WO2011141136A1 - Glas-schmelzwanne mit vorbau und verfahren zum betrieb - Google Patents
Glas-schmelzwanne mit vorbau und verfahren zum betrieb Download PDFInfo
- Publication number
- WO2011141136A1 WO2011141136A1 PCT/EP2011/002217 EP2011002217W WO2011141136A1 WO 2011141136 A1 WO2011141136 A1 WO 2011141136A1 EP 2011002217 W EP2011002217 W EP 2011002217W WO 2011141136 A1 WO2011141136 A1 WO 2011141136A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- stem
- melting tank
- feed
- melt
- length
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B3/00—Charging the melting furnaces
- C03B3/02—Charging the melting furnaces combined with preheating, premelting or pretreating the glass-making ingredients, pellets or cullet
- C03B3/023—Preheating
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B3/00—Charging the melting furnaces
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B3/00—Charging the melting furnaces
- C03B3/005—Charging the melting furnaces using screw feeders
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B3/00—Charging the melting furnaces
- C03B3/02—Charging the melting furnaces combined with preheating, premelting or pretreating the glass-making ingredients, pellets or cullet
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B5/00—Melting in furnaces; Furnaces so far as specially adapted for glass manufacture
- C03B5/04—Melting in furnaces; Furnaces so far as specially adapted for glass manufacture in tank furnaces
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
Definitions
- the invention relates to a glass melting tank with at least one stem for the input of the feed and at least one charging device.
- parts of the dust are introduced into the regenerative chambers.
- the dust also reacts there with the refractory material and leads to corrosion.
- the dust can also enforce the so-called grid in the regenerative chambers and reduce the efficiency of the air preheating.
- this type of dusting is reinforced with the consequences shown.
- the feed also loses heat energy to the atmosphere, which is lost for the melting process. It has been shown that a mere enlargement of the stems does not help.
- the invention is therefore an object of the invention to improve the feeding technology on the stems of glass tank ovens to the effect that heat losses to the atmosphere and dust transport are reduced in the upper furnace of the tub and yet the heating of the feed is intensified.
- a length "LG" of at least 1 200 mm is provided with an insulating roof which, towards the charging device, has an end wall which encloses, with the roof, a gas space which is open towards the melting tank,
- the task is solved to the full extent, namely heat losses to the atmosphere and a dust transport in the upper furnace of the tub reduced and yet intensified the heating of the feed.
- the stem is enlarged, and its superstructure is open to the tub, so that heat can penetrate radiation in the said superstructure of the stem. With the radiant heat in the stem it is achieved that the mixture is both preheated and sintered.
- the enlargement of the stem also leads to increased flow from the middle of the tub (hot glass) back into this stem. This is accompanied by the transport of heat, which serves to melt the mixture from below accelerated.
- the flow of glass into the stem area is determined by convection. As a result, melting in the actual well area is shortened in terms of time and space, which leads to an increase in output of the plant.
- the driving force is thermal convection.
- the end wall has a lower edge which lies above a plane "E-E" in which the upper edge of the tub is arranged and which delimits a feed gap
- the loading device has a periodically movable insert sheet through which portions of feed material can be metered through the feed gap into the stem and onto the melt,
- the feeder has a screw conveyor through which the feed material can be metered into the stem and onto the melt
- the screw conveyor has a housing that is sealed in the front wall of the stem
- the roof of the porch together with the end wall, encloses a gas space which is open in the direction of the gas space above the melting tank,
- the gas space above the level E-E of the tub rim has a height "H" of at least 600 mm
- the stem has side walls which enclose between them an angle “he” of 0 to 45 degrees open towards the melting tank, in particular if the side walls have an angle “a” of 5 to 30 degrees between them open toward the melting tank lock in,
- the stem at its entrance to the melting tank has a width "BV" of at least 1000 mm.
