WO2007051750A3 - Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan - Google Patents

Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan Download PDF

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Publication number
WO2007051750A3
WO2007051750A3 PCT/EP2006/067784 EP2006067784W WO2007051750A3 WO 2007051750 A3 WO2007051750 A3 WO 2007051750A3 EP 2006067784 W EP2006067784 W EP 2006067784W WO 2007051750 A3 WO2007051750 A3 WO 2007051750A3
Authority
WO
WIPO (PCT)
Prior art keywords
propane
mixture
carrying
acrylic acid
continuously producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2006/067784
Other languages
English (en)
French (fr)
Other versions
WO2007051750A2 (de
Inventor
Martin Dieterle
Goetz-Peter Schindler
Catharina Klanner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to CN200680041219XA priority Critical patent/CN101300218B/zh
Priority to KR1020087013316A priority patent/KR101278795B1/ko
Priority to DE502006003491T priority patent/DE502006003491D1/de
Priority to JP2008538337A priority patent/JP4956544B2/ja
Priority to EP06807555A priority patent/EP1945600B1/de
Priority to AT06807555T priority patent/ATE428679T1/de
Publication of WO2007051750A2 publication Critical patent/WO2007051750A2/de
Publication of WO2007051750A3 publication Critical patent/WO2007051750A3/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0461—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds
    • B01J8/0469—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2208/00274—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00477—Controlling the temperature by thermal insulation means
    • B01J2208/00495—Controlling the temperature by thermal insulation means using insulating materials or refractories

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Ein Verfahren zum stabilen Betreiben eines kontinuierlich ausgeübten Herstellprozesses zur Erzeugung von Acrolein, oder Acrylsäure oder deren Gemisch aus Propan, bei dem Zufuhrrate an Frischpropan zum Verfahren als Stellgröße für einen stabilen stationären Betrieb benutzt wird.
PCT/EP2006/067784 2005-11-03 2006-10-26 Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan Ceased WO2007051750A2 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CN200680041219XA CN101300218B (zh) 2005-11-03 2006-10-26 以稳定地方式操作由丙烷连续制备丙烯醛或丙烯酸或其混合物的方法的方法
KR1020087013316A KR101278795B1 (ko) 2005-11-03 2006-10-26 프로판으로부터 아크롤레인 또는 아크릴산 또는 그의혼합물을 수득하기 위한 안정한 연속 제조 방법
DE502006003491T DE502006003491D1 (de) 2005-11-03 2006-10-26 Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan
JP2008538337A JP4956544B2 (ja) 2005-11-03 2006-10-26 プロパンからアクロレインまたはアクリル酸あるいはそれらの混合物を連続的に製造する工程を安定した方式で実施するための方法
EP06807555A EP1945600B1 (de) 2005-11-03 2006-10-26 Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan
AT06807555T ATE428679T1 (de) 2005-11-03 2006-10-26 Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US73265805P 2005-11-03 2005-11-03
DE102005052923A DE102005052923A1 (de) 2005-11-03 2005-11-03 Verfahren zum stabilen Betreiben eines kontinuierlich ausgeübten Herstellprozesses zur Erzeugung von Acrolein, oder Acrylsäure oder deren Gemisch aus Propan
US60/732,658 2005-11-03
DE102005052923.2 2005-11-03

Publications (2)

Publication Number Publication Date
WO2007051750A2 WO2007051750A2 (de) 2007-05-10
WO2007051750A3 true WO2007051750A3 (de) 2007-06-28

Family

ID=37949866

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/067784 Ceased WO2007051750A2 (de) 2005-11-03 2006-10-26 Verfahren zum stabilen betreiben eines kontinuierlich ausgeübten herstellprozesses zur erzeugung von acrolein, oder acrylsäure oder deren gemisch aus propan

Country Status (9)

