WO2005029045A1 - A method of measuring the consistency of a mixture as well as an apparatus for carrying out the method - Google Patents

A method of measuring the consistency of a mixture as well as an apparatus for carrying out the method Download PDF

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Publication number
WO2005029045A1
WO2005029045A1 PCT/DK2004/000644 DK2004000644W WO2005029045A1 WO 2005029045 A1 WO2005029045 A1 WO 2005029045A1 DK 2004000644 W DK2004000644 W DK 2004000644W WO 2005029045 A1 WO2005029045 A1 WO 2005029045A1
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Prior art keywords
measuring
mixture
agitator
force
mixer
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Ceased
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PCT/DK2004/000644
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French (fr)
Inventor
Niels Høll NIELSEN
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CONVI
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CONVI
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Priority to EP04762864A priority Critical patent/EP1664732B1/en
Priority to PL04762864T priority patent/PL1664732T3/en
Priority to DE602004013995T priority patent/DE602004013995D1/en
Priority to DK04762864T priority patent/DK1664732T3/en
Publication of WO2005029045A1 publication Critical patent/WO2005029045A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
    • G01N11/14—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/38—Concrete; Lime; Mortar; Gypsum; Bricks; Ceramics; Glass
    • G01N33/383—Concrete or cement

Definitions

  • the invention relates to a method of measuring the consistency of a mixture, said method involving a measuring of the force exerted on a measuring device immersed in the mixture while said mixture is subjected to a movement relative to said measuring device.
  • the invention relates furthermore to an apparatus for carrying out the method.
  • the flowability viz. the workability of the con- crete is controlled by way of two fundamentally different methods.
  • One method is based on a measurement of the power consumed by the mixer as an expression of how viscous the concrete is. In many respects this method has been developed so as to correct various weaknesses, but the method suffers inter alia from the weakness that the modern concrete mixtures are so fluid that nothing but an insignificant dif- ference applies to the power consumed by the mixer when said mixer is idle running and when the mixing of the ready concrete takes place.
  • the second method is based on a measuring of the moisture present in the materials involved, either before or after said materials have been placed in the mixer, where- after the amount of water to be added in order to obtain the desired flowability is calculated.
  • Both methods are focussed on developing a recipe for the desired concrete whereafter the data of the recipe are registered. These methods do not result in a measure- ment of the viscosity of the concrete, but merely in a comparison value based on a single parameter, viz. either on the power consumed by the mixer or on the present amount of water, and such a single parameter is not providing a sufficient description of the flowability of the concrete.
  • Rheology teaches the flowing properties of various substances.
  • y indicates a power
  • x indicates a speed.
  • the two constants_a and b must be determined, which can be done in viscosin eters adapted to such a purpose and determining the shear stress in the substance in question at two different speeds.
  • the above measurement of the power consumed by the mixer results in nothing but a determination of a point on the straight line, which does not suffice for defining said line.
  • the registration of the moisture does not involve a measuring of the flowability of the concrete at all, but in stead a measuring of the water content.
  • the water content represents only one factor of the many factors affecting the flowing properties.
  • the amount of water and the amount of plasticizing additives do indeed represent the two factors with the highest effect on the flowing properties.
  • Viscosimeters are known for measuring the flowing properties of concrete, but the use thereof is not advantageous because the measuring is carried out outside the mixer. Such a measuring requires many resources, and when the measurement forms the basis of an approval of the concrete, said measuring prolongs the cycle time of a mixture.
  • the use of a viscosimeter renders it possible to determine the above straight line.
  • the concrete mixture is poured into a container in which measuring devices are immersed. Subsequently, the container is caused to rotate, and the force exerted by the concrete on the measuring device is measured. The force measured depends on the rotating speed of the container and on the rheological properties of the concrete.
  • the yield stress can be described as the force necessary for causing the concrete to move and corresponds to the above constant b, and the viscosity is an expression of the force necessary for increasing the rotational speed.
  • the latter force corresponds to the above factor a, where the speed representing the variable x is the rotational speed at the measuring site.
  • the object of the invention is to provide a method and an apparatus rendering it possible to determine the flowing properties of a mixture, especially of a concrete mixture, directly in connection with the mixing process per se.
  • This object is according to the invention achieved by carrying out the measuring of the exerted force and the speed at at least two different relative speeds inside the mixer.
  • the flowing properties of the mixture in question can be determined without delaying the mixing process.
