SU628810A3 - Способ получени 1,5,-диметилтетралина - Google Patents

Способ получени 1,5,-диметилтетралина

Info

Publication number: SU628810A3
Authority: SU; USSR - Soviet Union
Prior art keywords: dmt; product; catalyst; dmn; cyclization
Prior art date: 1975-03-03

Application number

SU762328253A

Other languages

English (en)

Russian (ru)

Inventor

Мануэл Чонг Виктор (Сша)

Original Assignee

Сан Венчерс Инк Сша (Фирма)

Тейдзин Лтд Япония (Фирма)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-03-03

Filing date

1976-03-01

Publication date

1978-10-15

1976-03-01 Application filed by Сан Венчерс Инк Сша (Фирма), Тейдзин Лтд Япония (Фирма) filed Critical Сан Венчерс Инк Сша (Фирма)

1978-10-15 Application granted granted Critical

1978-10-15 Publication of SU628810A3 publication Critical patent/SU628810A3/ru

Links

238000000034 method Methods 0.000 title description 10
239000000047 product Substances 0.000 claims description 16
238000007363 ring formation reaction Methods 0.000 claims description 12
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 10
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
239000011787 zinc oxide Substances 0.000 claims description 5
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
238000004519 manufacturing process Methods 0.000 claims description 4
239000000741 silica gel Substances 0.000 claims description 4
229910002027 silica gel Inorganic materials 0.000 claims description 4
239000007795 chemical reaction product Substances 0.000 claims description 3
238000000746 purification Methods 0.000 claims description 3
238000001179 sorption measurement Methods 0.000 claims description 3
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 2
239000003456 ion exchange resin Substances 0.000 claims description 2
229920003303 ion-exchange polymer Polymers 0.000 claims description 2
229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
238000003776 cleavage reaction Methods 0.000 claims 1
239000006260 foam Substances 0.000 claims 1
230000007017 scission Effects 0.000 claims 1
YGYNBBAUIYTWBF-UHFFFAOYSA-N 2,6-dimethylnaphthalene Chemical compound C1=C(C)C=CC2=CC(C)=CC=C21 YGYNBBAUIYTWBF-UHFFFAOYSA-N 0.000 description 15
BMADLDGHUBLVMQ-UHFFFAOYSA-N 1,5-dimethyltetralin Chemical compound C1=CC=C2C(C)CCCC2=C1C BMADLDGHUBLVMQ-UHFFFAOYSA-N 0.000 description 14
239000003054 catalyst Substances 0.000 description 12
238000006356 dehydrogenation reaction Methods 0.000 description 10
239000003377 acid catalyst Substances 0.000 description 6
239000003463 adsorbent Substances 0.000 description 6
239000000463 material Substances 0.000 description 6
LRQYSMQNJLZKPS-UHFFFAOYSA-N 2,7-dimethylnaphthalene Chemical group C1=CC(C)=CC2=CC(C)=CC=C21 LRQYSMQNJLZKPS-UHFFFAOYSA-N 0.000 description 5
230000002378 acidificating effect Effects 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
239000000203 mixture Substances 0.000 description 3
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 3
SDDBCEWUYXVGCQ-UHFFFAOYSA-N 1,5-dimethylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1C SDDBCEWUYXVGCQ-UHFFFAOYSA-N 0.000 description 2
238000009835 boiling Methods 0.000 description 2
229930195733 hydrocarbon Natural products 0.000 description 2
150000002430 hydrocarbons Chemical class 0.000 description 2
239000002808 molecular sieve Substances 0.000 description 2
239000011347 resin Substances 0.000 description 2
229920005989 resin Polymers 0.000 description 2
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
239000010457 zeolite Substances 0.000 description 2
ABIPNDAVRBMCHV-UHFFFAOYSA-N 4,4-dimethyl-2,3-dihydro-1h-naphthalene Chemical class C1=CC=C2C(C)(C)CCCC2=C1 ABIPNDAVRBMCHV-UHFFFAOYSA-N 0.000 description 1
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
229910021536 Zeolite Inorganic materials 0.000 description 1
239000002253 acid Substances 0.000 description 1
230000002411 adverse Effects 0.000 description 1
239000003513 alkali Substances 0.000 description 1
CSDREXVUYHZDNP-UHFFFAOYSA-N alumanylidynesilicon Chemical compound [Al].[Si] CSDREXVUYHZDNP-UHFFFAOYSA-N 0.000 description 1
239000003957 anion exchange resin Substances 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
239000002585 base Substances 0.000 description 1
125000002091 cationic group Chemical group 0.000 description 1
150000001768 cations Chemical class 0.000 description 1
229920001429 chelating resin Polymers 0.000 description 1
238000010908 decantation Methods 0.000 description 1
230000018044 dehydration Effects 0.000 description 1
238000006297 dehydration reaction Methods 0.000 description 1
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
239000000374 eutectic mixture Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
239000012535 impurity Substances 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
238000006317 isomerization reaction Methods 0.000 description 1
XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
229910052808 lithium carbonate Inorganic materials 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
239000011707 mineral Substances 0.000 description 1
239000002245 particle Substances 0.000 description 1
229920001568 phenolic resin Polymers 0.000 description 1
239000005011 phenolic resin Substances 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
229910052697 platinum Inorganic materials 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
239000011734 sodium Substances 0.000 description 1
239000007787 solid Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/20—Polycyclic condensed hydrocarbons
- C07C15/24—Polycyclic condensed hydrocarbons containing two rings
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C13/00—Cyclic hydrocarbons containing rings other than, or in addition to, six-membered aromatic rings
- C07C13/28—Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof
- C07C13/32—Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with condensed rings
- C07C13/47—Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with condensed rings with a bicyclo ring system containing ten carbon atoms
- C07C13/48—Completely or partially hydrogenated naphthalenes
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
- C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
- C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
- C07C5/31—Rearrangement of carbon atoms in the hydrocarbon skeleton changing the number of rings
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
- C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Analytical Chemistry (AREA)
Oil, Petroleum & Natural Gas (AREA)
Water Supply & Treatment (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Treatment Of Liquids With Adsorbents In General (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)

