WO2004057253A3 - Lean reflux-high hydrocarbon recovery process - Google Patents

Lean reflux-high hydrocarbon recovery process Download PDF

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Publication number
WO2004057253A3
WO2004057253A3 PCT/US2003/040733 US0340733W WO2004057253A3 WO 2004057253 A3 WO2004057253 A3 WO 2004057253A3 US 0340733 W US0340733 W US 0340733W WO 2004057253 A3 WO2004057253 A3 WO 2004057253A3
Authority
WO
WIPO (PCT)
Prior art keywords
stream
absorber
sent
feed
bottoms
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2003/040733
Other languages
French (fr)
Other versions
WO2004057253B1 (en
WO2004057253A2 (en
Inventor
Sanjiv N Patel
Jorge H Foglietta
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lummus Technology LLC
Original Assignee
ABB Lummus Global Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ABB Lummus Global Inc filed Critical ABB Lummus Global Inc
Priority to CA2510022A priority Critical patent/CA2510022C/en
Priority to EP03813816.0A priority patent/EP1588111B1/en
Priority to AU2003297417A priority patent/AU2003297417B2/en
Priority to JP2004562340A priority patent/JP5276763B2/en
Publication of WO2004057253A2 publication Critical patent/WO2004057253A2/en
Publication of WO2004057253A3 publication Critical patent/WO2004057253A3/en
Publication of WO2004057253B1 publication Critical patent/WO2004057253B1/en
Anticipated expiration legal-status Critical
Priority to NO20053375A priority patent/NO339135B1/en
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/005—Processes comprising at least two steps in series
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/11—Purification; Separation; Use of additives by absorption, i.e. purification or separation of gaseous hydrocarbons with the aid of liquids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G5/00—Recovery of liquid hydrocarbon mixtures from gases, e.g. natural gas
    • C10G5/04—Recovery of liquid hydrocarbon mixtures from gases, e.g. natural gas with liquid absorbents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G5/00—Recovery of liquid hydrocarbon mixtures from gases, e.g. natural gas
    • C10G5/06—Recovery of liquid hydrocarbon mixtures from gases, e.g. natural gas by cooling or compressing
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0209—Natural gas or substitute natural gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0219—Refinery gas, cracking gas, coke oven gas, gaseous mixtures containing aliphatic unsaturated CnHm or gaseous mixtures of undefined nature
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0233—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 1 carbon atom or more
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0238—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 2 carbon atoms or more
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0242—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 3 carbon atoms or more
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/02—Processes or apparatus using separation by rectification in a single pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/04—Processes or apparatus using separation by rectification in a dual pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/30—Processes or apparatus using separation by rectification using a side column in a single pressure column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/70—Refluxing the column with a condensed part of the feed stream, i.e. fractionator top is stripped or self-rectified
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/76—Refluxing the column with condensed overhead gas being cycled in a quasi-closed loop refrigeration cycle
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/78—Refluxing the column with a liquid stream originating from an upstream or downstream fractionator column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/02—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum
    • F25J2205/04—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum in the feed line, i.e. upstream of the fractionation step
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/12—Refinery or petrochemical off-gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2230/00—Processes or apparatus involving steps for increasing the pressure of gaseous process streams
    • F25J2230/60—Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being hydrocarbons or a mixture of hydrocarbons
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/60—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being (a mixture of) hydrocarbons
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/02—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/12—External refrigeration with liquid vaporising loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/60—Closed external refrigeration cycle with single component refrigerant [SCR], e.g. C1-, C2- or C3-hydrocarbons
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/90—External refrigeration, e.g. conventional closed-loop mechanical refrigeration unit using Freon or NH3, unspecified external refrigeration
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/40—Vertical layout or arrangement of cold equipments within in the cold box, e.g. columns, condensers, heat exchangers etc.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treating Waste Gases (AREA)