  • the measuring results can be used for determining the parameters to be adjusted for obtaining the desired flowing properties.
  • the measurings can be carried out by means of separate probes, but according to the invention they are advantageously carried out in connection with the agitators of the mixer.
  • the speeds can be determined as the maximum speed and the minimum speed at the measuring site in question based on the geometry and ro- tational speed of the agitator, and the corresponding exerted forces are registered when the measurements thereof are at a maximum and minimum, respectively.
  • the rotational speed of the driving shaft and the relative speeds of the agitator are substantially unaffected by the flowing properties of the mixture in question, it is possible in advance to determine the maximum speed and the minimum speed at the measuring site in question.
  • the measurements relating to the mixing are thus restricted to a measurement of the forces exerted at the measuring site in question while the mixer is running, and thus the exerted forces corresponding to the maximum speed and the minimum speed are only registered when said speeds are at a maximum and minimum, respectively.
  • the apparatus for carrying out the method is according to the invention advantageously a mixer with an agitator, where at least one force measuring device is asso- ciated with the agitator.
  • the force measuring device may according to the invention advanta- geously be provided in connection with at least one of said parts in such a manner that the speeds can be calculated in advance.
  • Fig. 1 is a diagrammatic top view of an apparatus according to the invention.
  • Fig. 2 is a graphical view of measurements carried out in accordance with the present invention. Best Mode for Carrying out the Invention
  • the mixer illustrated in the drawing is designated the general reference numeral 1 and includes a circumferential wall 2 and an agitator designated the general reference numeral 3.
  • the agitator is of the planetary mixer type, i.e. it includes a main driving shaft 4 causing the agitator to rotate in the direction of an arrow 5 and carrying two agitating members 6 and 7. These agitating members 6 and 7 are carried at each end of a substantially horizontal carrying device 8. The agitating members 6 and 7 are caused to rotate individually in the direction of the arrows 9 and 10, respectively.
  • a measuring device 11 is arranged on one of these two agitating members 6 and 7. This measuring device 11 is placed at a location being exerted to a force during the mixing process.
  • the agitator When the mixer is running, the agitator is caused to rotate by means of the driving shaft 4 at a specific rotational speed, and the simultaneous rotation of the agitating members 6 and 7 per se has the result that the relative movement between the measuring site in question and the mixture in the mixer 1 varies as a function of the position of the agitating member 6 relative to the carrying device 8.
  • the force exerted at the measuring device 11 is suitably provided by means of a strain gauge, and the resulting measurement is transferred to a receiving station (not shown) via a radio signal. The latter signal is subsequently transferred to a control device (not shown) where it is subjected to a processing.
  • the energy necessary for this purpose can be provided in a conventionally known manner by means of for instance batteries, and the necessary components are mounted in a suitably protected manner on the parts in question of the agitator 3.
  • the speed of the measuring de- vice 11 is initially calculated relative to the concrete mixture in question on the basis of the rotational speed of the agitator 3 and the rotational speed of the agitating members 6 and 7 as well as on the basis of the position of said measuring device 11.
  • a continuous measuring is carried out at regular intervals of the force exerted on said measuring device 11, and based on these measurements the registration of maximum and minimum force are deducted.
  • Fig. 2 illustrates an example of the use of the invention.
  • Fig. 2 has been drafted on the basis of the following measurements carried out in a mixture after 100 seconds and 130 seconds, respectively, from the activation of a mixer. At 110 seconds, 7 litres of water per m 3 of concrete were added on the basis of the measurements carried out at 100 seconds. The measurements carried out and the subsequent calculations appear from the following table:
  • the invention has been described with reference to a preferred embodiment. Many modifications can be carried out without thereby deviating from the scope of the invention.
  • Separate probes can for instance be mounted in connection with the agitator for measuring the exerted forces and for instance such that two probes are arranged at their respective distances from the axis of rotation of the driving shaft with the result that measurings of the force are carried out at various speeds.

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Immunology (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Analytical Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Abstract

A method of measuring the consistency of a mixture implies that a measuring is carried out of the force exerted on a measuring device (11) immersed in said mixture during a relative movement of said mixture relative to the measuring device (11). The measuring of the exerted force and the speed at least two different relative speeds inside a mixer (1). An apparatus for carrying out the method includes at least one force measuring device (11) in connection with an agitator (3).

