WO2009041579A1 - 気泡塔型炭化水素反応器、及びスラリー液面検知方法 - Google Patents

気泡塔型炭化水素反応器、及びスラリー液面検知方法 Download PDF

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Publication number
WO2009041579A1
WO2009041579A1 PCT/JP2008/067427 JP2008067427W WO2009041579A1 WO 2009041579 A1 WO2009041579 A1 WO 2009041579A1 JP 2008067427 W JP2008067427 W JP 2008067427W WO 2009041579 A1 WO2009041579 A1 WO 2009041579A1
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WO
WIPO (PCT)
Prior art keywords
slurry
reactor
pressure
bubbling tower
synthesis gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/067427
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English (en)
French (fr)
Inventor
Yasuhiro Onishi
Yuzuru Kato
Eiichi Yamada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cosmo Oil Co Ltd
Japan Petroleum Exploration Co Ltd
Inpex Corp
Japan Oil Gas and Metals National Corp
Nippon Steel Engineering Co Ltd
Eneos Corp
Original Assignee
Cosmo Oil Co Ltd
Japan Petroleum Exploration Co Ltd
Inpex Corp
Japan Oil Gas and Metals National Corp
Nippon Oil Corp
Nippon Steel Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to CN2008801086869A priority Critical patent/CN101835876B/zh
Priority to US12/733,892 priority patent/US8479572B2/en
Priority to EA201070309A priority patent/EA019139B1/ru
Priority to AU2008304801A priority patent/AU2008304801B2/en
Priority to BRPI0817732 priority patent/BRPI0817732A2/pt
Priority to JP2009534408A priority patent/JP5401318B2/ja
Application filed by Cosmo Oil Co Ltd, Japan Petroleum Exploration Co Ltd, Inpex Corp, Japan Oil Gas and Metals National Corp, Nippon Oil Corp, Nippon Steel Engineering Co Ltd filed Critical Cosmo Oil Co Ltd
Priority to EP08834246A priority patent/EP2199369A1/en
Priority to CA2700139A priority patent/CA2700139C/en
Publication of WO2009041579A1 publication Critical patent/WO2009041579A1/ja
Priority to ZA2010/02081A priority patent/ZA201002081B/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/14—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measurement of pressure
    • G01F23/16—Indicating, recording, or alarm devices being actuated by mechanical or fluid means, e.g. using gas, mercury, or a diaphragm as transmitting element, or by a column of liquid
    • G01F23/165—Indicating, recording, or alarm devices being actuated by mechanical or fluid means, e.g. using gas, mercury, or a diaphragm as transmitting element, or by a column of liquid of bubbler type
    • G01F23/168—Indicating, recording, or alarm devices being actuated by mechanical or fluid means, e.g. using gas, mercury, or a diaphragm as transmitting element, or by a column of liquid of bubbler type with electric indicating or recording
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1809—Controlling processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818—Feeding of the fluidising gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
    • B01J8/226—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement internally, i.e. the particles rotate within the vessel
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/34—Apparatus, reactors
    • C10G2/342—Apparatus, reactors with moving solid catalysts
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/14—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measurement of pressure
    • G01F23/18—Indicating, recording or alarm devices actuated electrically
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/14—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measurement of pressure
    • G01F23/18—Indicating, recording or alarm devices actuated electrically
    • G01F23/185—Indicating, recording or alarm devices actuated electrically for discrete levels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/00132—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00539—Pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00584—Controlling the density
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/0061—Controlling the level
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/002—Sensing a parameter of the reaction system inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/0022—Control algorithm comparing a sensed parameter with a pre-set value calculating difference
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00227—Control algorithm taking actions modifying the operating conditions
    • B01J2219/00229—Control algorithm taking actions modifying the operating conditions of the reaction system
    • B01J2219/00234—Control algorithm taking actions modifying the operating conditions of the reaction system inside the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Measurement Of Levels Of Liquids Or Fluent Solid Materials (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　この気泡塔型炭化水素反応器は、水素及び一酸化炭素を主成分とする合成ガスと、液体中に固体の触媒粒子を懸濁させてなるスラリーとの化学反応によって炭化水素化合物を合成する気泡塔型炭化水素反応器であって、前記スラリーを収容する反応器本体と、前記合成ガスを前記スラリーに供給する合成ガス供給部と、 　前記スラリーの液面よりも上方に配されて前記液面上における前記合成ガスの圧力を測定する一の圧力センサと、前記スラリーの液面よりも下方に配されて前記スラリーの圧力を測定する他の圧力センサと、前記圧力センサの測定結果に基づいて前記スラリーの液面位置を検知する液面検知手段と、を備え、前記他の圧力センサが、前記反応器本体の軸方向に間隔をあけて複数設けられている。
PCT/JP2008/067427 2007-09-27 2008-09-26 気泡塔型炭化水素反応器、及びスラリー液面検知方法 Ceased WO2009041579A1 (ja)

