WO2006042675A3 - Extraktion von nickel(0)-komplexen aus nitrilgemischen mit verminderter mulmbildung - Google Patents

Extraktion von nickel(0)-komplexen aus nitrilgemischen mit verminderter mulmbildung Download PDF

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Publication number
WO2006042675A3
WO2006042675A3 PCT/EP2005/010956 EP2005010956W WO2006042675A3 WO 2006042675 A3 WO2006042675 A3 WO 2006042675A3 EP 2005010956 W EP2005010956 W EP 2005010956W WO 2006042675 A3 WO2006042675 A3 WO 2006042675A3
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WIPO (PCT)
Prior art keywords
extraction
complexes
nickel
stream
powder formation
Prior art date
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Ceased
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PCT/EP2005/010956
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English (en)
French (fr)
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WO2006042675A2 (de
Inventor
Petra Deckert
Peter Bassler
Michael Bartsch
Gerd Haderlein
Hermann Luyken
Jens Scheidel
Peter Pfab
Tobias Aechtner
Wolfgang Siegel
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BASF SE
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BASF SE
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=36120664&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO2006042675(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority to JP2007536077A priority Critical patent/JP2008516907A/ja
Priority to KR1020077011215A priority patent/KR101222389B1/ko
Priority to BRPI0516617-9A priority patent/BRPI0516617A/pt
Priority to PL05798767T priority patent/PL1817108T3/pl
Priority to CA002582813A priority patent/CA2582813A1/en
Application filed by BASF SE filed Critical BASF SE
Priority to DE502005004359T priority patent/DE502005004359D1/de
Priority to US11/577,231 priority patent/US7935229B2/en
Priority to EP05798767A priority patent/EP1817108B1/de
Publication of WO2006042675A2 publication Critical patent/WO2006042675A2/de
Publication of WO2006042675A3 publication Critical patent/WO2006042675A3/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4053—Regeneration or reactivation of catalysts containing metals with recovery of phosphorous catalyst system constituents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/50—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using organic liquids
    • B01J38/56—Hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/0434—Counter-current multistage extraction towers in a vertical or sloping position comprising rotating mechanisms, e.g. mixers, rotational oscillating motion, mixing pumps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185—Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4023—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper
    • B01J31/403—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing iron group metals or copper
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/08—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds
    • C07C253/10—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds to compounds containing carbon-to-carbon double bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32—Addition reactions to C=C or C-C triple bonds
    • B01J2231/323—Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/847—Nickel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

Verfahren zur extraktiven Abtrennung von homogen gelösten Katalysatoren aus einem Reaktionsaustrag einer Hydrocyanierung von ungesättigten Mononitrilen zu Dinitrilen, durch Extraktion mittels eines Kohlenwasserstoffs (K), dadurch gekennzeichnet, dass man: a) dem Reaktionsaustrag eine unpolare aprotische Flüssigkeit (F) zufügt, wobei ein Strom (I) erhalten wird, und b) den Strom (I) bei einer Temperatur (T) mit dem Kohlenwasserstoff (K) extrahiert, wobei ein Strom (II) enthaltend den mit dem Katalysator angereicherten Kohlenwasserstoff (K), und ein katalysatorarmer Strom (III) erhalten wird.
PCT/EP2005/010956 2004-10-18 2005-10-12 Extraktion von nickel(0)-komplexen aus nitrilgemischen mit verminderter mulmbildung Ceased WO2006042675A2 (de)

Priority Applications (8)

Application Number Priority Date Filing Date Title
EP05798767A EP1817108B1 (de) 2004-10-18 2005-10-12 Extraktion von nickel(0)-komplexen aus nitrilgemischen mit verminderter mulmbildung
KR1020077011215A KR101222389B1 (ko) 2004-10-18 2005-10-12 감소된 분말 형성으로 니트릴 혼합물로부터 니켈(0) 착체의추출법
BRPI0516617-9A BRPI0516617A (pt) 2004-10-18 2005-10-12 processo para remoção por extração de catalisadores dissolvidos homogeneamente
PL05798767T PL1817108T3 (pl) 2004-10-18 2005-10-12 Ekstrakcja kompleksów niklu(0) z mieszanin nitryli ze zmniejszonym powstawaniem kożucha
CA002582813A CA2582813A1 (en) 2004-10-18 2005-10-12 Extraction of nickel(0) complexes from nitrile mixtures with reduced powder formation
JP2007536077A JP2008516907A (ja) 2004-10-18 2005-10-12 ラグ形成減少下でのニトリル混合物からのニッケル（０）錯体の抽出
DE502005004359T DE502005004359D1 (de) 2004-10-18 2005-10-12 Extraktion von nickel(0)-komplexen aus nitrilgemischen mit verminderter mulmbildung
US11/577,231 US7935229B2 (en) 2004-10-18 2005-10-12 Extraction of nickel (0) complexes from nitrile mixtures with reduced rag formation

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102004050935A DE102004050935A1 (de) 2004-10-18 2004-10-18 Extraktion von Nickel(0)-Komplexen aus Nitrilgemischen mit verminderter Mulmbildung
DE102004050935.2 2004-10-18

Publications (2)

Publication Number Publication Date
WO2006042675A2 WO2006042675A2 (de) 2006-04-27
WO2006042675A3 true WO2006042675A3 (de) 2006-07-13

Family

ID=36120664

Family Applications (1)

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PCT/EP2005/010956 Ceased WO2006042675A2 (de) 2004-10-18 2005-10-12 Extraktion von nickel(0)-komplexen aus nitrilgemischen mit verminderter mulmbildung

Country Status (13)