Description

Title: A method of measuring the consistency of a mixture as well as an apparatus for carrying out the method
Technical Field
The invention relates to a method of measuring the consistency of a mixture, said method involving a measuring of the force exerted on a measuring device immersed in the mixture while said mixture is subjected to a movement relative to said measuring device. The invention relates furthermore to an apparatus for carrying out the method.
Background Art
During the production of concrete, the flowability, viz. the workability of the con- crete is controlled by way of two fundamentally different methods. One method is based on a measurement of the power consumed by the mixer as an expression of how viscous the concrete is. In many respects this method has been developed so as to correct various weaknesses, but the method suffers inter alia from the weakness that the modern concrete mixtures are so fluid that nothing but an insignificant dif- ference applies to the power consumed by the mixer when said mixer is idle running and when the mixing of the ready concrete takes place.
The second method is based on a measuring of the moisture present in the materials involved, either before or after said materials have been placed in the mixer, where- after the amount of water to be added in order to obtain the desired flowability is calculated.
Both methods are focussed on developing a recipe for the desired concrete whereafter the data of the recipe are registered. These methods do not result in a measure- ment of the viscosity of the concrete, but merely in a comparison value based on a single parameter, viz. either on the power consumed by the mixer or on the present amount of water, and such a single parameter is not providing a sufficient description of the flowability of the concrete.
Rheology teaches the flowing properties of various substances. The flowing properties of a substance can be mathematically expressed by the expression y = ax + b. i.e. the equation of a straight line. In the equation y indicates a power and x indicates a speed. In order to describe the flowability of a substance, the two constants_a and b must be determined, which can be done in viscosin eters adapted to such a purpose and determining the shear stress in the substance in question at two different speeds.
The above measurement of the power consumed by the mixer results in nothing but a determination of a point on the straight line, which does not suffice for defining said line. In addition, the registration of the moisture does not involve a measuring of the flowability of the concrete at all, but in stead a measuring of the water content. The water content represents only one factor of the many factors affecting the flowing properties. The amount of water and the amount of plasticizing additives do indeed represent the two factors with the highest effect on the flowing properties. However, factors, such as the grain size distributions and the grain shape of the individual aggregate fractions, the hardness of the water and the reaction of the additives in the relevant mixture as well as the temperature of the concrete and the variations of the cement and the fly ash have also a significant effect on the flowing properties when it is a question of a substance, such as concrete.
Viscosimeters are known for measuring the flowing properties of concrete, but the use thereof is not advantageous because the measuring is carried out outside the mixer. Such a measuring requires many resources, and when the measurement forms the basis of an approval of the concrete, said measuring prolongs the cycle time of a mixture. The use of a viscosimeter renders it possible to determine the above straight line. By a known viscosimeter, the concrete mixture is poured into a container in which measuring devices are immersed. Subsequently, the container is caused to rotate, and the force exerted by the concrete on the measuring device is measured. The force measured depends on the rotating speed of the container and on the rheological properties of the concrete. The yield stress can be described as the force necessary for causing the concrete to move and corresponds to the above constant b, and the viscosity is an expression of the force necessary for increasing the rotational speed. The latter force corresponds to the above factor a, where the speed representing the variable x is the rotational speed at the measuring site.
Disclosure of Invention
The object of the invention is to provide a method and an apparatus rendering it possible to determine the flowing properties of a mixture, especially of a concrete mixture, directly in connection with the mixing process per se.
This object is according to the invention achieved by carrying out the measuring of the exerted force and the speed at at least two different relative speeds inside the mixer.
As a result the flowing properties of the mixture in question can be determined without delaying the mixing process. In addition, based on known relationships between the effect of the various ingredients and of the variations in said ingredients on the factors a and b in the above formula, the measuring results can be used for determining the parameters to be adjusted for obtaining the desired flowing properties.
The measurings can be carried out by means of separate probes, but according to the invention they are advantageously carried out in connection with the agitators of the mixer.
According to the invention, the speeds can be determined as the maximum speed and the minimum speed at the measuring site in question based on the geometry and ro- tational speed of the agitator, and the corresponding exerted forces are registered when the measurements thereof are at a maximum and minimum, respectively. Based on the knowledge that in a modern mixer the rotational speed of the driving shaft and the relative speeds of the agitator are substantially unaffected by the flowing properties of the mixture in question, it is possible in advance to determine the maximum speed and the minimum speed at the measuring site in question. The measurements relating to the mixing are thus restricted to a measurement of the forces exerted at the measuring site in question while the mixer is running, and thus the exerted forces corresponding to the maximum speed and the minimum speed are only registered when said speeds are at a maximum and minimum, respectively.
Based on these two measurements, two points are determined on the line corresponding to the above equation.
The apparatus for carrying out the method is according to the invention advantageously a mixer with an agitator, where at least one force measuring device is asso- ciated with the agitator.
When the agitator according to the invention includes parts moving at varying speeds relative to the mixture during the mixing process while being in contact with said mixture, the force measuring device may according to the invention advanta- geously be provided in connection with at least one of said parts in such a manner that the speeds can be calculated in advance.
Brief Description of the Drawings
The invention is explained in detail below with reference to the accompanying drawings, in which
Fig. 1 is a diagrammatic top view of an apparatus according to the invention, and
Fig. 2 is a graphical view of measurements carried out in accordance with the present invention. Best Mode for Carrying out the Invention
The mixer illustrated in the drawing is designated the general reference numeral 1 and includes a circumferential wall 2 and an agitator designated the general reference numeral 3. The agitator is of the planetary mixer type, i.e. it includes a main driving shaft 4 causing the agitator to rotate in the direction of an arrow 5 and carrying two agitating members 6 and 7. These agitating members 6 and 7 are carried at each end of a substantially horizontal carrying device 8. The agitating members 6 and 7 are caused to rotate individually in the direction of the arrows 9 and 10, respectively. A measuring device 11 is arranged on one of these two agitating members 6 and 7. This measuring device 11 is placed at a location being exerted to a force during the mixing process.
When the mixer is running, the agitator is caused to rotate by means of the driving shaft 4 at a specific rotational speed, and the simultaneous rotation of the agitating members 6 and 7 per se has the result that the relative movement between the measuring site in question and the mixture in the mixer 1 varies as a function of the position of the agitating member 6 relative to the carrying device 8.
The force exerted at the measuring device 11 is suitably provided by means of a strain gauge, and the resulting measurement is transferred to a receiving station (not shown) via a radio signal. The latter signal is subsequently transferred to a control device (not shown) where it is subjected to a processing. The energy necessary for this purpose can be provided in a conventionally known manner by means of for instance batteries, and the necessary components are mounted in a suitably protected manner on the parts in question of the agitator 3.
When the mixer according to the invention is used, the speed of the measuring de- vice 11 is initially calculated relative to the concrete mixture in question on the basis of the rotational speed of the agitator 3 and the rotational speed of the agitating members 6 and 7 as well as on the basis of the position of said measuring device 11. During the mixing process, a continuous measuring is carried out at regular intervals of the force exerted on said measuring device 11, and based on these measurements the registration of maximum and minimum force are deducted. The measuring result is used by the control device in question for determining a line defined by the equa- tion y = ax + b, which represents the flowing properties of the mixture in question. Two points on the line are determined by means of on one hand the measured maximum force and the calculated maximum speed and on the other hand the measured minimum force and the calculated minimum speed. Based on the knowledge of the effect of the various components in the mixture on the constants a and_b in the equa- tion, it is subsequently possible to add further additives in such a manner that a mixture possessing the desired flowing properties is obtained, i.e. the desired yield stress and the desired viscosity. Fig. 2 illustrates an example of the use of the invention. Fig. 2 has been drafted on the basis of the following measurements carried out in a mixture after 100 seconds and 130 seconds, respectively, from the activation of a mixer. At 110 seconds, 7 litres of water per m3 of concrete were added on the basis of the measurements carried out at 100 seconds. The measurements carried out and the subsequent calculations appear from the following table:
Figure imgf000007_0001
Measurings carried out after 100 seconds appear at the symbol o and after 130 sec- onds at the symbol +. The invention has been described with reference to a preferred embodiment. Many modifications can be carried out without thereby deviating from the scope of the invention. Separate probes can for instance be mounted in connection with the agitator for measuring the exerted forces and for instance such that two probes are arranged at their respective distances from the axis of rotation of the driving shaft with the result that measurings of the force are carried out at various speeds.

