以下、P:0.10%以下
が許容できる。On the other hand, REM is 0.02% or Ca is 0.01%
If it exceeds, the inclusions will be excessive and the cleanliness will be lowered and the ductility will be deteriorated. Therefore, REM: 0.02% or less and Ca: 0.01% or less are preferable. The balance other than the above components is Fe
And unavoidable impurities. As unavoidable impurities, N: 0.01% or less, O: 0.01% or less, and P: 0.10% or less are acceptable.
【0026】つぎに、本発明鋼管の好ましい組織につい
て説明する。本発明鋼管は、マルテンサイトおよびフェ
ライトの混合組織、もしくはマルテンサイト、フェライ
トおよび残留オーステナイトの混合組織、あるいはマル
テンサイト、フェライトおよびベイナイトの混合組織、
あるいはマルテンサイト、フェライト、残留オーステナ
イトおよびベイナイトの混合組織を有することが好まし
い。混合組織におけるフェライトは、面積率で70%以下
とすることが好ましい。フェライトの存在量が面積率で
70%を超えて多くなると所望の高強度が確保できなくな
る。なお、より好ましくは、50%以下である。Next, a preferable structure of the steel pipe of the present invention will be described. The steel pipe of the present invention is a mixed structure of martensite and ferrite, or martensite, a mixed structure of ferrite and retained austenite, or a mixed structure of martensite, ferrite and bainite,
Alternatively, it preferably has a mixed structure of martensite, ferrite, retained austenite and bainite. The area ratio of the ferrite in the mixed structure is preferably 70% or less. The amount of ferrite is the area ratio
If it exceeds 70%, the desired high strength cannot be secured. Incidentally, it is more preferably 50% or less.
【0027】フェライト以外の残部は、主として、マル
テンサイトである。なお、残留オーステナイトは、面積
率で15%以下、ベイナイトは25%以下とすることが好ま
しい。残留オーステナイトが15%を超え、あるいはベイ
ナイトが25%を超えると所望の高強度が確保できなくな
る。つぎに、本発明の高強度鋼管の製造方法について説
明する。The balance other than ferrite is mainly martensite. The area ratio of retained austenite is preferably 15% or less, and that of bainite is preferably 25% or less. If the retained austenite exceeds 15% or the bainite exceeds 25%, the desired high strength cannot be secured. Next, a method for manufacturing the high strength steel pipe of the present invention will be described.
【0028】本発明の製造方法においては、上記した組
成を有する鋼管を素材鋼管(素管)として、 該素材鋼管
に、加熱および均熱処理を施したのち、絞り圧延を施し
て製品管とする。本発明では、素材鋼管の製造方法は、
通常公知の造管法がいずれも好適であり、特に限定する
必要はない。造管方法としては、例えば、帯鋼を冷間ま
たは熱間でロール成形あるいは曲げ加工してオープン管
とし、 該オープン管の両エッジ部を高周波電流を利用し
て融点以上に加熱しスクイズロールで衝合接合する電気
抵抗溶接法(素管名称:電縫管、熱管の場合は熱間電縫
管)、オープン管両エッジ部を固相圧接温度域に加熱し
圧接接合する固相圧接法(素管名称:固相圧接管)、鍛
接法(素管名称:鍛接管)およびマンネスマン式穿孔圧
延法(素管名称:継目無鋼管)のいずれも好適に使用で
きる。In the manufacturing method of the present invention, a steel pipe having the above-mentioned composition is used as a raw steel pipe (base pipe), and the raw steel pipe is heated and soaked, and then drawn and rolled to obtain a product pipe. In the present invention, the manufacturing method of the material steel pipe,
Any of the commonly known pipe making methods is suitable and is not particularly limited. As a method for producing a pipe, for example, a steel strip is cold or hot roll-formed or bent to form an open pipe, and both edge portions of the open pipe are heated to a melting point or higher by using a high frequency current and squeeze roll is used. Butt-joining electric resistance welding method (name of raw tube: ERW pipe, hot-welding pipe in case of hot pipe), solid-state pressure welding method of heating both edges of open pipe to solid-state pressure welding temperature range and pressure welding It is possible to suitably use any of the name of the raw pipe: solid-phase pressure welded pipe), the forge welding method (name of the raw pipe: forged pipe) and the Mannesmann-type piercing and rolling method (name of the raw pipe: seamless steel pipe).
