WO2008079250A3 - Hydrogenation of caryophyllene - Google Patents

Hydrogenation of caryophyllene Download PDF

Info

Publication number
WO2008079250A3
WO2008079250A3 PCT/US2007/025983 US2007025983W WO2008079250A3 WO 2008079250 A3 WO2008079250 A3 WO 2008079250A3 US 2007025983 W US2007025983 W US 2007025983W WO 2008079250 A3 WO2008079250 A3 WO 2008079250A3
Authority
WO
WIPO (PCT)
Prior art keywords
hydrogenation
caryophyllene
caryophyllenes
skin
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2007/025983
Other languages
French (fr)
Other versions
WO2008079250A2 (en
Inventor
Keith W Hutchenson
Scott Christopher Jackson
Leo Ernest Manzer
Mark A Scialdone
Mayis Seapan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Priority to HK10103757.5A priority Critical patent/HK1137738B/en
Priority to BRPI0719468-4A2A priority patent/BRPI0719468A2/en
Priority to CN200780047643.XA priority patent/CN101568503B/en
Priority to CA2671531A priority patent/CA2671531C/en
Priority to EP07863142A priority patent/EP2129643A2/en
Priority to US12/519,614 priority patent/US8293217B2/en
Publication of WO2008079250A2 publication Critical patent/WO2008079250A2/en
Publication of WO2008079250A3 publication Critical patent/WO2008079250A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0038—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing more than six carbon atoms
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00—Formulations or additives for perfume preparations
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/02—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by hydrogenation
    • C07C5/03—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by hydrogenation of non-aromatic carbon-to-carbon double bonds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
    • C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
    • C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2523/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00
    • C07C2523/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals
    • C07C2523/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals of the platinum group metals
    • C07C2523/44—Palladium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

A process for the hydrogenation of a mixture of caryophyllenes by contact with hydrogen in the presence of a supported catalyst. The resulting products are useful for the application to skin.
PCT/US2007/025983 2006-12-21 2007-12-20 Hydrogenation of caryophyllene Ceased WO2008079250A2 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
HK10103757.5A HK1137738B (en) 2006-12-21 2007-12-20 Hydrogenation of caryophyllene
BRPI0719468-4A2A BRPI0719468A2 (en) 2006-12-21 2007-12-20 "PROCESS FOR THE PREPARATION OF A REACT PRODUCT, COMPOSITION OF MATTER OR MANUFACTURING ARTICLE AND METHOD FOR PROVIDING FRAGRANCE OR REVITALIZING SKIN, LEATHER, FUR, FEATHER OR OTHER SURFACE"
CN200780047643.XA CN101568503B (en) 2006-12-21 2007-12-20 Hydrogenation of caryophyllene
CA2671531A CA2671531C (en) 2006-12-21 2007-12-20 Hydrogenation of caryophyllene
EP07863142A EP2129643A2 (en) 2006-12-21 2007-12-20 Hydrogenation of caryophyllene
US12/519,614 US8293217B2 (en) 2006-12-21 2007-12-20 Hydrogenation of caryophellene

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US87655506P 2006-12-21 2006-12-21
US60/876,555 2006-12-21

Publications (2)

Publication Number Publication Date
WO2008079250A2 WO2008079250A2 (en) 2008-07-03
WO2008079250A3 true WO2008079250A3 (en) 2008-12-24

Family

ID=39563079

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2007/025983 Ceased WO2008079250A2 (en) 2006-12-21 2007-12-20 Hydrogenation of caryophyllene

Country Status (6)

