WO2005016479A3 - Use of disulfonated anthracenes as inert fluorescent tracers - Google Patents

Use of disulfonated anthracenes as inert fluorescent tracers Download PDF

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Publication number
WO2005016479A3
WO2005016479A3 PCT/US2004/017815 US2004017815W WO2005016479A3 WO 2005016479 A3 WO2005016479 A3 WO 2005016479A3 US 2004017815 W US2004017815 W US 2004017815W WO 2005016479 A3 WO2005016479 A3 WO 2005016479A3
Authority
WO
WIPO (PCT)
Prior art keywords
inert fluorescent
fluorescent tracers
disulfonated
anthracenes
disulfonated anthracenes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2004/017815
Other languages
French (fr)
Other versions
WO2005016479A2 (en
Inventor
Martin R Godfrey
John E Hoots
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ChampionX LLC
Original Assignee
Nalco Co LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nalco Co LLC filed Critical Nalco Co LLC
Priority to CA002534211A priority Critical patent/CA2534211A1/en
Priority to EP04754426A priority patent/EP1649078A2/en
Priority to AU2004265235A priority patent/AU2004265235A1/en
Publication of WO2005016479A2 publication Critical patent/WO2005016479A2/en
Publication of WO2005016479A3 publication Critical patent/WO2005016479A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/008—Control or steering systems not provided for elsewhere in subclass C02F
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F22—STEAM GENERATION
    • F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
    • F22B37/00—Component parts or details of steam boilers
    • F22B37/02—Component parts or details of steam boilers applicable to more than one kind or type of steam boiler
    • F22B37/38—Determining or indicating operating conditions in steam boilers, e.g. monitoring direction or rate of water flow through water tubes
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00—Investigating fluid-tightness of structures
    • G01M3/02—Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/04—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
    • G01M3/20—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material
    • G01M3/22—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material for pipes, cables or tubes; for pipe joints or seals; for valves; for welds; for containers, e.g. radiators
    • G01M3/226—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material for pipes, cables or tubes; for pipe joints or seals; for valves; for welds; for containers, e.g. radiators for containers, e.g. radiators
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64—Fluorescence; Phosphorescence
    • G01N21/6428—Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes"
    • G01N2021/6439—Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes" with indicators, stains, dyes, tags, labels, marks
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/18—Water
    • G01N33/1826—Organic contamination in water

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Organic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Thermal Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • General Physics & Mathematics (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Electroluminescent Light Sources (AREA)

Abstract

The use of an isomer of anthracene disulfonic acid as an inert fluorescent tracer is described and claimed. The utility of this type of inert fluorescent tracer in boiler systems to trace unwanted carryover of boiler water into a steam line is also described and claimed.
PCT/US2004/017815 2003-07-31 2004-06-07 Use of disulfonated anthracenes as inert fluorescent tracers Ceased WO2005016479A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CA002534211A CA2534211A1 (en) 2003-07-31 2004-06-07 Use of disulfonated anthracenes as inert fluorescent tracers
EP04754426A EP1649078A2 (en) 2003-07-31 2004-06-07 Use of disulfonated anthracenes as inert fluorescent tracers
AU2004265235A AU2004265235A1 (en) 2003-07-31 2004-06-07 Use of disulfonated anthracenes as inert fluorescent tracers

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/631,606 US7220382B2 (en) 2003-07-31 2003-07-31 Use of disulfonated anthracenes as inert fluorescent tracers
US10/631,606 2003-07-31

Publications (2)

Publication Number Publication Date
WO2005016479A2 WO2005016479A2 (en) 2005-02-24
WO2005016479A3 true WO2005016479A3 (en) 2005-07-21

Family

ID=34104150

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2004/017815 Ceased WO2005016479A2 (en) 2003-07-31 2004-06-07 Use of disulfonated anthracenes as inert fluorescent tracers

Country Status (5)