【0029】上記した組成を有し、好ましくは上記した
造管法のいずれかで製造された素材鋼管に、まず、加熱
あるいは均熱処理を施す。素材鋼管に施す加熱処理ある
いは均熱処理の条件は、後述する絞り圧延条件を満足す
ることができればとくに限定されないが、Ac3 変態点〜
Ac1 変態点間に加熱するか、あるいはAc3 変態点以上に
加熱し、 冷却することにより絞り圧延条件を満足するよ
うに調整することが好ましい。なお、素材鋼管の製造が
温間または熱間で行われ、絞り圧延に際し、充分な温度
を保有している場合には、室温まで冷却することなく、
管温度分布の均熱化のために均熱処理を施すのみで充分
である。素材鋼管の保有する温度が低い場合には、加熱
処理を施すことが好ましい。なお、加熱処理に際し、必
ずしも室温まで冷却する必要はない。なお、本発明で
は、加熱または均熱処理後の冷却を適宜調整して、所望
の絞り圧延条件を満足させることが好ましい。The material steel pipe having the above-mentioned composition and preferably produced by any of the above-mentioned pipe-making methods is first subjected to heating or soaking. The conditions of the heat treatment or soaking treatment applied to the raw material steel pipe are not particularly limited as long as they can satisfy the reduction rolling conditions described below, but the Ac 3 transformation point to
It is preferable to adjust so as to satisfy the squeeze rolling conditions by heating between the Ac 1 transformation points or by heating to the Ac 3 transformation point or higher and cooling. The production of the raw material steel pipe is carried out warm or hot, and at the time of drawing rolling, if it has a sufficient temperature, without cooling to room temperature,
It is sufficient to carry out soaking for the uniform temperature distribution of the tube temperature. When the temperature of the raw steel pipe is low, it is preferable to perform heat treatment. Note that the heat treatment does not necessarily need to be cooled to room temperature. In the present invention, it is preferable to appropriately adjust the cooling after heating or soaking to satisfy the desired draw rolling condition.
【0030】加熱処理または均熱処理を施された素材鋼
管は、ついで絞り圧延を施される。絞り圧延は、累積縮
径率:20%以上、より好ましくは30%以上とすることが
好ましい。累積縮径率が20%未満では、圧延集合組織の
発達が不十分で高いr値が得られないため、優れた加工
性を確保できない。r値を高くする観点からは、累積縮
径率は高い方が好ましいが、生産性の観点からは上限を
95%とすることが望ましい。なお、 好ましくは40〜80%
である。The material steel pipe that has been subjected to the heat treatment or soaking is then subjected to squeeze rolling. The squeeze rolling is preferably performed with a cumulative diameter reduction ratio of 20% or more, more preferably 30% or more. If the cumulative diameter reduction ratio is less than 20%, the rolling texture is not sufficiently developed and a high r value cannot be obtained, so that excellent workability cannot be secured. From the viewpoint of increasing the r value, the cumulative diameter reduction ratio is preferably high, but from the viewpoint of productivity, the upper limit is set.
95% is preferable. In addition, preferably 40-80%
Is.
【0031】絞り圧延の圧延終了温度は400 ℃以上 800
℃未満、より好ましくは400 ℃以上700 ℃未満とするこ
とが好ましい。なお、より好ましくはα+γ二相域、あ
るいは二相域直上で、加工することが好ましい。α+γ
二相域、あるいは二相域直上で、加工することにより、
オ−ステナイトが不安定となり、フェライトへの変態が
促進され、オ−ステナイト(γ)分率が低下するため、
γへのC,Mnの濃縮が進行しやすくなり、焼入れ性が向
上する。The rolling end temperature of the draw rolling is 400 ° C. or higher 800
The temperature is preferably lower than ℃, more preferably from 400 ℃ to less than 700 ℃. In addition, it is more preferable to process in the α + γ two-phase region or directly above the two-phase region. α + γ
By processing in the two-phase region or directly above the two-phase region,
Since the austenite becomes unstable, the transformation to ferrite is promoted, and the austenite (γ) fraction decreases,
Concentration of C and Mn in γ is facilitated, and hardenability is improved.
