WO1999052618A2

WO1999052618A2 - Filter for removing solids from liquids

Info

Publication number: WO1999052618A2
Application number: PCT/ZA1999/000016
Authority: WO
Inventors: William Graham
Original assignee: Garfield International Investments Ltd
Current assignee: Garfield International Investments Ltd
Priority date: 1998-04-15
Filing date: 1999-04-15
Publication date: 1999-10-21
Anticipated expiration: 2000-10-15
Also published as: CO4880803A1; NO20005195L; CN1296425A; JP2003526492A; KR20010040807A; GB2352985A; EE200000593A; AR019068A1; ID28081A; HUP0102953A3; PL343548A1; EP1077754A2; NO20005195D0; SK13962000A3; MA25864A1; IL137567A0; AU4102699A; IS5616A; BG104650A; PA8470701A1

Abstract

A filter (10) is disclosed which comprises a casing (18) having an inlet (42) for water to be purified. There is a first stage filter (12, 16, 58) for removing solids from the water. The water flows from the first stage filter to a second stage filter (66) for the purpose of subjecting the water to ultra filtration or micro filtration and/or to reverse osmosis.

Description

FILTER FOR REMOVING SOLIDS FROM LIQUIDS

FIELD OF THE INVENTION

THIS INVENTION relates to filters for removing solids from liquids. The

filter is particularly, but not exclusively, intended for the purpose of removing solids

from water in the purification of the water for drinking and other purposes such as for

use as boiler water.

BACKGROUND TO THE INVENTION

Water which is, without treatment, usable for drinking, agricultural or

industrial purposes is in extremely short supply. The sea, which constitutes the most

abundant source of water, carries a heavy load (30000 to 40000 parts per million) of

dissolved solids. Depending on the particular geographic region it also carries a

load of silt and/or sand in suspension. It must therefore be filtered and desalinated

before it can be used for any purpose whatsoever.

Water from rivers, lakes and underground sources is usually

contaminated with dissolved solids and with solid material which is suspended or

dispersed in the water. There can in addition be biological material requiring micro

or ultra filtration to remove it.

The object of the present invention is to provide a filter which is an improvement over known filters.

BRIEF DESCRIPTION OF THE INVENTION

According to one aspect of the present invention there is provided a

filter which comprises a casing having an inlet for water to be filtered, a first stage

filter within the casing for removing solid material from the water entering the casing

and a second stage filter within the casing to which the water flows from the first

stage filter, and which second stage filter includes reverse osmosis membranes for

performing ultra filtration or micro filtration and/or for removing solids that are

dissolved in the water.

In the preferred form said casing is of elongate form, said first and

second stage filters being adjacent to one another in the direction of the length of

said casing.

According to a further aspect of the present invention there is provided

a filter comprising an elongate casing bounding an elongate space, an inlet to said

space for water to be purified, an outlet from said space for permeate water, an

outlet from said space for brine, a first stage filter in said space for removing solids

from the water which has entered said space through said inlet, a chamber forming

part of said space and a second stage filter, the second stage filter including reverse

osmosis membranes for performing ultra filtration or micro filtration and/or for

removing solids that are dissolved in the water, the first stage filter, the chamber and the membranes being positioned so that water flows in the direction of the length of

the casing to pass through said first stage filter to said chamber and through the

second stage filter to said outlets from the chamber.

BRIEF DESCRIPTION OF THE DRAWINGS

For a better understanding of the present invention, and to show how

the same may be carried into effect, reference will now be made, by way of example,

to the accompanying drawings in which:

Figure 1 is a diagrammatic section through a filter in accordance with the

present invention, Figure 1 also showing the piping connected to the filter;

Figure 2 is a front view of a disc of the filter of Figure 1 , Figure 2 being to a

larger scale than Figure 1 ;

Figure 3 is a section through the disc on the line Ill-Ill of Figure 2;

Figure 4 is a rear view of the disc;

Figure 5 is a view, to a larger scale than Figures 2 to 4, of a spiral flow guide;

Figure 6 is a section, to a greatly exaggerated scale, illustrating the manner in

which a part of the filter operates;

Figure 7 is a pictorial view of a reverse osmosis cartridge;

Figure 8 is a section through a further form of filter;

Figure 9 is an end view of the filter of Figure 8;

Figure 10 is an "exploded" diagrammatic view of the filter of Figures 8 and 9;

Figure 11 is a pictorial view, to a larger scale, of part of the filter of Figures 8 o 10;

Figure 12 is a section through another form of filter;

Figure 13 is an end view of the filter of Figure 12; and

Figure 14 is an "exploded" diagrammatic view of the filter of Figures 12 and

13.