Abstract

A two-tower scheme process for the recovery of propane and heavier components from a hydrocarbon gas stream is provided. Feed gas (12) is cooled (14), partially condensed, and then separated (24) to give a first liquid stream (22) and a first vapor stream (26). First liquid stream is sent to a distillation tower (28) that recovers at the bottoms a major portion of propane and heavier components (54) and produces an overhead gas stream (42). First vapor stream (26) is expanded (30) and sent as bottom feed (34) to the absorber. Absorber produces an absorber overhead stream (16) containing essentially all the ethane and lighter components and an absorber bottoms stream (18). Absorber bottoms stream is heated (14) and sent to the distillation tower (28) as middle feed (52). Absorber overhead stream is warmed (40) and optionally compressed (48, 49). A part of the compressed stream (20) is substantially condensed and sent to absorber as top feed. The process and apparatus can be used to recover ethane and heavier hydrocarbons.
PCT/US2003/040733 2002-12-19 2003-12-19 Lean reflux-high hydrocarbon recovery process Ceased WO2004057253A2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CA2510022A CA2510022C (en) 2002-12-19 2003-12-19 Lean reflux-high hydrocarbon recovery process
EP03813816.0A EP1588111B1 (en) 2002-12-19 2003-12-19 Lean reflux-high hydrocarbon recovery process
AU2003297417A AU2003297417B2 (en) 2002-12-19 2003-12-19 Lean reflux-high hydrocarbon recovery process
JP2004562340A JP5276763B2 (en) 2002-12-19 2003-12-19 Low reflux and high yield hydrocarbon recovery method
NO20053375A NO339135B1 (en) 2002-12-19 2005-07-11 Process for the recovery of hydrocarbons from gas stream containing methane.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US43511902P 2002-12-19 2002-12-19
US60/435,119 2002-12-19

Publications (3)

Publication Number Publication Date
WO2004057253A2 WO2004057253A2 (en) 2004-07-08
WO2004057253A3 true WO2004057253A3 (en) 2004-10-07
WO2004057253B1 WO2004057253B1 (en) 2004-11-25

Family

ID=32682162

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2003/040733 Ceased WO2004057253A2 (en) 2002-12-19 2003-12-19 Lean reflux-high hydrocarbon recovery process

Country Status (8)

Country Link
US (1) US7069744B2 (en)
EP (1) EP1588111B1 (en)
JP (2) JP5276763B2 (en)
KR (1) KR101035819B1 (en)
AU (1) AU2003297417B2 (en)
CA (1) CA2510022C (en)
NO (1) NO339135B1 (en)
WO (1) WO2004057253A2 (en)