【0032】絞り圧延の圧延終了温度が400 ℃未満で
は、圧延時の負荷が過大となるとともに、圧延時の加工
硬化量が大きくなり、そのため加工性が低下し、所望の
優れた加工性を確保することができなくなる。一方、絞
り圧延の圧延終了温度が 800℃以上では、低温短時間熱
処理硬化性が低下し、所望の低温短時間熱処理後の特性
が確保できなくなる。なお、圧延終了温度は高強度化の
観点から、マルテンサイトまたはベイナイト変態終了温
度以上とするのが好ましい。If the rolling finish temperature of the draw rolling is less than 400 ° C., the load during rolling becomes excessive and the amount of work hardening during rolling increases, so that the workability decreases and the desired excellent workability is secured. Can not do. On the other hand, when the rolling end temperature of the drawing rolling is 800 ° C. or higher, the low temperature short time heat treatment hardenability deteriorates, and desired properties after the low temperature short time heat treatment cannot be secured. The rolling end temperature is preferably equal to or higher than the martensite or bainite transformation end temperature from the viewpoint of increasing strength.
【0033】なお、絞り圧延終了後は、常法に従って冷
却すればよい。冷却は空冷または水冷いずれでもよい。
また、絞り圧延には、レデューサーと称される複数の孔
型圧延機をタンデムに配列した圧延機列を使用すること
が好ましい。なお、本発明では、絞り圧延は、潤滑下で
の圧延(潤滑圧延)とすることが好適である。絞り圧延
を潤滑圧延とすることにより、厚み方向の歪み分布が均
一となり、組織の微細化や集合組織の形成を厚み方向で
均一にすることができる。無潤滑圧延では、剪断効果に
より材料表層部にのみ圧延歪が集中し、厚み方向に不均
一な組織が形成される傾向となる。After the squeeze rolling is finished, it may be cooled according to a conventional method. Cooling may be either air cooling or water cooling.
Further, it is preferable to use a rolling mill train in which a plurality of hole rolling mills called reducers are arranged in tandem for the reduction rolling. In the present invention, the reduction rolling is preferably rolling under lubrication (lubrication rolling). When the reduction rolling is the lubrication rolling, the strain distribution in the thickness direction becomes uniform, so that the fine structure and the formation of texture can be made uniform in the thickness direction. In unlubricated rolling, rolling strain tends to concentrate only on the surface layer of the material due to the shearing effect, and a nonuniform structure tends to be formed in the thickness direction.
【0034】[0034]
【実施例】表1に示す組成の熱延鋼板(2.3 mm厚)を、
管状にロール成形した後、 両端を誘導加熱して衝合接合
し、溶接鋼管(電縫鋼管:外径 146mmφ)とした。これ
ら溶接鋼管を素材鋼管とし、素材鋼管に表2に示す加熱
処理を施し、さらに、表2に示す条件で絞り圧延を施
し、製品管とした。絞り圧延はダンデム配置のレデュー
サーを使用して行った。Example A hot rolled steel sheet (2.3 mm thick) having the composition shown in Table 1 was
After roll-forming into a tubular shape, both ends were induction-heated and abutted to form a welded steel pipe (electric resistance welded pipe: outer diameter 146 mmφ). These welded steel pipes were used as raw material pipes, the raw steel pipes were subjected to the heat treatment shown in Table 2, and further subjected to drawing rolling under the conditions shown in Table 2 to obtain product pipes. The squeeze rolling was performed using a reducer arranged in tandem.
【0035】得られた製品管について、組織、引張特
性、低温短時間熱処理硬化特性、引張曲げ特性、拡管率
を調査した。また、一部の鋼管については、自由バルジ
試験によりハイドロフォーム加工を行い、バーストした
時の拡管率を調査した。試験方法は下記のとおりであ
る。
(1)組織
各製品管から、試験片を採取し、管長手方向と直交する
断面について、光学顕微鏡、走査型電子顕微鏡を用いて
組織を撮像した。得られた組織写真について画像解析装
置を用い、組織の種類、組織分率を求めた。
(2)引張特性
各製品管から長手方向にJIS 12 A号試験片(標点間距離
50mm)を採取して、JIS Z 2241の規定に準拠して引張り
試験を実施し、降伏応力YS、引張強さTS、伸びE
l、加工硬化指数n値、およびランクフォード値r値を
求めた。The resulting product pipe was examined for structure, tensile properties, low temperature short time heat treatment hardening properties, tensile bending properties, and tube expansion ratio. In addition, some steel pipes were hydroformed by a free bulge test, and the pipe expansion ratio when burst was investigated. The test method is as follows. (1) Tissue A test piece was taken from each product tube, and the tissue of the cross section orthogonal to the tube longitudinal direction was imaged using an optical microscope and a scanning electron microscope. The type of tissue and the tissue fraction of the obtained tissue photograph were determined using an image analyzer. (2) Tensile property JIS 12 A test piece (gauge distance between each product pipe in the longitudinal direction)
50 mm) is sampled and subjected to a tensile test in accordance with JIS Z 2241, yield stress YS, tensile strength TS, elongation E
1, the work hardening index n value, and the Rankford value r value were determined.