DETAILED DESCRIPTION OF THE DRAWINGS

The filter shown in Figure 1 is designated 10 and comprises a plurality

of porous pipes, the pipes being designated 12. Each pipe 12 has a hairpin bend 14

therein, and the ends of the pipes are attached to a disc 16 which fits in a cylindrical

casing 18. Seals (not shown) are provided between the casing 18 and the disc 16,

the seals fitting in the grooves 20 (see particularly Figure 3) which are formed in the

outer periphery of the disc 16.

Opposite ends of the casing are closed by end caps 22 and 24 which

are held in place by two part locking ring structures 26. The outer ring 28 of each

locking ring structure 26 is embedded in the wall of the casing 18 when the casing is

manufactured using glass fibre reinforcing and resin. The inner ring 30 is in the form

of a removable split ring which is decreased in diameter before being inserted into

the ring 28. The inner rings 30 can be removed by reducing their diameters and

sliding them out of the casing 18 thereby to release the end caps.

O-rings (not shown) seal between the end caps 22 and 24 and the casing 18, the O-rings being in grooves 32 and 34 of the end caps 22 and 24.

The end cap 22 and the disc 16 define a chamber 36 which contains

the pipes 12. A tube 38 extends through the end cap 22, across the chamber 36 and

terminates in communication with a central bore 40 of the disc 16. A bore 42 passes

through the end cap 22 and communicates with the chamber 36. A pump 44 is

connected to the bore 42 by a pipe 46 and feeds the water to be filtered to the

chamber 36 from a source 48. The pump 44 is also connected to a reservoir 50 of

clean, filtered water. Valves 52, 54 enable filtered or raw water selectively to be

pumped by the pump 44.

The disc 16 has bores 56 therethrough, each end of each pipe 12

communicating with a respective bore 56 and the pipes hanging in U-formation

below the disc 16 in the chamber 36. The bores 56 are not arranged axially but at an

angle (see Figures 2 to 4) so that water entering the conical vortex chamber

designated 58 formed in the upper face of the disc 16 swirls in the chamber 58. As

will be seen from Figures 2 and 4 the bores 56 are arranged in a spiral array.

A spiral flow guide 60 is integral with, or secured to, the disc 16 and is

within the vortex chamber 58. The guide lies within the peripheral flange 62 that

protrudes from the main body of the disc 16.

The chamber 58 constitutes one end portion of the space designated 64 which is bounded by the disc 16 and the end cap 24.

Within the space 64 there is a hollow envelope 66 comprising two

sheets of membrane material through which water can permeate. The two sheets

are welded or otherwise secured together around their peripheries. Any type of

membrane material can be used. For example ultra filtration membranes, micro

filtration membranes or reverse osmosis membranes can be employed. When the

sheets are welded together two tubes 68 and 70 are welded in. The tube 68 extends

from the envelope 66, through the walling of the casing 18 to a shut-off valve 72.

The valve 72 is connected to a source 74 of air or water under pressure.

The tube 70 passes through a central bore 76 of the end cap 24,

emerges from the casing 18 and is connected to a valve 78. A plurality of

side-by-side envelopes 66 forming a pack can be provided. Spacers 80 inside the

envelopes 66 and further spacers (not shown) between the envelopes 66 prevent

collapse of the envelopes in normal operation and also prevent excessive expansion

of the envelopes 66 when they are internally pressurized.

An outlet bore 82 for water containing any last remaining solids passes

through the end cap 24. A pipe 84 leads from the bore 82 to a T-piece 86. The other

pipes which connect to the T-piece are designated 88 and 90. The pipe 88 leads to

a valve 92 and the pipe 90 to a valve 94. Between the valve 94 and the pump 44 there is a T-piece 96. A valve

98 is connected between the pipe 46 and the T-piece 96. A branch pipe 100 leads

from the pipe 46 to a valve 102. The tube 38 is connected by a pipe 104 to a valve

106.