Country Link
US (1) US7220382B2 (en)
EP (1) EP1649078A2 (en)
AU (1) AU2004265235A1 (en)
CA (1) CA2534211A1 (en)
WO (1) WO2005016479A2 (en)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060254624A1 (en) * 2003-12-17 2006-11-16 Zeiher E H K Method of monitoring membrane cleaning processes
US7179384B2 (en) * 2004-04-30 2007-02-20 Nalco Company Control of cooling water system using rate of consumption of fluorescent polymer
WO2007148981A1 (en) * 2006-06-20 2007-12-27 Institutt For Energiteknikk The use of biphenyl, terphenyl, and fluorene sulphonic acid based tracers for monitoring streams of fluids
US7448255B2 (en) * 2006-06-29 2008-11-11 Nalco Company Very high-temperature fluorescent tracer and automation for boiler water applications
US7985318B2 (en) * 2007-05-10 2011-07-26 Nalco Company Method of monitoring and inhibiting scale deposition in pulp mill evaporators and concentrators
US20090101587A1 (en) 2007-10-22 2009-04-23 Peter Blokker Method of inhibiting scale formation and deposition in desalination systems
US8352207B2 (en) 2010-03-31 2013-01-08 Ecolab Usa Inc. Methods for calibrating a fluorometer
US8373140B2 (en) 2010-03-31 2013-02-12 Ecolab Usa Inc. Fluorometric sensor
US8269193B2 (en) 2010-03-31 2012-09-18 Ecolab Usa Inc. Handheld fluorometer and method of use
US8248611B2 (en) 2010-03-31 2012-08-21 Ecolab Usa Inc. Handheld optical measuring device and method of use
US9266797B2 (en) 2013-02-12 2016-02-23 Ecolab Usa Inc. Online monitoring of polymerization inhibitors for control of undesirable polymerization
US8956875B2 (en) 2013-03-14 2015-02-17 Ecolab USA, Inc. Water hardness monitoring via fluorescence
US9303360B2 (en) 2013-08-08 2016-04-05 Ecolab Usa Inc. Use of nanocrystaline cellulose and polymer grafted nanocrystaline cellulose for increasing retention in papermaking process
US9410288B2 (en) 2013-08-08 2016-08-09 Ecolab Usa Inc. Use of nanocrystaline cellulose and polymer grafted nanocrystaline cellulose for increasing retention in papermaking process
US9034145B2 (en) 2013-08-08 2015-05-19 Ecolab Usa Inc. Use of nanocrystaline cellulose and polymer grafted nanocrystaline cellulose for increasing retention, wet strength, and dry strength in papermaking process
US10139385B2 (en) 2013-08-12 2018-11-27 Ecolab Usa Inc. Method of tracing chemical quantities using encapsulated fluorescent dyes
US9399622B2 (en) 2013-12-03 2016-07-26 Ecolab Usa Inc. Nitroxide hydroxylamine and phenylenediamine combinations as polymerization inhibitors for ethylenically unsaturated monomer processes
US9834730B2 (en) 2014-01-23 2017-12-05 Ecolab Usa Inc. Use of emulsion polymers to flocculate solids in organic liquids
US9261459B1 (en) 2014-08-12 2016-02-16 Ecolab Usa Inc. Handheld fluorometer
US10317385B2 (en) 2015-07-01 2019-06-11 Ecolab Usa Inc. Calibration method for water hardness measurement
PT3325135T (en) 2015-07-20 2019-10-28 Ecolab Usa Inc Methods of conditioning membranes
CA2995721C (en) 2015-08-14 2020-03-31 Chemtreat, Inc. Fluid system evaluation with multiple chemical tracers
WO2017066540A1 (en) 2015-10-15 2017-04-20 Ecolab Usa Inc. Nanocrystalline cellulose and polymer-grafted nanocrystalline cellulose as rheology modifying agents for magnesium oxide and lime slurries
EP3290451B1 (en) * 2016-09-01 2021-08-18 The Swatch Group Research and Development Ltd. Substrate comprising a surface covered with an epilame agent and method for coating such a substrate with epilame
CN110997593B (en) 2017-07-17 2023-01-24 埃科莱布美国股份有限公司 Process for modifying the rheology of slurries

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4783314A (en) * 1987-02-26 1988-11-08 Nalco Chemical Company Fluorescent tracers - chemical treatment monitors

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4992380A (en) * 1988-10-14 1991-02-12 Nalco Chemical Company Continuous on-stream monitoring of cooling tower water
US5041386A (en) * 1988-12-19 1991-08-20 Nalco Chemical Company Concentration cycles, percent life holding time and continuous treatment concentration monitoring in boiler systems by inert tracers
US5006311A (en) * 1990-03-23 1991-04-09 Nalco Chemical Company Monitoring performance of a treating agent added to a body of water
US5171450A (en) * 1991-03-20 1992-12-15 Nalco Chemical Company Monitoring and dosage control of tagged polymers in cooling water systems
US5282379A (en) * 1992-04-03 1994-02-01 Nalco Chemical Company Volatile tracers for diagnostic use in steam generating systems
US5278074A (en) * 1992-04-22 1994-01-11 Nalco Chemical Company Method of monitoring and controlling corrosion inhibitor dosage in aqueous systems
US5304800A (en) * 1992-11-10 1994-04-19 Nalco Chemical Company Leak detection and responsive treatment in industrial water processes
US5320967A (en) * 1993-04-20 1994-06-14 Nalco Chemical Company Boiler system leak detection
US5503775A (en) * 1994-05-09 1996-04-02 Nalco Chemical Company Method of preventing yellow metal corrosion in aqueous systems with superior corrosion performance in reduced environmental impact
US5736405A (en) 1996-03-21 1998-04-07 Nalco Chemical Company Monitoring boiler internal treatment with fluorescent-tagged polymers
ZA984976B (en) 1997-06-11 1999-04-19 Nalco Chemical Co Solid-state fluorometer and methods of use therefore
US6336058B1 (en) 2000-05-01 2002-01-01 Nalco Chemical Company Use of control matrix for boiler control
US6315909B1 (en) 2000-05-01 2001-11-13 Nalco Chemical Company Use of control matrix for cooling water systems control
US6369894B1 (en) 2000-05-01 2002-04-09 Nalco Chemical Company Modular fluorometer
US6587753B2 (en) 2000-05-01 2003-07-01 Ondeo Nalco Company Use of control matrix for boiler control
US6436711B1 (en) 2000-12-13 2002-08-20 Nalco Chemical Company Fluorometric control of aromatic oxygen scavengers in a boiler system
US6556027B2 (en) 2001-01-12 2003-04-29 Ondeo Nalco Company Low cost, on-line corrosion monitor and smart corrosion probe
US6821428B1 (en) * 2002-03-28 2004-11-23 Nalco Company Method of monitoring membrane separation processes
US6730227B2 (en) * 2002-03-28 2004-05-04 Nalco Company Method of monitoring membrane separation processes

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4783314A (en) * 1987-02-26 1988-11-08 Nalco Chemical Company Fluorescent tracers - chemical treatment monitors

Also Published As

Publication number Publication date
WO2005016479A2 (en) 2005-02-24
EP1649078A2 (en) 2006-04-26
AU2004265235A2 (en) 2005-02-24
CA2534211A1 (en) 2005-02-24
US7220382B2 (en) 2007-05-22
AU2004265235A1 (en) 2005-02-24
US20050025659A1 (en) 2005-02-03

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