【0036】n値は、5〜10%間の真応力の変化に対す
る真歪の変化の値、 すなわち、n=(lnσ10% ーln
σ5%)/(lne10% −lne5%)により求めた。なお、σ
は真応力、eは真歪である。また、r値は、引張試験に
おける板厚真歪に対する板幅真歪の比で定義される。The n value is the value of the change in true strain with respect to the change in true stress between 5 and 10%, that is, n = (lnσ 10% -ln
σ 5% ) / (lne 10% −lne 5% ). Note that σ
Is the true stress, and e is the true strain. The r value is defined by the ratio of the true strain of the plate width to the true strain of the plate thickness in the tensile test.
【0037】
r=ln(Wi /Wf )/ln(Ti /Tf )
ここで、Wi :最初の板幅、Wf :最終の板幅、Ti :
最初の板厚、Tf :最終の板厚。
ただし、板厚測定は、かなりの誤差を伴うためr、通常
は試験片の体積は一定であるとして、次式によりr値を
求める。R = ln (W i / W f ) / ln (T i / T f ), where W i : initial plate width, W f : final plate width, T i :
First plate thickness, T f : Final plate thickness. However, since the measurement of the plate thickness involves a considerable error, it is assumed that the volume of the test piece is usually constant, and the r value is calculated by the following equation.
【0038】r=ln(Wi /Wf )/ln(Lf Wf
/Li Wi )
ここで、Wi :最初の板幅、Wf :最終の板幅、Li :
最初の長さ、Lf :最終の長さ。
本発明では、r値は、引張試験片にゲージ長さが2mmの
歪ゲージを貼り付け、公称歪で6〜7%の引張を行った
時の長手方向の真歪、幅方向の真歪を測定し、前記式に
より算出した。
(3)低温短時間熱処理硬化特性
得られた各製品管から長手方向にJIS 12 A号試験片(標
点間距離50mm)を採取して、まず引張塑性歪5%を付与
する予変形を実施した。ついで、試験片に、 180℃×20
min の低温短時間熱処理を施した。 そして、引張試験片
に再引張りを行い、予変形時の最大応力と再引張り時の
0.2 %耐力との差を求め、低温短時間熱処理硬化量(B
H量)として低温短時間熱処理硬化特性を評価した。な
お、低温短時間熱処理後の降伏比についても測定した。
(4)拡管率
外径38.1mm以上の製品管を500 mmの長さに切断しハイド
ロフォーム用試験体とした。このハイドロフォーム用試
験体を、図1に示すように、 ハイドロフォーム加工装置
にセットし、試験体の両端から水を供給して、円形断面
自由バルジ変形させ、 バースト(破断)させた。バース
トしたときの試験体の最大外径dmax を測定し、 次式
LBR (%)={(dmax −d0 )/d0 }×100
(ここに、d0 :製品管(試験体)の外径)で限界拡管
率LBR を算出した。なお、使用した金型の断面図を図2
に示す。R = ln (W i / W f ) / ln (L f W f
/ L i W i ) where W i : the initial plate width, W f : the final plate width, L i :
First length, L f : Final length. In the present invention, the r value is the true strain in the longitudinal direction and the true strain in the width direction when a strain gauge having a gauge length of 2 mm is attached to a tensile test piece and a tensile strain of 6 to 7% is performed. It was measured and calculated by the above formula. (3) Low-temperature short-time heat treatment Hardening property JIS 12 A test pieces (gauge length 50 mm) are sampled in the longitudinal direction from each product pipe obtained, and first pre-deformed to give 5% tensile plastic strain. did. Then, on the test piece, 180 ℃ × 20
Heat treatment was performed at low temperature for a short time of min. Then, the tensile test piece is re-pulled, and the maximum stress at the time of pre-deformation and the
The difference from the 0.2% proof stress is calculated, and the low temperature short time heat treatment hardening amount (B
As the H content), the low temperature short time heat treatment hardening characteristics were evaluated. The yield ratio after the low temperature short time heat treatment was also measured. (4) Expansion ratio A product pipe with an outer diameter of 38.1 mm or more was cut into a length of 500 mm to obtain a test piece for hydroform. As shown in FIG. 1, this hydroform test body was set in a hydroform processing apparatus, and water was supplied from both ends of the test body to cause free bulge deformation in a circular cross section and burst (break). The maximum outer diameter d max of the test piece when bursted was measured, and the following equation LBR (%) = {(d max −d 0 ) / d 0 } × 100 (where d 0 : product pipe (test piece) Outer diameter) was used to calculate the limit expansion rate LBR. A cross-sectional view of the mold used is shown in FIG.