In use water containing solids that are to be filtered out is withdrawn

from the source 48 by the pump 44 and fed under pressure to the chamber 36 via

the T-piece 96, the valve 98 and the pipe 46. The pipes 12 filter out the bulk of the

solids in the water as will be described hereinafter.

The water which penetrates the walls of the pipes 12 through the pores

in the pipe walls enters their interiors, flows along the bores of the pipes 12, enters

the bores 56 and then flows into the vortex chamber 58.

The angle at which the bores 56 enter the vortex chamber 58, and the

provision of the spiral guide 60, promotes swirling of the water in the vortex chamber

58 and in the part of the space 64 immediately above the vortex chamber 58.

The valve 106 is fully open at start-up and the pressure in the space

64 causes an initially strong water outflow through the central bore 40, tube 38 and

pipe 104. This results in the creation of the vortex at the centre of the chamber 58.

The bulk of the solids not filtered out by the pipes 12 enters the bore 40. It will be understood that all the water that enters the bore 40 is flowing to

waste. The flow rate through the valve 106 is thus adjusted after start up until the

minimum outflow of water is obtained consistent with the continued existence of the

vortex. By adjustment of this flow rate it is possible to achieve a flow pattern in which

the so-called overflow vortex which normally exists co-axially with the main vortex is

suppressed. Experimental work has shown that the main vortex extends a distance

above the disc 16, steadily diminishing in strength and eventually becoming

undetectable. Above the main vortex there is an upward flow of water but little or no

overflow vortex capable of carrying particles upwardly with it.

The final stage in the filtering process takes place when the water

permeates through the membrane material constituting the envelopes 66. Solid

particles remain on the outside of the envelopes 66 and water which is substantially

devoid of solid particles flows through the tube 70 to the valve 78 and then to a

storage reservoir, water main or point of use.

The pressure at the outlet bore 76 of the filter 10 is monitored and,

when a pressure loss of sufficient magnitude is detected, an automatic cleaning

sequence is initiated.

The main part of the cleaning sequence involves closure of the valves

52, 98, 92 and 106 for a brief period and opening of the valves 54, 94 and 102 for a

brief period. This results in clean water being drawn from the reservoir 50 and pumped by the pump 44 through the valve 94 to the space 64. The increase in

pressure in the space 64 results in a commensurate increase in pressure in the

pipes 12. The reverse flow through the pores of the pipes 12 cleans the pipes as will

be described hereinafter. Cleaning of the pipes 12 is thus effected by temporarily

increasing their internal pressure above their external pressure.

The material dislodged from the outside of the pipes 12 exits from the

chamber 36 via the bore 42, pipe 100 and valve 102.

The reverse flow of water causes the vortex in the chamber 58 to

collapse. When the valves 52, 98, 92 and 106 re-open, and valves 54, 94 and 102

re-close, the valve 106 must be fully opened and then subsequently adjusted to

re-establish the vortex.

Because clean water is being fed to the space 64, flow of water

through the envelopes 66 is not interrupted during the cleaning procedure for the

pipes 12.

To clean the envelopes 66, the valve 72 is opened briefly, typically for

a second or less, and hence the envelopes 66 are inflated by air or water under

pressure. Simultaneously the valve 78 is closed briefly. The external spacers between the envelopes 66 prevent them over inflating and bursting. The sudden

expansion of the envelopes dislodges solid material which has adhered to the outside thereof and the general flow from the space 64 to the bore 82 carries away

the dislodged solid material which exits through the valve 92.

It will be understood that there is a tube 68 and a tube 70 for each

envelope 66. The tubes 68 and 70 lead to common manifolds.

The pipes 12 are of rubber, a rubber compound or a synthetic plastics

material which has a surface to which the solid material will not adhere strongly. The

type of surface required can be compared to that of a motor vehicle tyre. Whilst mud

will adhere to the tyre, the bond is not strong and the mud can, if dry, easily be

knocked off or, if wet, can easily be washed off.