Country Link
US (1) US8293217B2 (en)
EP (1) EP2129643A2 (en)
CN (1) CN101568503B (en)
BR (1) BRPI0719468A2 (en)
CA (1) CA2671531C (en)
WO (1) WO2008079250A2 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7547793B2 (en) * 2003-03-19 2009-06-16 E.I. Du Pont De Nemours And Company Method for making insect repellent composition
WO2007133683A2 (en) * 2006-05-10 2007-11-22 E. I. Du Pont De Nemours And Company Formulated tick and insect repellent compositions
CN101563334B (en) * 2006-12-21 2012-08-22 纳幕尔杜邦公司 Production of dihydronepetalactone by hydrogenation of nepetalactone
WO2008079253A1 (en) 2006-12-21 2008-07-03 E. I. Du Pont De Nemours And Company Hydrogenation of catmint oil
US8558015B2 (en) * 2006-12-21 2013-10-15 E I Du Pont De Nemours And Company Solvent addition and removal in the hydrogenation of catmint oil
BRPI0719458A2 (en) * 2006-12-21 2014-02-04 Du Pont "Processes for obtaining spinning oil"
US9521844B2 (en) 2006-12-21 2016-12-20 E I Du Pont De Nemours And Company Solvent addition and removal in the hydrogenation of catmint oil
KR101577472B1 (en) * 2007-11-26 2015-12-14 이 아이 듀폰 디 네모아 앤드 캄파니 Method for converting trans-cis nepetalactone to cis-trans nepetalactone using molecular sieves
PH12012500935A1 (en) 2009-11-11 2012-11-26 Du Pont Method for the enhanced recovery of catmint oil
EP3233780B1 (en) * 2014-12-19 2018-08-01 Basf Se 1-(7,10,10-trimethyl-4-bicyclo(6.2.0)decanyl)ethanone as novel aroma chemical
CN106083517A (en) * 2016-06-28 2016-11-09 广西梧松林化集团有限公司 The preparation method of high-purity longifolene
CN110818626B (en) * 2019-11-26 2022-06-28 南京林业大学 β-Caryophyllene-5-ester picolinate compound and preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3966819A (en) * 1973-09-05 1976-06-29 Firmenich S.A. Sesquiterpenic derivatives as odor- and taste modifying agents
US6359000B1 (en) * 1996-07-03 2002-03-19 Millennium Pharmaceuticals, Inc. Anticancer agent
US20070264297A1 (en) * 2006-05-10 2007-11-15 Scialdone Mark A Formulated tick and insect repellent compositions

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1116396C (en) * 2000-06-13 2003-07-30 芦建仁 Tiannu magnolia oil
CA2342403A1 (en) * 2001-03-28 2002-09-28 Jean Legault Sesquiterpene derivatives as anticancer agents
US6707000B2 (en) * 2001-08-24 2004-03-16 Illinois Tool Works Inc. Consumables storage box
US20030079786A1 (en) * 2001-10-30 2003-05-01 Diana Michael J. Modular fluid pressure regulator with bypass
KR20040083092A (en) * 2002-01-23 2004-09-30 이 아이 듀폰 디 네모아 앤드 캄파니 Fragrance Compound
US7067677B2 (en) * 2002-04-03 2006-06-27 E. I. Du Pont De Nemours And Company Production of dihydronepetalactone by hydrogenation of nepetalactone
US20060148842A1 (en) * 2004-12-29 2006-07-06 Scialdone Mark A Nepetalactams and N-substituted derivatives thereof
CN101563334B (en) * 2006-12-21 2012-08-22 纳幕尔杜邦公司 Production of dihydronepetalactone by hydrogenation of nepetalactone
US8558015B2 (en) * 2006-12-21 2013-10-15 E I Du Pont De Nemours And Company Solvent addition and removal in the hydrogenation of catmint oil
WO2008079253A1 (en) * 2006-12-21 2008-07-03 E. I. Du Pont De Nemours And Company Hydrogenation of catmint oil

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3966819A (en) * 1973-09-05 1976-06-29 Firmenich S.A. Sesquiterpenic derivatives as odor- and taste modifying agents
US6359000B1 (en) * 1996-07-03 2002-03-19 Millennium Pharmaceuticals, Inc. Anticancer agent
US20070264297A1 (en) * 2006-05-10 2007-11-15 Scialdone Mark A Formulated tick and insect repellent compositions

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
NAVES ET PERROTTET: "Etudes sur les matières végétales volatiles. XIV. Sur la structure du caryophyllène", HELVETICA CHIMICA ACTA., vol. 16, no. VI, 1941, CHVERLAG HELVETICA CHIMICA ACTA. BASEL., pages 789 - 804, XP008094321 *