Shown in.
【0039】上部金型2a,下部金型2bは、ぞれぞれ
長さ方向両端側に、鋼管の外径dOに略等しい径の半筒
状面で構成される鋼管保持部3を有し、長さ方向中央部
には、径dc の半筒状変形部4および傾斜角θ=45°の
テーパー状変形部5よりなる変形部6を有する。なお、
変形部6の長さ1cはdO の2倍としている。また、半
円筒状変形部4の径dc は、鋼管の外径dO の2倍程度
あればよい。The upper die 2a and the lower die 2b each have a steel pipe holding portion 3 formed on each of both ends in the length direction, which is a semi-cylindrical surface having a diameter substantially equal to the outer diameter d O of the steel pipe. At the center in the length direction, there is a deforming portion 6 including a semi-cylindrical deforming portion 4 having a diameter d c and a tapered deforming portion 5 having an inclination angle θ = 45 °. In addition,
Length 1c of the deformation portion 6 is two times the d O. Further, the diameter d c of the semi-cylindrical deformable portion 4 may be about twice the outer diameter d O of the steel pipe.
【0040】試験方法の詳細についてさらに説明する。
図1に示すように、この上部金型2aと下部金型2bと
で、金型それぞれの鋼管保持部3に鋼管1が嵌まるよう
に鋼管1を挟み込む。この状態で、鋼管1の両端から該
鋼管1の内面側に、軸押シリンダ7aを介して水等の液
体を供給して、液圧Pを付与し、円形断面自由バルジ変
形させてバーストした時の最大外径dma x を測定する。
なお、図1中の8,9はぞれぞれ金型2a,2bが鋼管
が鋼管を挟み込んだ状態に保持しておくための、金型ホ
ルダ、アウターリングである。なお、ハイドロフォーム
では、管の両端を固定した場合と、管の両端から圧縮力
を加える場合(軸方向圧縮という)があるが、一般に、
管端圧縮の方が高い拡管率を得ることが可能である。こ
こでは、高い拡管率が得られるよう、管の両端から圧縮
力を適宜負荷した。この圧縮力の負荷は、図1におい
て、軸押シリンダ7a,7bに対して軸方向に圧縮力F
を負荷することにより実施できる。なお、ここで使用し
た金型寸法(図2)は、lC が127.0 mm、dc が127.0
mm、rd が5mm、lO が550 mm、θが45°であった。The details of the test method will be further described.
As shown in FIG. 1, the steel pipe 1 is sandwiched between the upper mold 2a and the lower mold 2b so that the steel pipe 1 is fitted in the steel pipe holding portion 3 of each mold. In this state, when a liquid such as water is supplied from both ends of the steel pipe 1 to the inner surface side of the steel pipe 1 through the shaft pressing cylinder 7a to apply the hydraulic pressure P, the circular cross-section is bulged and the burst occurs. measuring the maximum outer diameter d ma x of.
It should be noted that reference numerals 8 and 9 in FIG. 1 denote a mold holder and an outer ring for holding the molds 2a and 2b, respectively, with the steel pipe sandwiching the steel pipe. In hydroform, there are cases where both ends of the tube are fixed and cases where a compressive force is applied from both ends of the tube (called axial compression), but in general,
It is possible to obtain a higher expansion ratio by tube end compression. Here, a compressive force was appropriately applied from both ends of the tube so that a high expansion rate was obtained. The load of the compressive force is the compressive force F in the axial direction with respect to the shaft pressing cylinders 7a and 7b in FIG.
Can be carried out by loading. The mold dimensions used here (Fig. 2) are l C = 127.0 mm and d c = 127.0.
mm, r d is 5 mm, l O is 550 mm, theta was 45 °.