Each pipe 12 has therein a plurality of pores which extend from the

outer surface of the pipe to the inner surface of the pipe. One such pore, designated

108, is shown in Figure 6. The pore 108 is, at the external surface of the pipe, wider

than at the internal surface of the pipe. Preferably the diameter at the outer end of

the pore is in the region of five microns and at the inner end of the pore is of the

order of one micron or two microns. The pipe wall thickness is about 15mm.

Grains of solid material, designated 110 in Figure 3, lodge in the pores

108 and, within a short period of time after start up (from a few seconds to a few

minutes), each pore 108 has therein a mass of grains which act as a filter allowing water to permeate into the hollow interior of the pipe 12 but preventing other solid material from passing through. It will be understood that as the water passes

through the filter constituted by the grains in each pore 108, the solid material that

was entrained therein is deposited onto the outer surface of the pipe 12. This

accumulation of solid material is designated 112 in Figure 6. When flow in the

reverse direction through the pores 108 occurs as described the accumulations of

solid material are swept away.

It has also been found that the pressure drop across each pore 108

should not be excessive. If the pressure drop is excessive the grains 110 in the

pores 108 and the solids accumulation 112 are sucked into the pores 108 with such

force that it becomes difficult to dislodge the accumulation 112 of material. The

pores 108 are thus blocked and flow through the filter from the pipe 46, through the

pores 108 in the pipes 12 to the hollow interiors of the pipes and thence to the vortex

chamber 58 drops significantly.

The envelopes 66 can be replaced by a spirally wound membrane, for

example, a reverse osmosis membrane in the form of a cartridge 114 as shown in

Figure 7. Such a filter will be described in more detail with reference to Figures 12,

13 and 14.

The cartridge 114 comprises a central pipe 116 around which reverse

osmosis packages 118 each comprising two sheets 120, 122 of complex polymer

and an intervening spacer 124 are wound. The pipe 116 has holes 126 in it, the holes being in rows extending along the pipe. Water in the permeate passages

designated 128 enters the pipe 116 through these holes. The salt retention

passages are designated 130.

Two sheets 120 and 122 are welded together around three of their

edges to form each package 118. The fourth edges are not welded together but

secured by adhesive to the pipe 116 on opposite sides of a row of holes 126 in the

pipe 116. Thus each row of holes 126 is in communication with the permeate

passage 128 of a respective package.

In Figure 7, simply for illustrative purposes, the membrane sheets 120

and 122 of the top package 118 are shown separated so that the spacer 124 can be

seen. The other packages 118 are shown as having the edges of the sheets 120

and 122 welded togther so that the spacer 124 is concealed.

The number of packages 118 used depends on the number of rows of

holes 126 because each package must be positioned so that its permeate passage

128 communicates with a respective row of holes.

Once wound onto the pipe 116, the membrane sheets 120 and 122 of

each package 118 are in face-to-face contact with the sheets 120 and 122 of the

adjacent packages 118. Once all the packages 118 have had the inner edges of their sheets

120 and 122 adhered to the pipe 116, the packages are wound tightly around the

pipe 116 and then taped to prevent them unwinding. An outer sleeve (not shown) is

then provided to prevent the packages 118 bursting when pressure is applied to the

sheets 120 and 122 upon feed water being introduced into the cartridge 114. The

outer sleeve fits into the casing 18.

It will be understood that the passages 130 are open at both axial ends

of the wound cartridge.

The cartridge is used in conjunction with two end caps designated 132

and 134. The end cap 132 comprises a disc 136 and a flange 138 which extends

around the periphery of the disc 136. The cap 132 is at the end of the cartridge from

which the brine stream emerges. The disc 136 has in it a central hole 140 which

registers with the pipe 116 and a plurality of holes 142 through which the brine

stream flows. There is a gap of, for example, two to four centimetres between the

end of the cartridge and the disc 136. The function of the end cap 132 is to cause a

back pressure immediately adjacent the exit ends of the brine passages. The axes

of the holes 140, 142 are parallel to the axis of the pipe 116.

The end cap 134 is at the inlet end of the cartridge. It comprises a disc

144 having a central hole 146 which registers with the pipe 116 and a plurality of

holes 148 between the hole 146 and a peripheral flange 150 that extends around the periphery of the disc 144. The disc 144 can be against the end of the cartridge

or up to four centimetres from the cartridge.