- the length "LG" of the canopy is at least 1 .200 mm, and / or if:
- the invention also relates to a method for heating feed material to glass melting tanks with at least one stem with a feed device for the input of the feed.
- the width "BV" of the transport path of the feed material in the stem at the entrance to the melting tank is selected to be at least 1.0 m.
- the invention does not produce appreciable gas flow in the region of the stems, so that the risk of dust carryover is greatly reduced. While below the pan cover in the core flow of the combustion region mean flow velocities between 10 and 15 m / sec. were measured, the mean flow velocity in the stems only below 1 m / sec, but were measured temperatures to over 1,300 ° C, resulting in a high energy transfer of about 50 kW / m 2 .
- FIG. 1 shows a vertical cross section through a melting tank in conjunction with vertical longitudinal sections through two stems
- FIG. 2 shows a detail enlargement from FIG. 1 with dimensions
- FIG. 4 shows the prior art with a conventional stem
- FIG. 5 shows the left-hand half of FIG. 1 on an enlarged scale and with an insert plate as loading device in operation
- FIG. 6 shows the left half of FIG. 1 on an enlarged scale and with a screw conveyor as a charging device in operation
- Figure 7 is a plan view of the prior art furnace contents in the operating condition with a carpet of unsintered feedstock
- Figure 8 is a plan view of the furnace contents analogous to Figure 7, but with a carpet of sintered feed.
- a melting tank 1 which is heated with their contents, a molten glass 2 by Brenne rbatterien 3, which are arranged in the end wall 1 a of the melting tank 1 below the mouth of a shaft 4 for combustion air.
- These shafts 4 are associated with heat exchangers, for example, those from the group of regenerators.
- the burner batteries 3 and the shafts 4 are in a known manner, for. B., in the 15- to 30-minute cycle, operated in alternation, ie, while a burner battery 3 is operated, the exhaust gases are withdrawn via the other shaft 4.
- On both sides of the melting tank 1 are in mirror-symmetrical arrangement so-called.
- the melting tank 1 and the stems 6 end up in a common horizontal plane EE.
- the end walls 8 end at the bottom in each case a lower edge 1 1, which leaves about the level E-E narrowest possible feed gap 1 1a for the dosing of feed.
- the length "LG" of the gas space 9 below the canopy 7 is minimally about 70% of the inner length "LV" of the stem 6, in such a way that between the end wall 8 and the adjacent edge of the melting tank 1 and stem 6 still a surface for the storage of the feed material 14 remains free above the molten glass 2. Further details will be described below with reference to Figures 2 and 3.
- the height "H” of the gas chamber 9 via “said plane EE should be at least 600 mm in order to promote the input of energy by radiation and / or flame gases. There are also values of up to 900 mm or more conceivable. In one after the outside sloping course of the canopy 7 is the measure "H" for the height at the entrance of the stem 6 in the gas space 10 of the melting tank first
- FIG. 3 shows, while maintaining and updating the previous reference numbers, that the stem 6 has two side walls 6a and 6b which are connected to the melting tank 1 and enclose therebetween an angle " ⁇ " which opens in the direction of the melting tank 1 and between 0 and 45 degrees, preferably between 5 and 30 degrees.
- This and the width "BV" of at least 1000 mm, preferably of at least 1500 mm, at the transition point, make it possible that the flow paths of the molten glass also run within the stems 6 and are involved to a very considerable extent in the heat exchange. Further details will be given below with reference to Figures 5 and 6 described.
- the figure 4 shows the state of the art the following: In a side wall 1 c of the melting tank 1, an opening is arranged above the very short stem 6, which is preceded by a gate valve 1 d.
- the space bounded by this is so tiny that neither the flame gases nor their radiation have a significant influence on the heat input into the feed material 14 from above.
- the heat input through the molten glass 2 from below is very limited, so that the feed material 14 drives unsintered into the melting tank 1. The effect will be explained in more detail with reference to FIG.
