WO2006092291A3 - Verfahren zum herstellen von alkylaniliden - Google Patents

Verfahren zum herstellen von alkylaniliden Download PDF

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Publication number
WO2006092291A3
WO2006092291A3 PCT/EP2006/001871 EP2006001871W WO2006092291A3 WO 2006092291 A3 WO2006092291 A3 WO 2006092291A3 EP 2006001871 W EP2006001871 W EP 2006001871W WO 2006092291 A3 WO2006092291 A3 WO 2006092291A3
Authority
WO
WIPO (PCT)
Prior art keywords
anilides
alkyl
fluorine
producing alkyl
represents hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2006/001871
Other languages
English (en)
French (fr)
Other versions
WO2006092291A2 (de
Inventor
Alexander Straub
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer CropScience AG
Original Assignee
Bayer CropScience AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer CropScience AG filed Critical Bayer CropScience AG
Priority to US11/817,373 priority Critical patent/US8053572B2/en
Priority to CN2006800139605A priority patent/CN101166728B/zh
Priority to JP2007557418A priority patent/JP5173443B2/ja
Priority to EP20060723163 priority patent/EP1858858B1/de
Priority to ES06723163.9T priority patent/ES2542710T3/es
Priority to DK06723163.9T priority patent/DK1858858T3/en
Publication of WO2006092291A2 publication Critical patent/WO2006092291A2/de
Publication of WO2006092291A3 publication Critical patent/WO2006092291A3/de
Priority to IL185627A priority patent/IL185627A/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16—Halogen atoms or nitro radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

Abstract

Die vorliegende Erfindung betrifft ein Verfahren zum Herstellen von bekannten fungizid wirksamen Alklaniliden (I), in welcher R1 für Wasserstoff oder Fluor steht, R2 für Wasserstoff, Halogen, C1-C4-Alkyl oder C1-C4-Halogenalkyl mit 1 bis 9 Fluor-, Chlor- und/oder Bromatomen steht, aus Säurechloriden und Aminoacetophenon über Hydroxyalkyl-substituierte Carbox-anilide, Alkenylanilide und Benzoxazin-Derivate.
PCT/EP2006/001871 2005-03-02 2006-03-01 Verfahren zum herstellen von alkylaniliden Ceased WO2006092291A2 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
US11/817,373 US8053572B2 (en) 2005-03-02 2006-03-01 Alkyl-analide producing method
CN2006800139605A CN101166728B (zh) 2005-03-02 2006-03-01 制备烷基n-酰基苯胺的方法
JP2007557418A JP5173443B2 (ja) 2005-03-02 2006-03-01 アルキルアニリド製造方法
EP20060723163 EP1858858B1 (de) 2005-03-02 2006-03-01 Verfahren zum herstellen von alkylaniliden
ES06723163.9T ES2542710T3 (es) 2005-03-02 2006-03-01 Procedimiento para la preparación de alquilanilidas
DK06723163.9T DK1858858T3 (en) 2005-03-02 2006-03-01 PROCEDURE FOR THE PREPARATION OF ALKYLANILIDES
IL185627A IL185627A (en) 2005-03-02 2007-08-30 A process for making alkyl-anilides and their intermediates

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102005009457A DE102005009457A1 (de) 2005-03-02 2005-03-02 Verfahren zum Herstellen von Alkylaniliden
DE102005009457.0 2005-03-02

Publications (2)

Publication Number Publication Date
WO2006092291A2 WO2006092291A2 (de) 2006-09-08
WO2006092291A3 true WO2006092291A3 (de) 2006-11-30

Family

ID=36754120

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/001871 Ceased WO2006092291A2 (de) 2005-03-02 2006-03-01 Verfahren zum herstellen von alkylaniliden

Country Status (10)

Country Link
US (1) US8053572B2 (de)
EP (1) EP1858858B1 (de)
JP (1) JP5173443B2 (de)
CN (1) CN101166728B (de)
DE (1) DE102005009457A1 (de)
DK (1) DK1858858T3 (de)
ES (1) ES2542710T3 (de)
IL (1) IL185627A (de)
TW (1) TWI372145B (de)
WO (1) WO2006092291A2 (de)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004005787A1 (de) * 2004-02-06 2005-08-25 Bayer Cropscience Ag Carboxamide
DE102004005786A1 (de) * 2004-02-06 2005-08-25 Bayer Cropscience Ag Haloalkylcarboxamide
JP2006076990A (ja) 2004-03-12 2006-03-23 Bayer Cropscience Ag 殺虫性ベンゼンジカルボキサミド類
DE102005022147A1 (de) * 2005-04-28 2006-11-02 Bayer Cropscience Ag Wirkstoffkombinationen
DE102005028293A1 (de) 2005-06-18 2007-01-04 Bayer Cropscience Gmbh Verfahren zum Herstellen von Carboxamiden
EP2272345A1 (de) 2009-07-07 2011-01-12 Bayer CropScience AG Verfahren für erhöhtes Wachstum von Setzlingen und/oder frühes Aufgehen von Saat
EP2535334A1 (de) 2011-06-17 2012-12-19 Bayer CropScience AG Kristalline Modifikationen von Penflufen
US9656964B2 (en) * 2012-11-13 2017-05-23 Bayer Cropscience Ag Method for producing carboxamides
WO2014140111A1 (en) 2013-03-13 2014-09-18 Bayer Cropscience Ag Lawn growth-promoting agent and method of using same
DK3097081T3 (da) * 2014-01-24 2018-01-29 Bayer Cropscience Ag Fremgangsmåde til fremstilling af 1-alkyl-3-difluormethyl-5-fluor-1h-pyrazol-4-carbaldehyder og 1-alkyl-3-difluormethyl-5-fluor-1h-pyrazol-4-carboxylater
MX2016012936A (es) 2014-04-01 2016-12-07 Bayer Cropscience Ag Proceso para la preparacion de n-[3-(bencilcarbamoil)fenil]-1h-pir azol-5-carboxamidas.
CN110054595B (zh) * 2019-05-30 2020-10-16 山东省联合农药工业有限公司 一种解草酮的合成工艺

