WO2009103880A3 - Catalyseur comprenant au moins une zéolithe particuliere et au moins une silice-alumine et procédé d'hydrocraquage de charges hydrocarbonées utilisant un tel catalyseur - Google Patents

Catalyseur comprenant au moins une zéolithe particuliere et au moins une silice-alumine et procédé d'hydrocraquage de charges hydrocarbonées utilisant un tel catalyseur Download PDF

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Publication number
WO2009103880A3
WO2009103880A3 PCT/FR2008/001721 FR2008001721W WO2009103880A3 WO 2009103880 A3 WO2009103880 A3 WO 2009103880A3 FR 2008001721 W FR2008001721 W FR 2008001721W WO 2009103880 A3 WO2009103880 A3 WO 2009103880A3
Authority
WO
WIPO (PCT)
Prior art keywords
catalyst
hydrocracking
alumina
silica
hydrocarbon feedstock
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/FR2008/001721
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English (en)
Other versions
WO2009103880A2 (fr
Inventor
Emmanuelle Guillon
Christophe Bouchy
Johan Martens
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to BRPI0821825-0A priority Critical patent/BRPI0821825A2/pt
Priority to JP2010541077A priority patent/JP2011508667A/ja
Priority to EP08872627A priority patent/EP2234721A2/fr
Priority to US12/811,636 priority patent/US20110042270A1/en
Priority to CN2008801238113A priority patent/CN101909751A/zh
Publication of WO2009103880A2 publication Critical patent/WO2009103880A2/fr
Publication of WO2009103880A3 publication Critical patent/WO2009103880A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/80—Mixtures of different zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing iron group metals, noble metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing iron group metals, noble metals or copper
    • B01J29/74—Noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing iron group metals, noble metals or copper
    • B01J29/76—Iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/78—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • C10G47/20—Crystalline alumino-silicate carriers the catalyst containing other metals or compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12—Silica and alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/20—After treatment, characterised by the effect to be obtained to introduce other elements in the catalyst composition comprising the molecular sieve, but not specially in or on the molecular sieve itself
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/65—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the ferrierite type, e.g. types ZSM-21, ZSM-35 or ZSM-38, as exemplified by patent documents US4046859, US4016245 and US4046859, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7042—TON-type, e.g. Theta-1, ISI-1, KZ-2, NU-10 or ZSM-22
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7046—MTT-type, e.g. ZSM-23, KZ-1, ISI-4 or EU-13
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

L'invention décrit un catalyseur comprenant au moins un métal hydro-déshydrogénant choisi dans le groupe formé par les métaux du groupe VIB et les métaux du groupe VIII et un support comprenant au moins une silice-alumine, et au moins une zéolithe COK-7 seule, ou en mélange avec au moins une zéolithe ZBM-30, ainsi qu'un procédé d'hydrocraquage de charges hydrocarbonées mettant en oeuvre ledit catalyseur.
PCT/FR2008/001721 2008-01-04 2008-12-10 Catalyseur comprenant au moins une zéolithe particuliere et au moins une silice-alumine et procédé d'hydrocraquage de charges hydrocarbonées utilisant un tel catalyseur Ceased WO2009103880A2 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
BRPI0821825-0A BRPI0821825A2 (pt) 2008-01-04 2008-12-10 Catalisador que inclui pelo menos uma zeólita em particular e pelo menos uma sílica-alumina e processo para o hidrocraqueamento de estoque de alimentação de hidrocarboneto que usa tal catalisador
JP2010541077A JP2011508667A (ja) 2008-01-04 2008-12-10 少なくとも１種の特定のゼオライトと少なくとも１つのシリカ−アルミナとを含む触媒、および前記触媒を用いた炭化水素供給原料の水素化分解方法
EP08872627A EP2234721A2 (fr) 2008-01-04 2008-12-10 Catalyseur comprenant au moins une zéolithe particuliere et au moins une silice-alumine et procédé d'hydrocraquage de charges hydrocarbonées utilisant un tel catalyseur
US12/811,636 US20110042270A1 (en) 2008-01-04 2008-12-10 Catalyst comprising at least one particular zeolite and at least one silica-alumina, and process for hydrocracking hydrocarbon feeds using said catalyst
CN2008801238113A CN101909751A (zh) 2008-01-04 2008-12-10 包含至少一种特定沸石和至少一种二氧化硅-氧化铝的催化剂,和使用所述催化剂加氢裂化烃进料的方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0800055A FR2926028B1 (fr) 2008-01-04 2008-01-04 Catalyseur comprenant au moins une zeolithe particuliere et au moins une silice-alumine et procede d'hydrocraquage de charges hydrocarbonees utilisant un tel catalyseur
FR08/00055 2008-01-04

Publications (2)

Publication Number Publication Date
WO2009103880A2 WO2009103880A2 (fr) 2009-08-27
WO2009103880A3 true WO2009103880A3 (fr) 2009-12-03

Family

ID=39595569

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2008/001721 Ceased WO2009103880A2 (fr) 2008-01-04 2008-12-10 Catalyseur comprenant au moins une zéolithe particuliere et au moins une silice-alumine et procédé d'hydrocraquage de charges hydrocarbonées utilisant un tel catalyseur

Country Status (8)