Priority Applications (9)

Application Number Priority Date Filing Date Title
US12/733,892 US8479572B2 (en) 2007-09-27 2008-09-26 Bubble column type hydrocarbon synthesis reactor, and slurry level detecting method
EA201070309A EA019139B1 (ru) 2007-09-27 2008-09-26 Реактор синтеза углеводородов типа барботажной колонны и способ определения уровня суспензии
AU2008304801A AU2008304801B2 (en) 2007-09-27 2008-09-26 Bubbling tower hydrocarbon reactor and method of detecting slurry surface level
BRPI0817732 BRPI0817732A2 (pt) 2007-09-27 2008-09-26 Reator de síntese de hidrocarboneto tipo coluna de bolha, e processo de detecção de nível de pasta
JP2009534408A JP5401318B2 (ja) 2007-09-27 2008-09-26 気泡塔型炭化水素反応器、及びスラリー液面検知方法
CN2008801086869A CN101835876B (zh) 2007-09-27 2008-09-26 气泡塔型碳氢化合物反应器和浆液液面检测方法
EP08834246A EP2199369A1 (en) 2007-09-27 2008-09-26 Bubbling tower hydrocarbon reactor and method of detecting slurry surface level
CA2700139A CA2700139C (en) 2007-09-27 2008-09-26 Bubble column type hydrocarbon synthesis reactor, and slurry level detecting method
ZA2010/02081A ZA201002081B (en) 2007-09-27 2010-03-24 Bubble column type hydrocarbon synthesis reactor,and slurry level detecting method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007252522 2007-09-27
JP2007-252522 2007-09-27

Publications (1)

Publication Number Publication Date
WO2009041579A1 true WO2009041579A1 (ja) 2009-04-02

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PCT/JP2008/067427 Ceased WO2009041579A1 (ja) 2007-09-27 2008-09-26 気泡塔型炭化水素反応器、及びスラリー液面検知方法

Country Status (11)

Country Link
US (1) US8479572B2 (ja)
EP (1) EP2199369A1 (ja)
JP (1) JP5401318B2 (ja)
CN (1) CN101835876B (ja)
AU (1) AU2008304801B2 (ja)
BR (1) BRPI0817732A2 (ja)
CA (1) CA2700139C (ja)
EA (1) EA019139B1 (ja)
MY (1) MY152938A (ja)
WO (1) WO2009041579A1 (ja)
ZA (1) ZA201002081B (ja)

Cited By (3)

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WO2014073575A1 (ja) * 2012-11-09 2014-05-15 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素合成反応装置のスタートアップ方法
KR101836383B1 (ko) * 2017-10-26 2018-03-08 주식회사 환경에너지오앤엠 압력밀도식 수위 계측모듈
JP2020093236A (ja) * 2018-12-14 2020-06-18 東レエンジニアリング株式会社 薬液合成装置及び薬液合成方法