The axes of the holes 148 are not parallel to the axis of the pipe 116

but are at an angle to it. This results in the discrete streams of water which pass

through the holes 148 and impinge on the end of the cartridge 114 doing so at an

angle and not along paths parallel to the pipe 116. The orientation of the holes is

such that the streams swirl in the same direction as the packages are wound.

It will be understood that the cartridge 114 is positioned with the end

cap 134 adjacent the disc 16 and the end cap 132 at the other end of the casing 18

adjacent the end cap 24.

Turning now to Figures 8 to 11 this illustrates a filter 152 which

comprises a casing 154 in which there is a membrane cartridge 114 of the type

described with reference to Figure 7 and a pre-filter designated 156. The prefilter

156 comprises three cylinders 158 including walls of mesh screening material. The

cylinders 158 are in a chamber 160. The inlet to the chamber 160 is designated

162. The water flows through the walls of the mesh cylinders 158 into the interiors

of the cylinders and from the interiors of the cylinders 158 to a further chamber 164

via bores 166. The chamber 164 is bounded on one side by a disc 168 on which the cylinders 158 are mounted and in which the bores 166 are formed and on the other

side by the end cap 134 of the cartridge 114.

The brine outlet from the cartridge 114 is designated 170 and the

permeated water outlet is designated 172, these being in an end cap 174.

The cartridge 114 and disc 168 are held in place by spacers

designated 176, 178 and 180. The inlet 162 is in an end cap 182, there being ring

structures 184 and 186 for holding the end cap 182 and the end cap 174 in place.

Piping generally designated 188 connects the interiors of the cylinders

158 to an outlet 190 in the end cap 182. A waste pipe 192 leads from the chamber

164 through the end cap 182 to waste.

During normal operation water with solids entrained in it enters the

filter through the inlet 162, flows through the mesh cylinders 158, through the bores

166, across the chamber 164 and thence into the salt retention passages of the

cartridge 114. Permeate emerges through the outlet 172 and brine emerges

through the outlet 170.

To clean the filter, water under pressure is supplied to the outlet 172,

the water flowing from the permeate passages through the membranes to the salt

retention passages. On emerging from the salt retention passages into the chamber 164, some of the water can flow to waste through the pipe 192.

The remainder of the water flows through the bores 166 into the

cylinders 158. A portion of the water entering the cylinders 158 flows through the

mesh to clean the outside surfaces of the cylinders. The remainder of the water

flows through the piping 188 to the outlet 190 carrying with it solid material which

had previously passed through the mesh of the cylinders 158.

The piping shown in Figure 1 is modified to enable a cartridge to be

cleaned by removing the tube 68 and connecting the valve 72 and water source 74

directly to the bore 76. The valve 78 is closed whilst membrane cleaning takes

place.

Turning finally to Figures 12, 13 and 14 this illustrates a filter similar to

that shown in Figure 1 but which has a cartridge 114 in place of the envelopes 66.

Furthermore it is similar in construction to the filter of Figures 8 to 11 but in place of

the mesh cylinders 158 it has pipes 12 as described with reference to Figure 1.

The end cap 134 of Figure 14 is shown as having a pattern of holes

that differs from that shown in Figure 10. Otherwise, where applicable, like

reference numerals have been used in Figures 12, 13 and 14 on the one hand and 8

to 11 on the other hand. The filter of Figures 12 to 14 is cleaned in the same way as described

above in relation to the filter of Figures 8 to 11.

Filters which include the vortex chamber 58 are operated in a vertical

position as shown in Figures 1 and 12. The filter of Figures 12 to 14 hence has to

be operated in a vertical position. The filter of Figures 8 to 11 can be operated

horizontally.

The pipes 12 can remove all solids above twelve microns in size. The

filter cylinders 158, depending on the mesh used, remove all solids above about 20

micron. The type of prefilter selected depends on the solids load of the feed water

and the desired final water quality.

It is possible, in place of the hoses 12 and the cylinders 158, to use a

disc filter, preferably a self cleaning disc filter, or any other type of filter which will

remove solid material down to the requisite size before the water flows to the

cartridge 114 or envelopes 66 for ultra or micro filtration or for the removal of

dissolved solids.