Families Citing this family (57)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7159417B2 (en) * 2004-03-18 2007-01-09 Abb Lummus Global, Inc. Hydrocarbon recovery process utilizing enhanced reflux streams
US7316127B2 (en) * 2004-04-15 2008-01-08 Abb Lummus Global Inc. Hydrocarbon gas processing for rich gas streams
US7219513B1 (en) 2004-11-01 2007-05-22 Hussein Mohamed Ismail Mostafa Ethane plus and HHH process for NGL recovery
WO2006115597A2 (en) * 2005-04-20 2006-11-02 Fluor Technologies Corporation Integrated ngl recovery and lng liquefaction
US20060260330A1 (en) 2005-05-19 2006-11-23 Rosetta Martin J Air vaporizor
WO2008008335A2 (en) * 2006-07-10 2008-01-17 Fluor Technologies Corporation Configurations and methods for rich gas conditioning for ngl recovery
JP5356238B2 (en) * 2006-10-24 2013-12-04 シエル・インターナシヨネイル・リサーチ・マーチヤツピイ・ベー・ウイ Method and apparatus for treating hydrocarbon streams
US8650906B2 (en) * 2007-04-25 2014-02-18 Black & Veatch Corporation System and method for recovering and liquefying boil-off gas
US9103585B2 (en) * 2007-08-14 2015-08-11 Fluor Technologies Corporation Configurations and methods for improved natural gas liquids recovery
US9243842B2 (en) * 2008-02-15 2016-01-26 Black & Veatch Corporation Combined synthesis gas separation and LNG production method and system
US9528759B2 (en) * 2008-05-08 2016-12-27 Conocophillips Company Enhanced nitrogen removal in an LNG facility
US10113127B2 (en) 2010-04-16 2018-10-30 Black & Veatch Holding Company Process for separating nitrogen from a natural gas stream with nitrogen stripping in the production of liquefied natural gas
US9777960B2 (en) 2010-12-01 2017-10-03 Black & Veatch Holding Company NGL recovery from natural gas using a mixed refrigerant
US10451344B2 (en) 2010-12-23 2019-10-22 Fluor Technologies Corporation Ethane recovery and ethane rejection methods and configurations
WO2013033711A1 (en) * 2011-09-01 2013-03-07 Gtlpetrol Llc Integration of ft system and syn-gas generation
US10139157B2 (en) 2012-02-22 2018-11-27 Black & Veatch Holding Company NGL recovery from natural gas using a mixed refrigerant
US20140013796A1 (en) * 2012-07-12 2014-01-16 Zaheer I. Malik Methods for separating hydrocarbon gases
KR20150102931A (en) * 2012-08-30 2015-09-09 플루오르 테크놀로지스 코포레이션 Configurations and methods for offshore ngl recovery
US20140075987A1 (en) 2012-09-20 2014-03-20 Fluor Technologies Corporation Configurations and methods for ngl recovery for high nitrogen content feed gases
DE102012020354A1 (en) * 2012-10-16 2014-04-17 Linde Aktiengesellschaft Process for separating heavy hydrocarbons from a hydrocarbon-rich fraction
US10563913B2 (en) 2013-11-15 2020-02-18 Black & Veatch Holding Company Systems and methods for hydrocarbon refrigeration with a mixed refrigerant cycle
WO2015103403A1 (en) * 2014-01-02 2015-07-09 Fluor Technologies Corporation Systems and methods for flexible propane recovery
KR102367522B1 (en) 2014-03-14 2022-02-25 루머스 테크놀로지 엘엘씨 Process and apparatus for heavy hydrocarbon removal from lean natural gas before liquefaction
US9574822B2 (en) 2014-03-17 2017-02-21 Black & Veatch Corporation Liquefied natural gas facility employing an optimized mixed refrigerant system
EP2926882A1 (en) * 2014-04-01 2015-10-07 Linde Aktiengesellschaft Method and assembly for separating a gas mixture and method for retrofitting a separating system
US10017701B2 (en) * 2014-06-02 2018-07-10 Aspen Engineering Services, Llc Flare elimination process and methods of use
WO2016053668A1 (en) * 2014-09-30 2016-04-07 Dow Global Technologies Llc Process for increasing ethylene and propylene yield from a propylene plant
US10077938B2 (en) 2015-02-09 2018-09-18 Fluor Technologies Corporation Methods and configuration of an NGL recovery process for low pressure rich feed gas
US10365037B2 (en) 2015-09-18 2019-07-30 Exxonmobil Upstream Research Company Heating component to reduce solidification in a cryogenic distillation system
US10006701B2 (en) 2016-01-05 2018-06-26 Fluor Technologies Corporation Ethane recovery or ethane rejection operation
US10520249B2 (en) 2016-01-22 2019-12-31 Encana Corporation Process and apparatus for processing a hydrocarbon gas stream