- FIG. 5 also shows the following with respect to the invention:
- the stem 6 and the roofing 7 are associated with a charging device 12 which comprises: a reservoir 13 with a controllable bottom outlet 13a for the charge material 14.
- Underneath is an obliquely arranged insertion plate 15, which is offset by a drive 16 only indicated here in periodic oscillations with low frequency.
- the feed material 14 in the direction of the feed gap 1 1a is added in portions to the surface of the molten glass 2 and drives in the form of cushion 17 through the gas space 9 in the direction of the melting tank 1, in which it is deflected to a melt output.
- FIG. 6 shows a further exemplary embodiment of the invention with the following details:
- the inner length of the canopy 7 corresponds to the inner length "LV" of the stem 6 in FIGS. 2 and 3.
- a feed device 20 which contains: a Reservoir 13 with a controllable bottom outlet for the feed material 14.
- Beneath a horizontal screw conveyor 21 is arranged, which is driven by a motor M.
- the screw conveyor 21 has a cylindrical housing 21 a, which is sealingly guided through the end wall 8 therethrough.
- the feed material 14 is abandoned within the stem 6 on the surface of the molten glass 2 and drives in the form of cushion 17 through the Gas chamber 9 in the direction of the melting tank 1, in which it is not shown here.
- Melt outlet is deflected.
- the spatial design of the volume and the temperature control within the stems 6 according to the invention are chosen such that a flow pattern according to the drawn arrows is established within the glass melt 2.
- a flow in the direction of the inner end of the stems 6 occurs below the charge 14, as a result of which the glass melt 2 delivers a portion of its heat capacity to the charge 14.
- the molten glass 2 sinks in the direction of the bottom of the stem 6 and the trough 1 and returns to it.
- the feed material 14 is heated by the penetrating into the gas space 9 heat radiation, and by this combinatorial effect, the feed material 14 is heated to a high temperature, which favors a partial melting of the particles, a process that is also covered by the term sintering can, and that leads to a prevention of dust.
- FIG. 7 shows the distribution of the unsintered feed material 14 in the prior art with a vertical plan view of the tub contents. It covers a relatively large proportion of the melt surface; and the heat input into the melt 2 is relatively low.
- FIG. 8 shows the distribution of the sintered feed material 14 in the case of the subject invention with a vertical plan view of the tub contents. A significantly greater proportion of the melt surface is left free, and the heat input into the melt 2 is correspondingly greater.
- FIG. 8 clarifies that the feed material 14, starting from the respective stem 6, solidifies by sintering the surface flow according to FIGS. 5 and 6 into a kind of "carpet" which leaves a very large portion of the melt surface free, which in turn also favored the heat input by radiation. In particular, thereby the carryover of feed material is prevented in the melt outlet. It is indeed a synergistic effect.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Melting And Manufacturing (AREA)
- Furnace Charging Or Discharging (AREA)
- Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