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0824099A1 (de) * 1996-08-15 1998-02-18 MITSUI TOATSU CHEMICALS, Inc. Substituiertes Carboxanilid-Derivat und dieses als aktiven Bestandteil enthaltendes Mittel zur Bekämpfung von Pflanzenkrankheiten
WO2003010149A1 (de) * 2001-07-25 2003-02-06 Bayer Cropscience Ag Pyrazolylcarboxanilide als fungizide
WO2004103975A1 (de) * 2003-05-21 2004-12-02 Bayer Cropscience Aktiengesellschaft Iodpyrazolylcarboxanilide
WO2004103953A1 (de) * 2003-05-21 2004-12-02 Bayer Cropscience Aktiengesellschaft Difluormethylbenzanilide und deren verwendung zur bekämpfung bon mikroorganismen, sowie zwischen produkte und deren herstellung
WO2005075452A1 (de) * 2004-02-06 2005-08-18 Bayer Cropscience Aktiengesellschaft 2-halogenfuryl/thienyl-3-carboxamide

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2072015T3 (es) * 1990-08-21 1995-07-01 Upjohn Co Derivados del acido bisfosfonico como agente anti-artritico.
US5223526A (en) 1991-12-06 1993-06-29 Monsanto Company Pyrazole carboxanilide fungicides and use
DE4231517A1 (de) 1992-09-21 1994-03-24 Basf Ag Carbonsäureanilide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen
DE4231519A1 (de) 1992-09-21 1994-03-24 Basf Ag Cyclohex(en)ylcarbonsäureamide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen
GB9405347D0 (en) * 1994-03-18 1994-05-04 Agrevo Uk Ltd Fungicides
DE10325438A1 (de) 2003-05-21 2004-12-09 Bayer Cropscience Ag Difluormethylbenzanilide
DE10347090A1 (de) 2003-10-10 2005-05-04 Bayer Cropscience Ag Synergistische fungizide Wirkstoffkombinationen
DE102004005786A1 (de) 2004-02-06 2005-08-25 Bayer Cropscience Ag Haloalkylcarboxamide
DE102004005787A1 (de) 2004-02-06 2005-08-25 Bayer Cropscience Ag Carboxamide
JP2006076990A (ja) 2004-03-12 2006-03-23 Bayer Cropscience Ag 殺虫性ベンゼンジカルボキサミド類
DE102005022147A1 (de) 2005-04-28 2006-11-02 Bayer Cropscience Ag Wirkstoffkombinationen
DE102005035300A1 (de) 2005-07-28 2007-02-01 Bayer Cropscience Ag Synergistische fungizide Wirkstoffkombinationen
DE102006033090A1 (de) 2006-07-14 2008-01-24 Bayer Cropscience Ag Verfahren zum Herstellen von Alkylaniliden aus Halogenbenzolderivaten
EP2272345A1 (de) 2009-07-07 2011-01-12 Bayer CropScience AG Verfahren für erhöhtes Wachstum von Setzlingen und/oder frühes Aufgehen von Saat

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0824099A1 (de) * 1996-08-15 1998-02-18 MITSUI TOATSU CHEMICALS, Inc. Substituiertes Carboxanilid-Derivat und dieses als aktiven Bestandteil enthaltendes Mittel zur Bekämpfung von Pflanzenkrankheiten
WO2003010149A1 (de) * 2001-07-25 2003-02-06 Bayer Cropscience Ag Pyrazolylcarboxanilide als fungizide
WO2004103975A1 (de) * 2003-05-21 2004-12-02 Bayer Cropscience Aktiengesellschaft Iodpyrazolylcarboxanilide
WO2004103953A1 (de) * 2003-05-21 2004-12-02 Bayer Cropscience Aktiengesellschaft Difluormethylbenzanilide und deren verwendung zur bekämpfung bon mikroorganismen, sowie zwischen produkte und deren herstellung
WO2005075452A1 (de) * 2004-02-06 2005-08-18 Bayer Cropscience Aktiengesellschaft 2-halogenfuryl/thienyl-3-carboxamide