RU2635946C1 (en) * 2016-05-11 2017-11-17 Общество с ограниченной ответственностью "Научно-исследовательский институт природных газов и газовых технологий - Газпром ВНИИГАЗ" Plant for processing natural gas
RU2633563C1 (en) * 2016-05-11 2017-10-13 Общество с ограниченной ответственностью "Научно-исследовательский институт природных газов и газовых технологий - Газпром ВНИИГАЗ" Plant for absorption preparation of natural gas
US10330382B2 (en) 2016-05-18 2019-06-25 Fluor Technologies Corporation Systems and methods for LNG production with propane and ethane recovery
RU2645102C2 (en) * 2016-05-31 2018-02-15 Общество с ограниченной ответственностью "Научно-исследовательский институт природных газов и газовых технологий - Газпром ВНИИГАЗ" Natural gas preparation method
RU2645124C1 (en) * 2016-08-22 2018-02-15 Общество с ограниченной ответственностью "Научно-исследовательский институт природных газов и газовых технологий - Газпром ВНИИГАЗ" Natural gas absorption preparation method
US11402155B2 (en) 2016-09-06 2022-08-02 Lummus Technology Inc. Pretreatment of natural gas prior to liquefaction
MX2019001888A (en) 2016-09-09 2019-06-03 Fluor Tech Corp METHODS AND CONFIGURATION FOR GAS LIQUID PLANT READAPTATION (NGL) FOR HIGH ETHANE RECOVERY.
CN106693431A (en) * 2017-03-17 2017-05-24 河南中托力合化学有限公司 Novel heptane precise fractionation device
US20180274853A1 (en) * 2017-03-23 2018-09-27 Greg Luetkemeyer Gas plant
CN107032943A (en) * 2017-05-04 2017-08-11 宁夏磐泰能源科技有限公司 Cryogen phase propane extracts system out
FR3066491B1 (en) * 2017-05-18 2019-07-12 Technip France PROCESS FOR RECOVERING A C2 + HYDROCARBON CURRENT IN A REFINERY RESIDUAL GAS AND ASSOCIATED INSTALLATION
WO2019078892A1 (en) * 2017-10-20 2019-04-25 Fluor Technologies Corporation Phase implementation of natural gas liquid recovery plants
WO2019226156A1 (en) * 2018-05-22 2019-11-28 Fluor Technologies Corporation Integrated methods and configurations for propane recovery in both ethane recovery and ethane rejection
US12215922B2 (en) 2019-05-23 2025-02-04 Fluor Technologies Corporation Integrated heavy hydrocarbon and BTEX removal in LNG liquefaction for lean gases
US12098882B2 (en) 2018-12-13 2024-09-24 Fluor Technologies Corporation Heavy hydrocarbon and BTEX removal from pipeline gas to LNG liquefaction
RU2695209C1 (en) * 2019-01-11 2019-07-22 Общество с ограниченной ответственностью "Научно-исследовательский институт природных газов и газовых технологий - Газпром ВНИИГАЗ" Apparatus for regenerating an aqueous solution of methanol
RU2695211C1 (en) * 2019-01-11 2019-07-22 Общество с ограниченной ответственностью "Научно-исследовательский институт природных газов и газовых технологий - Газпром ВНИИГАЗ" Method of regenerating aqueous solution of methanol
JP7330446B2 (en) * 2019-05-24 2023-08-22 レール・リキード－ソシエテ・アノニム・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード An extraction system for extracting natural gas liquids (NGL) from liquefied natural gas (LNG)
EP4031820A1 (en) * 2019-09-19 2022-07-27 Exxonmobil Upstream Research Company (EMHC-N1-4A-607) Pretreatment, pre-cooling, and condensate recovery of natural gas by high pressure compression and expansion
JP7390860B2 (en) * 2019-11-05 2023-12-04 東洋エンジニアリング株式会社 Hydrocarbon separation method and separation device
CN112875783A (en) * 2021-04-14 2021-06-01 北京中科康仑环境科技研究院有限公司 System and method for treating wastewater containing volatile substances
TW202309456A (en) 2021-05-14 2023-03-01 美商圖表能源與化學有限公司 Side draw reflux heavy hydrocarbon removal system and method
US20230375263A1 (en) * 2022-05-17 2023-11-23 Gas Liquids Engineering Ltd. Gas processing methodology utilizing reflux and additionally synthesized stream optimization
US12247007B2 (en) * 2022-08-30 2025-03-11 Saudi Arabian Oil Company Reflux arrangement for distillation columns
US20240318910A1 (en) * 2023-03-22 2024-09-26 Bcck Holding Company System and method for improving propane recovery and ethane rejection in a gsp/ expander system
WO2025251088A1 (en) * 2024-05-31 2025-12-04 Lummus Technology Llc Dual tower propane recovery process