Country Link
EP (1) EP1945600B1 (de)
JP (1) JP4956544B2 (de)
CN (1) CN101300218B (de)
AT (1) ATE428679T1 (de)
DE (1) DE102005052923A1 (de)
MY (1) MY148411A (de)
RU (1) RU2429219C9 (de)
WO (1) WO2007051750A2 (de)
ZA (1) ZA200804663B (de)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005055826A1 (de) 2005-11-23 2007-05-24 Basf Ag Verfahren zum sicheren Betreiben einer Gasphasen-Partialoxidation
KR101370749B1 (ko) 2005-11-24 2014-03-06 바스프 에스이 프로판으로부터 아크롤레인 또는 아크릴산, 또는 그의혼합물의 제조 방법
US7842846B2 (en) 2006-03-30 2010-11-30 Basf Aktiengesellschaft Process for heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated
DE102006024901A1 (de) 2006-05-24 2007-11-29 Basf Ag Verfahren zur Herstellung von Acrolein, oder Acrylsäure oder deren Gemisch aus Propan
DE102006035718A1 (de) 2006-07-28 2008-01-31 Basf Ag Verfahren zum Langzeitbetrieb einer kontinuierlich betriebenen heterogen katalysierten partiellen Dehydrierung eines zu dehydrierenden Kohlenwasserstoffs
DE102007004960A1 (de) 2007-01-26 2008-07-31 Basf Se Verfahren zur Herstellung von Acrylsäure
DE102007055086A1 (de) 2007-11-16 2009-05-20 Basf Se Verfahren zur Herstellung von Acrylsäure
DE102007006647A1 (de) 2007-02-06 2008-08-07 Basf Se Verfahren zur Regenerierung eines im Rahmen einer heterogen katalysierten partiellen Dehydrierung eines Kohlenwasserstoffs deaktivierten Katalysatorbetts
DE102008044946B4 (de) 2008-08-29 2022-06-15 Evonik Superabsorber Gmbh Einsatz von Schaumkörpern in Oxidations-Reaktoren zur Herstellung ungesättigter Carbonsäuren
JP6204242B2 (ja) * 2014-03-27 2017-09-27 旭化成株式会社 酸化物触媒及びその製造方法、並びに不飽和アルデヒド又は不飽和ニトリルの製造方法
FR3082203B1 (fr) * 2018-06-12 2020-08-14 Arkema France Procede de production de 2,3,3,3-tetrafluoropropene et installation pour la mise en oeuvre de celui-ci.
FR3082202B1 (fr) 2018-06-12 2020-08-28 Arkema France Procede de production de 2,3,3,3-tetrafluoropropene et installation pour la mise en oeuvre de celui-ci.
FR3082200B1 (fr) * 2018-06-12 2020-08-28 Arkema France Procede de production de 2,3,3,3-tetrafluoropropene et reacteur pour la mise en oeuvre de celui-ci.
FR3082201A1 (fr) * 2018-06-12 2019-12-13 Arkema France Procede de production de 2,3,3,3-tetrafluoropropene, reacteur et installation pour la mise en oeuvre de celui-ci.
US20240343667A1 (en) 2021-07-28 2024-10-17 Basf Se Process for preparing acrylic acid
CN115707508B (zh) * 2021-08-19 2024-10-22 中国石油化工股份有限公司 气态烷烃在处理含氯丙烯和氧气的尾气中的应用
WO2025172146A1 (de) 2024-02-15 2025-08-21 Basf Se Verfahren zur herstellung von acrylsäure
WO2025219136A1 (en) 2024-04-17 2025-10-23 Basf Se Process for utilizing acrylic acid production waste streams
WO2025219137A1 (en) 2024-04-17 2025-10-23 Basf Se Process for utilizing acrylic acid production waste streams by gasification and fermentation
WO2025219135A1 (en) 2024-04-17 2025-10-23 Basf Se Process for utilizing high calorific acrylic acid production waste streams