- Tunnel Furnaces (AREA)
- Vertical, Hearth, Or Arc Furnaces (AREA)
Abstract
Description
Claims
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201180022944.3A CN102884012B (zh) | 2010-05-11 | 2011-05-04 | 具有投料口的玻璃熔槽和用于运行的方法 |
| PL11722730T PL2569257T3 (pl) | 2010-05-11 | 2011-05-04 | Sposób podgrzewania materiału wsadowego w topliwych wannach szklarskich z opalaniem U-płomiennym |
| JP2013509463A JP5717844B2 (ja) | 2010-05-11 | 2011-05-04 | 投入用突出拡張部を備えるガラス溶融槽及びこの種のガラス溶融槽内で装填物を加熱する方法 |
| RU2012153197/03A RU2520208C1 (ru) | 2010-05-11 | 2011-05-04 | Ванная стекловаренная печь с выступом и способ нагрева шихты в ванной стекловаренной печи |
| EP11722730.6A EP2569257B1 (de) | 2010-05-11 | 2011-05-04 | Verfahren zum Aufheizen von Beschickungsgut in Glasschmelzwannen mit U-Flammenheizung |
| US13/695,650 US9856162B2 (en) | 2010-05-11 | 2011-05-04 | Glass melting tank having a doghouse, and method for heating the charge material in such glass melting tanks |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102010020176.6 | 2010-05-11 | ||
| DE102010020176A DE102010020176A1 (de) | 2010-05-11 | 2010-05-11 | Glas-Schmelzwanne mit U-Flammenbeheizung und Verfahren zum Betrieb |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2011141136A1 true WO2011141136A1 (de) | 2011-11-17 |
Family
ID=44118749
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/EP2011/002217 Ceased WO2011141136A1 (de) | 2010-05-11 | 2011-05-04 | Glas-schmelzwanne mit vorbau und verfahren zum betrieb |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9856162B2 (de) |
| EP (1) | EP2569257B1 (de) |
| JP (1) | JP5717844B2 (de) |
| CN (1) | CN102884012B (de) |
| DE (2) | DE102010020176A1 (de) |
| PL (1) | PL2569257T3 (de) |
| RU (1) | RU2520208C1 (de) |
| WO (1) | WO2011141136A1 (de) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2991759B1 (fr) * | 2012-06-12 | 2014-06-20 | Saint Gobain Isover | Installation de fusion de verre |
| US9643869B2 (en) * | 2012-07-03 | 2017-05-09 | Johns Manville | System for producing molten glasses from glass batches using turbulent submerged combustion melting |
| CN104724907B (zh) * | 2013-12-24 | 2018-05-25 | 肖自江 | 节能环保玻璃棉生产方法及玻璃棉熔窑 |
| CN104724905B (zh) * | 2013-12-24 | 2018-05-04 | 肖自江 | 节能环保玻璃酒瓶生产方法及玻璃酒瓶熔窑 |
| PL3088369T3 (pl) * | 2015-04-27 | 2019-08-30 | Beteiligungen Sorg Gmbh & Co. Kg | Instalacja do wytapiania szkła |
| DE102015108195B4 (de) | 2015-04-27 | 2017-05-11 | Beteiligungen Sorg Gmbh & Co. Kg | Glasschmelzanlage mit einer Schmelzwanne mit U-Flammenbeheizung |
| KR102399011B1 (ko) | 2016-08-26 | 2022-05-17 | 코닝 인코포레이티드 | 유리 물품 제조를 위한 장치 및 방법 |
| WO2019006041A1 (en) * | 2017-06-28 | 2019-01-03 | Corning Incorporated | FUSION DEVICES FOR GLASS FORMING APPARATUS |
| US11912608B2 (en) | 2019-10-01 | 2024-02-27 | Owens-Brockway Glass Container Inc. | Glass manufacturing |
| US12252434B2 (en) | 2020-09-30 | 2025-03-18 | Owens-Brockway Glass Container Inc. | Feeder alcove and batch feeding apparats for a melter |
| CN111458544B (zh) * | 2020-04-18 | 2020-12-11 | 无锡市恒通电器有限公司 | 一种智能电表及其生产用便捷式防止堵塞的注塑装置 |
| MX2023003707A (es) | 2020-09-30 | 2023-05-26 | Owens Brockway Glass Container | Carga sumergida de materia prima de recipientes de fusion. |