【0041】得られた結果を表3に示す。The results obtained are shown in Table 3.
【0042】[0042]
【表1】 [Table 1]
【0043】[0043]
【表2】 [Table 2]
【0044】[0044]
【表3】 [Table 3]
【0045】本発明例は、いずれも引張強さ580MPa超で
かつ、70%以下の低降伏比と高延性を有し、さらに、拡
管率LBR が高く、ハイドロフォーム性にも優れている。
さらに、低温短時間熱処理により、大きなBH量が得ら
れ、また降伏比も80%以上の高YRが得られている。し
たがって、本発明例はいずれも、加工後に高強度を確保
することが可能となる。一方、本発明の範囲を外れる比
較例では、引張強さが低いか、降伏比が高いか、LBR が
低いかして加工性が低下している。Each of the examples of the present invention has a tensile strength of more than 580 MPa, a low yield ratio of 70% or less and a high ductility, and further has a high pipe expansion ratio LBR and an excellent hydroforming property.
Further, a large amount of BH is obtained by the low temperature short time heat treatment, and a high YR with a yield ratio of 80% or more is obtained. Therefore, in all the examples of the present invention, high strength can be ensured after processing. On the other hand, in Comparative Examples out of the range of the present invention, the workability is lowered depending on whether the tensile strength is low, the yield ratio is high, or the LBR is low.
【0046】[0046]
【発明の効果】以上のように、本発明によれば、オフラ
イン熱処理を行うことなく、高強度でかつ加工性に優れ
た高強度鋼管を安価に製造することができ、産業上格段
の効果を奏する。また、本発明の高強度鋼管は、高強度
に加え、高延性で高い限界拡管率を有してハイドロフォ
ーム性に優れ、自動車構造部材用として自動車車体の軽
量化に寄与できるという効果もある。As described above, according to the present invention, it is possible to inexpensively produce a high-strength steel pipe having high strength and excellent workability without performing off-line heat treatment, which is a significant industrial advantage. Play. Further, the high-strength steel pipe of the present invention has not only high strength but also high ductility and high limit pipe expansion ratio, is excellent in hydroformability, and has an effect of contributing to weight reduction of an automobile body as an automobile structural member.
【図1】自由バルジ試験に用いるハイドロフォーミング
加工装置の構成の例を示す断面図である。FIG. 1 is a cross-sectional view showing an example of the configuration of a hydroforming apparatus used for a free bulge test.
【図2】自由バルジ試験に用いる金型の一例を示す断面
図である。FIG. 2 is a sectional view showing an example of a mold used for a free bulge test.
1 試験体(試験鋼管) 2 金型 2a 上部金型 2b 下部金型 3 鋼管保持部 4 半円筒状変形部 5 テーパ状変形部 6 変形部 7a、7b 軸押シリンダ 8 金型ホルダ 9 アウターリング 1 test body (test steel pipe) 2 mold 2a Upper mold 2b Lower mold 3 Steel pipe holder 4 Semi-cylindrical deformation part 5 Tapered deformation part 6 Deformation part 7a, 7b Axial push cylinder 8 Mold holder 9 Outer ring
───────────────────────────────────────────────────── フロントページの続き (72)発明者 河端 良和 愛知県半田市川崎町1丁目1番地 川崎製 鉄株式会社知多製造所内 (72)発明者 西森 正徳 愛知県半田市川崎町1丁目1番地 川崎製 鉄株式会社知多製造所内 (72)発明者 木村 光男 愛知県半田市川崎町1丁目1番地 川崎製 鉄株式会社知多製造所内 (72)発明者 橋本 裕二 愛知県半田市川崎町1丁目1番地 川崎製 鉄株式会社知多製造所内 ─────────────────────────────────────────────────── ─── Continued front page (72) Inventor Yoshikazu Kawabata 1-1 Kawasaki-cho, Handa-shi, Aichi Made in Kawasaki Chita Works of Iron Co., Ltd. (72) Inventor Masanori Nishimori 1-1 Kawasaki-cho, Handa-shi, Aichi Made in Kawasaki Chita Works of Iron Co., Ltd. (72) Inventor Mitsuo Kimura 1-1 Kawasaki-cho, Handa-shi, Aichi Made in Kawasaki Chita Works of Iron Co., Ltd. (72) Inventor Yuji Hashimoto 1-1 Kawasaki-cho, Handa-shi, Aichi Made in Kawasaki Chita Works of Iron Co., Ltd.