Country Link
US (1) US20110042270A1 (fr)
EP (1) EP2234721A2 (fr)
JP (1) JP2011508667A (fr)
KR (1) KR20100110854A (fr)
CN (1) CN101909751A (fr)
BR (1) BRPI0821825A2 (fr)
FR (1) FR2926028B1 (fr)
WO (1) WO2009103880A2 (fr)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120022224A1 (en) 2010-07-22 2012-01-26 Geraldine Tosin Particles Including Zeolite Catalysts And Their Use In Oligomerization Processes
KR101743293B1 (ko) * 2010-10-22 2017-06-05 에스케이이노베이션 주식회사 다환방향족 탄화수소로부터 고부가의 경방향족 탄화수소를 제조하는 수소화 분해 촉매
CN103930206A (zh) * 2011-10-24 2014-07-16 道达尔炼油法国 用于制备包含介孔的催化剂的方法、由此获得的催化剂及其在加氢转化方法中的用途
RU2502787C1 (ru) * 2012-08-27 2013-12-27 Федеральное государственное бюджетное учреждение науки Институт проблем переработки углеводородов Сибирского отделения Российской академии наук Способ уменьшения вязкости мазута
FR3003563B1 (fr) * 2013-03-21 2015-03-20 IFP Energies Nouvelles Procede de conversion de charges issues de sources renouvelables mettant en oeuvre un catalyseur comprenant une zeolithe nu-10 et une silice alumine
KR101554265B1 (ko) 2013-12-19 2015-09-18 에쓰대시오일 주식회사 비결정질 실리카알루미나-제올라이트 복합체 및 이의 제조방법
WO2016029387A1 (fr) * 2014-08-27 2016-03-03 中国石油天然气集团公司 Catalyseur de transfert de mercaptan bimétallique utilisé dans l'élimination à basse température de mercaptans contenus dans le gaz de pétrole liquéfié
CN110249033A (zh) * 2016-12-21 2019-09-17 沙特阿拉伯石油公司 用于优化加氢裂化工艺的催化剂负载的方法
US11185850B2 (en) * 2019-12-02 2021-11-30 Saudi Arabian Oil Company Dual functional composite catalyst for olefin metathesis and cracking
US11577235B1 (en) * 2021-08-13 2023-02-14 Chevron U.S.A. Inc. Layered catalyst reactor systems and processes for hydrotreatment of hydrocarbon feedstocks

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0046504A1 (fr) * 1980-08-21 1982-03-03 BASF Aktiengesellschaft Zéolite métalsilicate cristalline ZBM-30 et procédé pour sa préparation
FR2852864A1 (fr) * 2003-03-24 2004-10-01 Inst Francais Du Petrole Catalyseur comprenant au moins une zeolithe choisie parmi zbm-30, zsm-48, eu-2 et eu-11 et au moins une zeolithe y et procede d'hydroconversion de charges hydrocarbonees utilisant un tel catalyseur
FR2863913A1 (fr) * 2003-12-23 2005-06-24 Inst Francais Du Petrole Catalyseur zeolithique,support a base de matrice silico-aluminique et de zeolithe, et procede d'hydrocraquage de charges hydrocarbonees
EP1702888A1 (fr) * 2005-03-07 2006-09-20 Institut Francais Du Petrole Solide cristallise COK-7, procécé de préparation et utilisation pour la transformation d'hydrocarbures

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2846574B1 (fr) * 2002-10-30 2006-05-26 Inst Francais Du Petrole Catalyseur et procede d'hydrocraquage de charges hydrocarbonees
FR2852865B1 (fr) * 2003-03-24 2007-02-23 Inst Francais Du Petrole Catalyseur et son utilisation pour l'amelioration du point d'ecoulement de charges hydrocarbonnees
US7402236B2 (en) * 2004-07-22 2008-07-22 Chevron Usa Process to make white oil from waxy feed using highly selective and active wax hydroisomerization catalyst
FR2874837B1 (fr) * 2004-09-08 2007-02-23 Inst Francais Du Petrole Catalyseur dope et procede ameliore de traitement de charges hydrocarbonees
FR2881128B1 (fr) * 2005-01-24 2007-03-23 Inst Francais Du Petrole Nouvelle methode de synthese de la zeolithe zbm-30 a partir d'un melange de composes amines

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0046504A1 (fr) * 1980-08-21 1982-03-03 BASF Aktiengesellschaft Zéolite métalsilicate cristalline ZBM-30 et procédé pour sa préparation
FR2852864A1 (fr) * 2003-03-24 2004-10-01 Inst Francais Du Petrole Catalyseur comprenant au moins une zeolithe choisie parmi zbm-30, zsm-48, eu-2 et eu-11 et au moins une zeolithe y et procede d'hydroconversion de charges hydrocarbonees utilisant un tel catalyseur
FR2863913A1 (fr) * 2003-12-23 2005-06-24 Inst Francais Du Petrole Catalyseur zeolithique,support a base de matrice silico-aluminique et de zeolithe, et procede d'hydrocraquage de charges hydrocarbonees
EP1702888A1 (fr) * 2005-03-07 2006-09-20 Institut Francais Du Petrole Solide cristallise COK-7, procécé de préparation et utilisation pour la transformation d'hydrocarbures

Also Published As

Publication number Publication date
EP2234721A2 (fr) 2010-10-06
JP2011508667A (ja) 2011-03-17
FR2926028A1 (fr) 2009-07-10
BRPI0821825A2 (pt) 2015-06-16
KR20100110854A (ko) 2010-10-13
FR2926028B1 (fr) 2010-02-12
WO2009103880A2 (fr) 2009-08-27
CN101909751A (zh) 2010-12-08
US20110042270A1 (en) 2011-02-24

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