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4689063A (en) * 1985-03-05 1987-08-25 Compagnie Francaise D'etudes Et De Construction "Technip" Process of fractionating gas feeds and apparatus for carrying out the said process
US5771712A (en) * 1995-06-07 1998-06-30 Elcor Corporation Hydrocarbon gas processing
US6401486B1 (en) * 2000-05-18 2002-06-11 Rong-Jwyn Lee Enhanced NGL recovery utilizing refrigeration and reflux from LNG plants
US20020157538A1 (en) * 2001-03-01 2002-10-31 Foglietta Jorge H. Cryogenic process utilizing high pressure absorber column
US20030221447A1 (en) * 2002-05-30 2003-12-04 Mealey W. Brent System and method for liquefied petroleum gas recovery

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4171964A (en) * 1976-06-21 1979-10-23 The Ortloff Corporation Hydrocarbon gas processing
US4157904A (en) 1976-08-09 1979-06-12 The Ortloff Corporation Hydrocarbon gas processing
US4278457A (en) 1977-07-14 1981-07-14 Ortloff Corporation Hydrocarbon gas processing
US4519824A (en) 1983-11-07 1985-05-28 The Randall Corporation Hydrocarbon gas separation
US4657571A (en) * 1984-06-29 1987-04-14 Snamprogetti S.P.A. Process for the recovery of heavy constituents from hydrocarbon gaseous mixtures
FR2571129B1 (en) 1984-09-28 1988-01-29 Technip Cie PROCESS AND PLANT FOR CRYOGENIC FRACTIONATION OF GASEOUS LOADS
US4596588A (en) * 1985-04-12 1986-06-24 Gulsby Engineering Inc. Selected methods of reflux-hydrocarbon gas separation process
US4690955A (en) * 1986-06-30 1987-09-01 Union Carbide Corporation Polyether silicone copolymers with mixed hydroxy alkoxy capping for stabilizing high solid content, molded, flexible urethane foam
US4854955A (en) 1988-05-17 1989-08-08 Elcor Corporation Hydrocarbon gas processing
US5799507A (en) * 1996-10-25 1998-09-01 Elcor Corporation Hydrocarbon gas processing
US5992175A (en) * 1997-12-08 1999-11-30 Ipsi Llc Enhanced NGL recovery processes
US6182469B1 (en) * 1998-12-01 2001-02-06 Elcor Corporation Hydrocarbon gas processing
US6116050A (en) * 1998-12-04 2000-09-12 Ipsi Llc Propane recovery methods
US6244712B1 (en) * 1999-09-27 2001-06-12 University Of Alabama In Huntsville Optical scanning spectroscopic apparatus and associated method
US6354105B1 (en) 1999-12-03 2002-03-12 Ipsi L.L.C. Split feed compression process for high recovery of ethane and heavier components
US6244070B1 (en) 1999-12-03 2001-06-12 Ipsi, L.L.C. Lean reflux process for high recovery of ethane and heavier components
UA76750C2 (en) * 2001-06-08 2006-09-15 Елккорп Method for liquefying natural gas (versions)
US6516631B1 (en) 2001-08-10 2003-02-11 Mark A. Trebble Hydrocarbon gas processing
US6425266B1 (en) * 2001-09-24 2002-07-30 Air Products And Chemicals, Inc. Low temperature hydrocarbon gas separation process
US6823692B1 (en) * 2002-02-11 2004-11-30 Abb Lummus Global Inc. Carbon dioxide reduction scheme for NGL processes

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4689063A (en) * 1985-03-05 1987-08-25 Compagnie Francaise D'etudes Et De Construction "Technip" Process of fractionating gas feeds and apparatus for carrying out the said process
US5771712A (en) * 1995-06-07 1998-06-30 Elcor Corporation Hydrocarbon gas processing
US6401486B1 (en) * 2000-05-18 2002-06-11 Rong-Jwyn Lee Enhanced NGL recovery utilizing refrigeration and reflux from LNG plants
US20020157538A1 (en) * 2001-03-01 2002-10-31 Foglietta Jorge H. Cryogenic process utilizing high pressure absorber column
US20030221447A1 (en) * 2002-05-30 2003-12-04 Mealey W. Brent System and method for liquefied petroleum gas recovery

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