Claims (5)
%、 Mn:1.0 〜4.0 %、 Al:0.005 〜0.10
%、 S:0.003 %以下 を含有し、残部Feおよび不可避的不純物からなる組成を
有し、引張強さが580Mpa超えで降伏比:70%以下を有
し、低温短時間熱処理を施した後の降伏比が80%以上と
なることを特徴とする加工性に優れる自動車構造部材用
高強度鋼管。1. In mass%, C: 0.05 to 0.30%, Si: 0.01 to 2.0
%, Mn: 1.0 to 4.0%, Al: 0.005 to 0.10
%, S: 0.003% or less, having a composition consisting of the balance Fe and unavoidable impurities, having a tensile strength of more than 580 Mpa and a yield ratio of 70% or less. High-strength steel pipe for automobile structural members with excellent workability characterized by a yield ratio of 80% or more.
るいはさらに残留オーステナイトおよび/またはベイナ
イトを含む混合組織であることを特徴とする請求項1に
記載の自動車構造部材用高強度鋼管。2. The high-strength steel pipe for an automobile structural member according to claim 1, wherein the structure is martensite, ferrite, or a mixed structure containing retained austenite and / or bainite.
u:1%以下、Ni:1%以下、Cr:0.05〜 1.0%、Mo:
1%以下、Nb:0.01〜 0.1%、Ti:0.01〜 0.1%、B:
0.005 %以下のうちから選ばれた1種または2種以上を
含有することを特徴とする請求項1または2に記載の自
動車構造部材用高強度鋼管。3. In addition to the above composition, further, in% by mass, C
u: 1% or less, Ni: 1% or less, Cr: 0.05 to 1.0%, Mo:
1% or less, Nb: 0.01 to 0.1%, Ti: 0.01 to 0.1%, B:
The high-strength steel pipe for an automobile structural member according to claim 1 or 2, containing one or more selected from 0.005% or less.
M :0.02%以下、Ca:0.01%以下のうちから選ばれた1
種または2種を含有することを特徴とする請求項1ない
し3のいずれかに記載の自動車構造部材用高強度鋼管。4. In addition to the composition, further, in% by mass, RE
M: 0.02% or less, Ca: 0.01% or less selected 1
A high-strength steel pipe for an automobile structural member according to any one of claims 1 to 3, wherein the high-strength steel pipe contains one or two kinds.
%、 Mn:1.0 〜4.0 %、 Al:0.005 〜0.10
%、 S:0.003 %以下 を含む組成を有する素材鋼管に、加熱および均熱処理を
施したのち、圧延終了温度:400 ℃以上 800℃未満、累
積縮径率:20%以上の絞り圧延を施して、引張強さが58
0Mpa超えで降伏比:70%以下を有し、低温短時間熱処理
を施した後の降伏比が80%以上となる製品管とすること
を特徴とする加工性に優れた自動車構造部材用高強度鋼
管の製造方法。5. In mass%, C: 0.05 to 0.30%, Si: 0.01 to 2.0
%, Mn: 1.0 to 4.0%, Al: 0.005 to 0.10
%, S: 0.003% or less, the raw material steel pipe is subjected to heating and soaking, and then subjected to reduction rolling at a rolling end temperature of 400 ° C to less than 800 ° C and a cumulative reduction ratio of 20% or more. , Tensile strength is 58
High strength for automobile structural members with excellent workability characterized by a product pipe having a yield ratio of 70% or less at 0 Mpa or more and a yield ratio of 80% or more after heat treatment at low temperature for a short time. Steel pipe manufacturing method.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002218541A JP3975852B2 (en) | 2001-10-25 | 2002-07-26 | Steel pipe excellent in workability and manufacturing method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001-328429 | 2001-10-25 | ||
| JP2001328429 | 2001-10-25 | ||
| JP2002218541A JP3975852B2 (en) | 2001-10-25 | 2002-07-26 | Steel pipe excellent in workability and manufacturing method thereof |
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| Publication Number | Publication Date |
|---|---|
| JP2003201543A true JP2003201543A (en) | 2003-07-18 |
| JP3975852B2 JP3975852B2 (en) | 2007-09-12 |
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|---|---|---|---|
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| JP (1) | JP3975852B2 (en) |
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