If small balls of a rubber-like material are placed in the chamber 160,

these are displaced by the flowing water and tend to "bounce" around in the

chamber keeping the solids in suspension and thus assisting in preventing clogging

of the filter. It is also possible to clean membranes by suddenly closing a valve in

the permeated water pipe. The shock wave passing in the reverse direction shakes

loose solids in the salt retention passages. A similar effect can be obtained by

feeding air under pressure into the permeate water pipe.

It is also possible to provide electrical coils around the cartridge 114 as

described in the specification of PCT application PCT/GB98/0054 (WO 98/30501 )

for the purpose of enhancing the performance of the cartridge. In Figures 8 and 12

the coils are designated 194, 196 and 198. They are embedded in the walls of the

casing as the casing is fabricated.

Claims

CLAIMS:

1. A filter which comprises a casing having an inlet for water to be filtered,

a first stage filter within the casing for removing solid material from the water

entering the casing and a second stage filter within the casing to which the water

flows from the first stage filter, and which second stage filter includes reverse

removing solids that are dissolved in the water.

2. A filter according to claim 1 , wherein said casing is of elongate form,

said first and second stage filters being adjacent to one another in the direction of

the length of said casing.

3. A filter according to claim 1 , wherein said casing is vertical and there is

an inlet at the lower end of the casing for feeding water to be purified into an inlet

chamber with the casing, a disc forming part of said first stage filter and constituting

the upper end of said chamber, a plurality of bores in said disc, a vortex chamber in

the upper face of said disc, the vortex chamber having the shape of an inverted

cone, the plurality of bores passing through said disc and entering said vortex

chamber, the bores being so orientated that water flowing into said vortex chamber

from the bores swirls in said chamber, an exit from said vortex chamber passing

downwardly through said disc from the apex of said vortex chamber, and a plurality

of pipes with porous walls in said chamber, the interiors of said pipes being in communication with said bores.

4. A filter according to claim 3, wherein said bores open into said vortex

chamber in a spiral array.

5. A filter according to claim 3 or 4, and including a spiral guide in said

vortex chamber for promoting spiral flow of water in said vortex chamber.

6. A filter according to claim 3 or 4, wherein each pipe has each of its

ends in communication with a respective one of said bores, each pipe hanging in

said inlet chamber in a U-shape.

7. A filter according to claim 1 , 2, 3 or 4, wherein said first stage filter is

constituted by a filter comprising a plurality of filter elements which are pressed

together and which define filter passages therebetween.

8. A filter according to claim 1, 2, 3 or 4, wherein said first stage filter

comprises a plurality of screens through which the water flows, the screens retaining

the solid material thereon.

9. A filter according to claim 1 , wherein said second stage filter comprises

a plurality of closed envelopes of reverse osmosis membrane in a second stage

chamber to which water flows from the first stage filter, a permeated water outlet from the interior of each envelope, means for feeding fluid under pressure to said

envelopes thereby temporarily to inflate the envelopes, and an outlet from said

second stage chamber for water with solids therein which have been separated out

from the permeate water.

10. A filter according to claim 1 , wherein said second stage filter comprises

reverse osmosis membranes wound around a permeate water pipe, the wound

membranes being in a second stage chamber to which the water flows from the first

stage filter, there being means for feeding clean water under pressure into said

permeate pipe for backwashing the membranes.

11. A filter according to claim 1 , wherein said first stage filter comprises a

plurality of compartments having walls of screening material, said compartments

being in an inlet chamber of the filter, a first outlet from each compartment leading to

said second stage filter, a second outlet from each compartment, there being a

normally closed valve in said second outlet and means for feeding water through

said screening material from inside the compartment to said inlet chamber thereby to

clean said screening material and for feeding water through said compartments to

said second outlet whilst said normally closed valve is open.

12. A filter comprising an elongate casing bounding an elongate space, an

inlet to said space for water to be purified, an outlet from said space for permeate

water, an outlet from said space for brine, a first stage filter in said space for removing solids from the water which has entered said space through said inlet, a

chamber forming part of said space and a second stage filter, the second stage filter

including reverse osmosis membranes for performing ultra filtration or micro filtration

and/or for removing solids that are dissolved in the water, the first stage filter, the

chamber and the membranes being positioned so that water flows in the direction of

the length of the casing to pass through said first stage filter to said chamber and

through the second stage filter to said outlets from the chamber.