Country Link
US (1) US7935229B2 (de)
EP (1) EP1817108B1 (de)
JP (1) JP2008516907A (de)
KR (1) KR101222389B1 (de)
CN (1) CN100493716C (de)
AT (1) ATE397489T1 (de)
BR (1) BRPI0516617A (de)
CA (1) CA2582813A1 (de)
DE (2) DE102004050935A1 (de)
ES (1) ES2306233T3 (de)
MY (1) MY140569A (de)
PL (1) PL1817108T3 (de)
WO (1) WO2006042675A2 (de)

Families Citing this family (30)

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FR2850966B1 (fr) 2003-02-10 2005-03-18 Rhodia Polyamide Intermediates Procede de fabrication de composes dinitriles
FR2854891B1 (fr) 2003-05-12 2006-07-07 Rhodia Polyamide Intermediates Procede de preparation de dinitriles
WO2007046799A1 (en) 2005-10-18 2007-04-26 Invista Technologies S.A R.L. Process of making 3-aminopentanenitrile
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US7919646B2 (en) 2006-07-14 2011-04-05 Invista North America S.A R.L. Hydrocyanation of 2-pentenenitrile
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US8906334B2 (en) 2007-05-14 2014-12-09 Invista North America S.A R.L. High efficiency reactor and process
US8101790B2 (en) 2007-06-13 2012-01-24 Invista North America S.A.R.L. Process for improving adiponitrile quality
US7977502B2 (en) 2008-01-15 2011-07-12 Invista North America S.A R.L. Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile
EP2229353B1 (de) 2008-01-15 2018-01-03 INVISTA Textiles (U.K.) Limited Hydrocyanierung von pentennitrilen
EP2257516A4 (de) * 2008-03-19 2012-12-12 Invista Tech Sarl Verfahren zur herstellung von cyclododecatrien und verfahren zur herstellung von laurolacton
EP2334624B1 (de) 2008-10-14 2014-10-01 Invista Technologies S.à.r.l. Verfahren zur herstellung von 2-sekundäralkyl-4,5-di-(normalalykl-)phenolen
KR20120047251A (ko) 2009-08-07 2012-05-11 인비스타 테크놀러지스 에스.에이.알.엘. 디에스테르를 형성하기 위한 수소화 및 에스테르화
EP2574191B1 (de) 2010-07-07 2013-11-20 Invista Technologies S.a r.l. Verfahren zur herstellung von nitrilen
KR20140127220A (ko) 2011-12-21 2014-11-03 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
KR20140108683A (ko) 2011-12-21 2014-09-12 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
KR20140127218A (ko) * 2011-12-21 2014-11-03 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
US9011691B2 (en) 2011-12-21 2015-04-21 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
EP3010615B1 (de) * 2013-06-20 2022-09-28 INVISTA Textiles (U.K.) Limited Verfahren zur rückgewinnung von diphosphonithaltigen verbindungen mittels eines mehrstufigen gegenstrom-flüssig-flüssig-extraktors mit misch-absetzer und rückführung der schweren phase
WO2014205195A1 (en) * 2013-06-20 2014-12-24 Invista Technologies S.A.R.L. Extraction solvent control for reducing stable emulsions
US9676800B2 (en) * 2013-06-20 2017-06-13 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
EP3010617B1 (de) * 2013-06-20 2022-11-30 INVISTA Textiles (U.K.) Limited Steuerung eines extraktionslösungsmittels zur reduzierung stabiler emulsionen
EP3010616B1 (de) * 2013-06-20 2022-09-28 INVISTA Textiles (U.K.) Limited Steuerung eines extraktionslösungsmittels zur reduzierung stabiler emulsionen
DK3102562T3 (en) 2014-02-07 2018-05-07 Basf Se PROCEDURE FOR CLEANING ADIPODINITRIL (ADN)
CN106573879B (zh) 2014-06-27 2019-09-24 英威达纺织（英国）有限公司 增强从包含腈的混合物萃取杂质
EP3160933B1 (de) 2014-06-27 2018-08-15 INVISTA Textiles (U.K.) Limited Integriertes verfahren zur herstellung von nitril mit verbesserter flüssig-flüssig-extraktion
US10640459B2 (en) * 2015-09-03 2020-05-05 Invista North America S.A.R.L. Inhibiting CPI formation from adiponitrile
CN109071421B (zh) 2016-05-02 2022-02-25 英威达纺织（英国）有限公司 减少二腈流中的cpi的方法
KR102800446B1 (ko) 2020-10-12 2025-04-23 주식회사 엘지화학 아크릴로니트릴 이량체의 제조 방법
CN112794948B (zh) 2020-12-31 2022-08-26 浙江大学 多孔聚合物及其制备方法、催化剂以及己二腈的制备方法

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US20040140263A1 (en) * 2003-01-08 2004-07-22 Jackson Scott C. Process for catalyst recovery from hydrocyanation product mixtures
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ATE397489T1 (de) 2008-06-15
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PL1817108T3 (pl) 2008-11-28
EP1817108B1 (de) 2008-06-04
DE102004050935A1 (de) 2006-04-20
KR101222389B1 (ko) 2013-01-15
BRPI0516617A (pt) 2008-09-16
KR20070072593A (ko) 2007-07-04
MY140569A (en) 2009-12-31
US20080083607A1 (en) 2008-04-10
CA2582813A1 (en) 2006-04-27
JP2008516907A (ja) 2008-05-22
DE502005004359D1 (de) 2008-07-17
ES2306233T3 (es) 2008-11-01
CN100493716C (zh) 2009-06-03
CN101043946A (zh) 2007-09-26
EP1817108A2 (de) 2007-08-15

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