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AP3958A (en) * 2010-12-13 2016-12-23 Sasol Tech Pty Ltd Slurry phase apparatus
JP5701070B2 (ja) 2011-01-13 2015-04-15 独立行政法人石油天然ガス・金属鉱物資源機構 触媒回収システム、炭化水素合成反応装置、および炭化水素合成反応システム、並びに触媒回収方法
CN102288256A (zh) * 2011-09-01 2011-12-21 中国海洋石油总公司 一种密闭容器液位测量系统
FR2998812B1 (fr) 2012-12-05 2014-11-21 IFP Energies Nouvelles Injection d'additif dans une unite de synthese d'hydrocarbures a partir de gaz de synthese permettant de controler et maintenir une concentration homogene en catalyseur
US20140305201A1 (en) * 2013-04-12 2014-10-16 Joe David Watson Electronic liquid level sensing device and gauge for liquid-immersed power transformers, reactors and similar equipment
US9377341B1 (en) * 2013-04-12 2016-06-28 Joe David Watson Electronic liquid level sensing device and gauge for liquid-immersed power transformers, reactors and similar equipment
CN106289442B (zh) * 2016-08-05 2019-11-05 河北省电力建设调整试验所 一种脱硫浆液液位准确计算及防止浆液溢流的方法
CN108079910B (zh) * 2016-11-21 2020-01-17 北京华石联合能源科技发展有限公司 一种上流差速控制裂化加氢的反应器及其应用
CN108079911B (zh) * 2016-11-21 2020-02-07 北京华石联合能源科技发展有限公司 一种上流差速控制裂化加氢的反应系统及其应用
GB201705039D0 (en) 2017-03-29 2017-05-10 Weston Aerospace Ltd A Liquid level monitoring system
CN108088531A (zh) * 2017-12-07 2018-05-29 中国恩菲工程技术有限公司 分离界面的检测方法和装置
US10625222B1 (en) 2018-09-28 2020-04-21 Uop Llc Process and apparatus for controlling anti-foam injection using a differential pressure transmitter
CN109724668B (zh) * 2019-03-05 2024-06-25 华北电力科学研究院有限责任公司 一种考虑浆液密度差异的吸收塔液位高度测量装置及方法
CN111412961B (zh) * 2020-02-29 2021-09-17 上海兖矿能源科技研发有限公司 一种多段压差式反应器床层料位测量装置及测量方法
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WO2014073575A1 (ja) * 2012-11-09 2014-05-15 独立行政法人石油天然ガス・金属鉱物資源機構 炭化水素合成反応装置のスタートアップ方法
JP2014095040A (ja) * 2012-11-09 2014-05-22 Japan Oil Gas & Metals National Corp 炭化水素合成反応装置のスタートアップ方法
AU2013342524B2 (en) * 2012-11-09 2016-01-28 Cosmo Oil Co., Ltd. Start-up method of hydrocarbon synthesis reaction apparatus
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EA029608B1 (ru) * 2012-11-09 2018-04-30 Джэпэн Ойл, Гэз Энд Металз Нэшнл Корпорейшн Способ запуска реакторной установки синтеза углеводородов
KR101836383B1 (ko) * 2017-10-26 2018-03-08 주식회사 환경에너지오앤엠 압력밀도식 수위 계측모듈
WO2019083228A1 (ko) * 2017-10-26 2019-05-02 주식회사 환경에너지오앤엠 압력밀도식 수위 계측모듈
JP2020528544A (ja) * 2017-10-26 2020-09-24 エンヴァイロメント エナジー オーアンドエム インコーポレーテッドＥｎｖｉｒｏｎｍｅｎｔ Ｅｎｅｒｇｙ Ｏ＆Ｍ Ｉｎｃ 圧力密度式水位計測モジュール
JP2020093236A (ja) * 2018-12-14 2020-06-18 東レエンジニアリング株式会社 薬液合成装置及び薬液合成方法
JP7175740B2 (ja) 2018-12-14 2022-11-21 東レエンジニアリング株式会社 薬液合成装置及び薬液合成方法

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JP5401318B2 (ja) 2014-01-29
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US20100242594A1 (en) 2010-09-30
MY152938A (en) 2014-12-15
CN101835876B (zh) 2013-08-14
CN101835876A (zh) 2010-09-15
AU2008304801B2 (en) 2011-03-24
ZA201002081B (en) 2011-05-25
BRPI0817732A2 (pt) 2015-03-31
AU2008304801A1 (en) 2009-04-02
JPWO2009041579A1 (ja) 2011-01-27
EA201070309A1 (ru) 2010-10-29

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