Claims

Claims
1. A method of measuring the consistency of a mixture, said method involving a measuring of the force exerted on a measuring device (11) immersed in the mixture while said mixture is subjected to a movement relative to said measuring device (11), characterised by carrying out the measuring of the exerted force and the speed at at least two different relative speeds inside the mixer.
2. A method according to claim 1, characterised by the measurings being carried out in connection with the agitator (3) of a mixer (1).
3. A Method according to claim 1, characterised by the speeds being determined as the maximum speed and the minimum speed at the measuring site in question based on the geometry and rotational speed of the agitator (3), and by the corre- sponding exerted forces being registered when the measurements thereof are at a maximum and minimum, respectively.
4. An apparatus for carrying out the method according to claims 1 to 3, and including a mixer (1) with an agitator (3), characterised in that at least one force measur- ing device (11) is associated with the agitator (3).
5. An apparatus according to claim 4, and where the agitator (3) includes members (6, 7), moving at a varying speed relative to the mixture during the mixing process while being in contact with said mixture, characterised in that the force measuring device (11) is provided in connection with at least one of said members (6, 7).
PCT/DK2004/000644 2003-09-24 2004-09-23 A method of measuring the consistency of a mixture as well as an apparatus for carrying out the method Ceased WO2005029045A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP04762864A EP1664732B1 (en) 2003-09-24 2004-09-23 A method of measuring the consistency of a mixture as well as an apparatus for carrying out the method
PL04762864T PL1664732T3 (en) 2003-09-24 2004-09-23 A method of measuring the consistency of a mixture as well as an apparatus for carrying out the method
DE602004013995T DE602004013995D1 (en) 2003-09-24 2004-09-23 METHOD FOR MEASURING THE CONSISTENCY OF A MIXTURE AND DEVICE FOR CARRYING OUT SAID METHOD
DK04762864T DK1664732T3 (en) 2003-09-24 2004-09-23 A method of measuring a blend consistency as well as an apparatus for practicing the method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DKPA200301388 2003-09-24
DKPA200301388 2003-09-24