SU762328253A 1975-03-03 1976-03-01 Способ получени 1,5,-диметилтетралина SU628810A3 (ru)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US55480175A	1975-03-03	1975-03-03

Publications (1)

Publication Number	Publication Date
SU628810A3 true SU628810A3 (ru)	1978-10-15

Family

ID=24214771

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SU762328253A SU628810A3 (ru)	1975-03-03	1976-03-01	Способ получени 1,5,-диметилтетралина

Country Status (8)

Country	Link
JP (1)	JPS51100054A (fr)
BE (1)	BE839122A (fr)
DE (1)	DE2608783A1 (fr)
FR (1)	FR2302987A1 (fr)
GB (1)	GB1538937A (fr)
IT (1)	IT1063334B (fr)
NL (1)	NL7602144A (fr)
SU (1)	SU628810A3 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6226512A (ja) *	1985-07-29	1987-02-04	Chino Corp	プログラムパタ−ン表示装置
JPS62237389A (ja) *	1986-04-07	1987-10-17	Harada Kogyo Kk	タイマ装置
JPS62235594A (ja) *	1986-04-07	1987-10-15	Harada Kogyo Kk	タイマ装置
JPS63310531A (ja) *	1987-06-11	1988-12-19	Sanyo Electric Co Ltd	電気機器のタイマ−時間表示装置
JPH046328A (ja) *	1990-04-24	1992-01-10	Matsushita Electric Works Ltd	床暖房コントローラ

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3244758A (en) *	1963-03-20	1966-04-05	Sun Oil Co	Reaction of aromatic hydrocarbons with diolefins
JPS4864061A (fr) *	1971-12-13	1973-09-05
JPS4918856A (fr) *	1972-02-28	1974-02-19

1976
- 1976-01-19 JP JP416776A patent/JPS51100054A/ja active Granted
- 1976-03-01 IT IT2073776A patent/IT1063334B/it active
- 1976-03-01 SU SU762328253A patent/SU628810A3/ru active
- 1976-03-02 GB GB825276A patent/GB1538937A/en not_active Expired
- 1976-03-02 FR FR7605811A patent/FR2302987A1/fr not_active Withdrawn
- 1976-03-02 NL NL7602144A patent/NL7602144A/xx not_active Application Discontinuation
- 1976-03-03 DE DE19762608783 patent/DE2608783A1/de active Pending
- 1976-03-03 BE BE164795A patent/BE839122A/fr unknown

Also Published As

Publication number	Publication date
JPS51100054A (ja)	1976-09-03
FR2302987A1 (fr)	1976-10-01
BE839122A (fr)	1976-09-03
GB1538937A (en)	1979-01-24
NL7602144A (nl)	1976-09-07
IT1063334B (it)	1985-02-11
JPS5610892B2 (fr)	1981-03-11
DE2608783A1 (de)	1976-09-16

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