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* Cited by examiner, † Cited by third party
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BOGERT, MARSTON TAYLOR ET AL: "Quinazolines. XXXVIII. Synthesis of some new analogs of cinchophen and intermediate products", JOURNAL OF THE AMERICAN CHEMICAL SOCIETY , 49, 2650-4 CODEN: JACSAT; ISSN: 0002-7863, 1927, XP002394112 *
BULLETIN OF THE KOREAN CHEMICAL SOCIETY , 19(10), 1109-1112 CODEN: BKCSDE; ISSN: 0253-2964, 1998 *
CHEMISCHE BERICHTE , 98(4), 1049-59 CODEN: CHBEAM; ISSN: 0009-2940, 1965 *
DATABASE CA [online] CHEMICAL ABSTRACTS SERVICE, COLUMBUS, OHIO, US; HAHN, HOH-GYU ET AL: "Anchimeric assistance in the rearrangement of dichloro-3-methyl-1,4- oxathianes to 2-chloromethyl dihydro-1,4-oxathiins", XP002394122, retrieved from STN Database accession no. 1998:699952 *
DATABASE CA [online] CHEMICAL ABSTRACTS SERVICE, COLUMBUS, OHIO, US; KOVENDI, ALEXANDER ET AL: "New synthesis for quinazoline N3-oxides and 1,2-dihydroquinazoline N3-oxides", XP002394123, retrieved from STN Database accession no. 1965:90918 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 10 November 2004 (2004-11-10), XP002394126, retrieved from STN Database accession no. RN - 777875-56-6 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 11 April 2005 (2005-04-11), XP002394130, retrieved from STN Database accession no. RN - 848249-78-5 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 2 October 1997 (1997-10-02), XP002394128, retrieved from STN Database accession no. RN - 194783-80-7 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 30 November 2004 (2004-11-30), XP002394125, retrieved from STN Database accession no. RN - 790679-71-9 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 4 July 2005 (2005-07-04), XP002394129, retrieved from STN Database accession no. RN - 853689-32-4 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 4 June 2002 (2002-06-04), XP002394127, retrieved from STN Database accession no. RN - 425399-14-0 *
DATABASE REGISTRY [online] Chemical Abstracts Service, Columbus, Ohio, US; 9 December 2002 (2002-12-09), XP002394124, retrieved from STN Database accession no. RN - 795292-48-7 *
DIXON W J ET AL: "Kinetics and mechanism of the addition of water and ring-opening of 2-methyl- and 2-aryl-4H-3,1-benzoxazines to 2-aminobenzyl esters in the acidic pH range; change in rate-limiting step with buffer concentration and evidence for a tetrahedral carbonyl addition intermediate", JOURNAL OF THE CHEMICAL SOCIETY, PERKIN TRANSACTIONS 2, CHEMICAL SOCIETY. LETCHWORTH, GB, vol. 8, 1997, pages 1503 - 1510, XP002323920, ISSN: 1472-779X *
HAHN H-G ET AL: "SYNTHESIS OF TRIFLUOROMETHYLATED DIHYDRO-1,4-OXATHIN-3-CARBOXANILIDES THROUGH POLYMER-BOUND ACTIVATED ESTER", HETEROCYCLES, ELSEVIER SCIENCE PUBLISHERS B.V. AMSTERDAM, NL, vol. 48, no. 11, 1998, pages 2253 - 2261, XP009038022, ISSN: 0385-5414 *
HARI ET AL: "Efficient synthesis of o-alkynyl-N-pivaloylanilines from o-acyl-N-pivaloylanilines and lithium trimethylsilyldiazomethane", TETRAHEDRON LETTERS, ELSEVIER, AMSTERDAM, NL, vol. 47, no. 7, 13 February 2006 (2006-02-13), pages 1137 - 1139, XP005247514, ISSN: 0040-4039 *
TARZIA, GIORGIO ET AL: "Synthesis and structure-activity relationships of a series of pyrrole cannabinoid receptor agonists", BIOORGANIC & MEDICINAL CHEMISTRY , 11(18), 3965-3973 CODEN: BMECEP; ISSN: 0968-0896, 2003, XP002394111 *

Also Published As

Publication number Publication date
ES2542710T3 (es) 2015-08-10
US20090209769A1 (en) 2009-08-20
CN101166728A (zh) 2008-04-23
IL185627A0 (en) 2008-01-06
EP1858858A2 (de) 2007-11-28
JP2008531629A (ja) 2008-08-14
IL185627A (en) 2015-10-29
JP5173443B2 (ja) 2013-04-03
CN101166728B (zh) 2011-08-31
DK1858858T3 (en) 2015-07-27
EP1858858B1 (de) 2015-04-29
US8053572B2 (en) 2011-11-08
TW200702331A (en) 2007-01-16
WO2006092291A2 (de) 2006-09-08
DE102005009457A1 (de) 2006-09-07
TWI372145B (en) 2012-09-11

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