Publications (1)

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WO2005029045A1 true WO2005029045A1 (en) 2005-03-31

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EP (1) EP1664732B1 (en)
AT (1) ATE396392T1 (en)
DE (1) DE602004013995D1 (en)
DK (1) DK1664732T3 (en)
ES (1) ES2305812T3 (en)
PL (1) PL1664732T3 (en)
WO (1) WO2005029045A1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2486385B1 (en) 2009-10-07 2016-05-11 I.B.B. Rheologie Inc. Rotatable cylindrical container comprising a rheological probe unit
US10520410B2 (en) 2009-10-07 2019-12-31 Command Alkon Incorporated Probe and method for obtaining rheological property value
EP2943321B1 (en) * 2013-01-11 2021-04-21 GCP Applied Technologies Inc. Concrete mixture measurement sensor and method
US11041794B2 (en) * 2016-08-31 2021-06-22 Command Alkon Incorporated Rheological probe
US11402312B2 (en) * 2018-02-08 2022-08-02 Command Alkon Incorporated Methods and systems for handling fresh concrete based on hydraulic pressure and on rheological probe pressure
US11420358B2 (en) * 2016-12-22 2022-08-23 Command Alkon Incorporated Methods and system for handling fresh concrete

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4299119A (en) * 1980-03-13 1981-11-10 National Metal And Refining Company, Ltd. Incremental rotary viscometer
US5321974A (en) * 1993-06-04 1994-06-21 Radian Corporation Method and device for determining rheological properties
US5456105A (en) * 1993-10-14 1995-10-10 International Paper Company Rheometer for determining extensional elasticity
US6227039B1 (en) * 1998-01-06 2001-05-08 Moshe Te'eni System and method for controlling concrete production
WO2003048743A1 (en) * 2001-11-28 2003-06-12 Stable Microsystems Limited Rheometer with axial resistive force measurement

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4299119A (en) * 1980-03-13 1981-11-10 National Metal And Refining Company, Ltd. Incremental rotary viscometer
US5321974A (en) * 1993-06-04 1994-06-21 Radian Corporation Method and device for determining rheological properties
US5456105A (en) * 1993-10-14 1995-10-10 International Paper Company Rheometer for determining extensional elasticity
US6227039B1 (en) * 1998-01-06 2001-05-08 Moshe Te'eni System and method for controlling concrete production
WO2003048743A1 (en) * 2001-11-28 2003-06-12 Stable Microsystems Limited Rheometer with axial resistive force measurement

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2486385B1 (en) 2009-10-07 2016-05-11 I.B.B. Rheologie Inc. Rotatable cylindrical container comprising a rheological probe unit
EP2486385B2 (en) † 2009-10-07 2019-06-19 Command Alkon Incorporated Rotatable cylindrical container comprising a rheological probe unit
US10520410B2 (en) 2009-10-07 2019-12-31 Command Alkon Incorporated Probe and method for obtaining rheological property value
EP2943321B1 (en) * 2013-01-11 2021-04-21 GCP Applied Technologies Inc. Concrete mixture measurement sensor and method
US11041794B2 (en) * 2016-08-31 2021-06-22 Command Alkon Incorporated Rheological probe
US11420358B2 (en) * 2016-12-22 2022-08-23 Command Alkon Incorporated Methods and system for handling fresh concrete
US11402312B2 (en) * 2018-02-08 2022-08-02 Command Alkon Incorporated Methods and systems for handling fresh concrete based on hydraulic pressure and on rheological probe pressure

Also Published As

Publication number Publication date
PL1664732T3 (en) 2008-10-31
ES2305812T3 (en) 2008-11-01
DK1664732T3 (en) 2008-09-08
EP1664732B1 (en) 2008-05-21
EP1664732A1 (en) 2006-06-07
DE602004013995D1 (en) 2008-07-03
ATE396392T1 (en) 2008-06-15

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