Also Published As

Publication number Publication date
US20100092404A1 (en) 2010-04-15
CN101568503A (en) 2009-10-28
HK1137738A1 (en) 2010-08-06
BRPI0719468A2 (en) 2014-02-11
US8293217B2 (en) 2012-10-23
EP2129643A2 (en) 2009-12-09
CA2671531C (en) 2016-06-14
WO2008079250A2 (en) 2008-07-03
CA2671531A1 (en) 2008-07-03
CN101568503B (en) 2015-02-04

Similar Documents

Publication Publication Date Title
WO2008079250A3 (en) Hydrogenation of caryophyllene
WO2009050292A3 (en) Catalyst for the hydrogenation of unsaturated hydrocarbons and process for its preparation
EP2277940A4 (en) Process for production of modified conjugated diene copolymer, modified conjugated diene copolymer produced by the process, rubber composition, and tire
EP2239054A4 (en) Catalyst, process for production of the same, and use of the same
CO6351813A2 (en) "METHODS AND COMPOSITIONS TO IMPROVE THE PRODUCTION OF PRODUCTS IN MICROORGANISMS"
EP2188408A4 (en) Catalyst production process
WO2010009077A3 (en) Process for the treatment of heavy oils using light hydrocarbon components as a diluent
PT2583959T (en) Integrated process to produce 2,3,3,3-tetrafluoropropene
WO2010008841A3 (en) Processes for producing fermentation products
SG155870A1 (en) Conjugated diene polymer, process for producing same, and conjugated diene polymer composition and vulcanizate
ATE527266T1 (en) PRODUCTION PROCESS FOR ASENAPINE AND INTERMEDIATE PRODUCTS USED IN THIS PROCESS
AU2009278929A8 (en) Pyrazolo [3,4] pyrimidin-4-yl derivatives and their uses to treat diabetes and obesity
WO2013016668A3 (en) Methylphenidate-prodrugs, processes of making and using the same
ZA200902558B (en) Process for producing modified polymer, modified polymer obtained by the process, and rubber composition containing the same
SG155871A1 (en) Conjugated diene polymer, conjugated diene polymer composition, and process for producing conjugated diene polymer
WO2010009879A3 (en) Methods for producing paricalcitol
ZA201006896B (en) Process for the preparation of branched polybutadiene with a high content of 1,4-cis units
BRPI0814603A2 (en) PROCESS FOR MAKING MALTOBIONATE, USE OF MALTOBIONATE, AND METHODS TO PREVENT OXIDATION DURING A FOOD OR FEED PRODUCTION PROCESS, AND TO PREVENT OXIDATION IN A FOOD OR FOOD PRODUCT
WO2011117360A3 (en) Process for the preparation of 4-cyclohexyl-2-methyl-2-butanol
WO2009062848A3 (en) Methods of preparing, optionally supported, ordered intermetallic palladium gallium compounds, the compounds as such, and their use in catalysis
WO2011004066A3 (en) Process and apparatus for producing hydrocarbons by hydrogenating a terpene feed
WO2010039222A3 (en) Processes for the selective amination of ketomorphinans
MY158885A (en) Method for producing glycerol
EP2184104A4 (en) Catalyst for the production of hydrogen at low temperature, process for production of the catalyst, and process for production of hydrogen
MY159490A (en) Process for the purification of an aqueous stream coming from the fischer-tropsch reaction

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200780047643.X

Country of ref document: CN

WWE Wipo information: entry into national phase

Ref document number: 2671531

Country of ref document: CA

WWE Wipo information: entry into national phase

Ref document number: 3806/DELNP/2009

Country of ref document: IN

WWE Wipo information: entry into national phase

Ref document number: 12519614

Country of ref document: US

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 2007863142

Country of ref document: EP

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 07863142

Country of ref document: EP

Kind code of ref document: A2

ENP Entry into the national phase

Ref document number: PI0719468

Country of ref document: BR

Kind code of ref document: A2

Effective date: 20090619