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0117146A1 (de) * 1983-02-22 1984-08-29 The Halcon Sd Group, Inc. Konversion von Propan zu Acrylsäure
EP0799169B1 (de) * 1994-12-22 2000-03-08 Den Norske Stats Oljeselskap A.S. Apparatur zur katalytischen dehydrogenierung von kohlenwasserstoffen mit selektiver oxidation von wasserstoff
DE10245585A1 (de) * 2002-09-27 2004-04-08 Basf Ag Verfahren zur Herstellung von wenigstens einem partiellen Oxidations- und/oder Ammoxidationsprodukt des Propylens
DE102004032129A1 (de) * 2004-07-01 2005-03-03 Basf Ag Verfahren zur Herstellung von Acrolein, oder Acrylsäure oder deren Gemisch aus Propan

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4413147A (en) * 1982-04-14 1983-11-01 The Halcon Sd Group, Inc. Conversion of isobutane to methacrolein
DE19837519A1 (de) * 1998-08-19 2000-02-24 Basf Ag Verfahren zur Herstellung von Acrolein und/oder Acrylsäure aus Propan
DE19837518A1 (de) * 1998-08-19 2000-02-24 Basf Ag Verfahren zur Herstellung von Acrolein und/oder Acrylsäure aus Propan
DE10122027A1 (de) * 2001-05-07 2002-05-23 Basf Ag Verfahren zur Herstellung von Acrylsäure durch heterogen katalysierte Partialoxidation von Propan
DE10028582A1 (de) * 2000-06-14 2001-12-20 Basf Ag Verfahren zur Herstellung von Acrolein oder Acrylsäure oder deren Gemischen aus Propan
DE10117678A1 (de) * 2001-04-09 2002-10-10 Basf Ag Verfahren und Vorrichtung zur zweistufigen Herstellung von Acrylsäure
DE10211275A1 (de) * 2002-03-13 2003-09-25 Basf Ag Verfahren der kontinuierlichen heterogen katalysierten partiellen Dehydrierung
US7326802B2 (en) * 2002-09-27 2008-02-05 Basf Aktiengesellschaft Preparation of at least one partial oxidation and/or ammoxidation product of propylene
KR20050122239A (ko) * 2003-04-07 2005-12-28 바스프 악티엔게젤샤프트 탄화수소의 하나 이상의 부분 산화 및(또는) 가암모니아산화 생성물의 제조 방법
US7388106B2 (en) * 2005-10-14 2008-06-17 Basf Aktiengesellschaft Process for preparing acrolein or acrylic acid or a mixture thereof from propane

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0117146A1 (de) * 1983-02-22 1984-08-29 The Halcon Sd Group, Inc. Konversion von Propan zu Acrylsäure
EP0799169B1 (de) * 1994-12-22 2000-03-08 Den Norske Stats Oljeselskap A.S. Apparatur zur katalytischen dehydrogenierung von kohlenwasserstoffen mit selektiver oxidation von wasserstoff
DE10245585A1 (de) * 2002-09-27 2004-04-08 Basf Ag Verfahren zur Herstellung von wenigstens einem partiellen Oxidations- und/oder Ammoxidationsprodukt des Propylens
DE102004032129A1 (de) * 2004-07-01 2005-03-03 Basf Ag Verfahren zur Herstellung von Acrolein, oder Acrylsäure oder deren Gemisch aus Propan

Also Published As

Publication number Publication date
RU2429219C9 (ru) 2012-08-27
JP4956544B2 (ja) 2012-06-20
ZA200804663B (en) 2009-08-26
DE102005052923A1 (de) 2007-05-10
MY148411A (en) 2013-04-30
ATE428679T1 (de) 2009-05-15
EP1945600B1 (de) 2009-04-15
CN101300218B (zh) 2012-02-22
JP2009514829A (ja) 2009-04-09
CN101300218A (zh) 2008-11-05
RU2008121873A (ru) 2009-12-10
RU2429219C2 (ru) 2011-09-20
WO2007051750A2 (de) 2007-05-10
EP1945600A2 (de) 2008-07-23

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