| WO2024226239A1 (en) * | 2023-04-24 | 2024-10-31 | Corning Incorporated | Melters for glass forming apparatuses |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB406577A (en) * | 1933-08-01 | 1934-03-01 | United Glass Bottle Mfg Ltd | Improvements in or relating to methods of and means for feeding raw material to glass melting furnaces |
| US2890547A (en) * | 1951-11-10 | 1959-06-16 | Emhart Mfg Co | Apparatus for and method of making glass |
| GB1067240A (en) * | 1964-12-21 | 1967-05-03 | Libbey Owens Ford Glass Co | Method and apparatus for feeding glass making materials to a glass melting tank furnace |
| GB1425461A (en) * | 1972-02-09 | 1976-02-18 | Glass Works Equipment Ltd | Charging of glass furnaces |
| DE8304858U1 (de) * | 1983-07-14 | Nikolaus Sorg GmbH & Co KG, 8770 Lohr a. Main | Einlegevorrichtung für einen Glasschmelzofen | |
| EP0580048A1 (de) * | 1992-07-22 | 1994-01-26 | BETEILIGUNGEN SORG GMBH & CO. KG | Vorrichtung zum Einlegen von Chargiermaterial in Glasschmelzöfen |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2397852A (en) * | 1944-12-23 | 1946-04-02 | Saint Gobain | Glassmaking furnace |
| US3074568A (en) * | 1958-02-05 | 1963-01-22 | Libbey Owens Ford Glass Co | Method of and apparatus for feeding glass batch materials |
| US3219209A (en) * | 1962-06-18 | 1965-11-23 | Libbey Owens Ford Glass Co | Apparatus for delivering fusible material to a glass melting furnace |
| US3294506A (en) * | 1962-06-19 | 1966-12-27 | Libbey Owens Ford Glass Co | Method and apparatus for consolidating batch |
| US3436200A (en) * | 1965-04-22 | 1969-04-01 | Libbey Owens Ford Co | Method of feeding glass batch material |
| US3836349A (en) * | 1972-10-26 | 1974-09-17 | Ppg Industries Inc | Method of making glass |
| US3941576A (en) * | 1974-11-29 | 1976-03-02 | Ppg Industries, Inc. | Method and apparatus for making molten glass with batch guiding means |
| GB1531742A (en) | 1975-01-31 | 1978-11-08 | Pilkington Brothers Ltd | Manufacture of glass |
| JPS52111912A (en) * | 1976-03-18 | 1977-09-20 | Asahi Glass Co Ltd | Glass material melting control method |
| US4329165A (en) * | 1981-02-26 | 1982-05-11 | Ppg Industries, Inc. | Method for enhanced melting of glass batch and apparatus therefor |
| SU1362711A1 (ru) * | 1986-03-07 | 1987-12-30 | Производственное Объединение "Смоленскстеклотара" | Пр моточна регенеративна стекловаренна печь |
| SU1604757A1 (ru) * | 1988-12-26 | 1990-11-07 | Курловский Стекольный Завод Им.Володарского | Стекловаренна ванна печь |
| US5123942A (en) * | 1991-03-21 | 1992-06-23 | Frazier-Simplex, Inc. | System for charging batch/cullet in a glass furnace |
| FR2728254B1 (fr) * | 1994-11-08 | 1997-01-31 | Saint Gobain Vitrage | Procede et dispositif pour la fusion du verre |
| RU2250879C2 (ru) * | 2003-06-05 | 2005-04-27 | Кондрашов Дмитрий Валерьевич | Способ варки бесцветных и цветных железосодержащих стекол из стеклянного боя |
| RU2291116C1 (ru) * | 2005-09-14 | 2007-01-10 | Сергей Владимирович Перфилов | Стекловаренная печь |
| DE102009022696B8 (de) | 2009-05-26 | 2012-05-16 | Beteiligungen Sorg Gmbh & Co. Kg | Verfahren und Vorrichtung zum Beschicken von Glas-Schmelzöfen mit schüttfähigen Glasgemengen |
-
2010
- 2010-05-11 DE DE102010020176A patent/DE102010020176A1/de not_active Withdrawn
- 2010-05-11 DE DE202010017541U patent/DE202010017541U1/de not_active Expired - Lifetime
-
2011
- 2011-05-04 PL PL11722730T patent/PL2569257T3/pl unknown
- 2011-05-04 JP JP2013509463A patent/JP5717844B2/ja active Active
- 2011-05-04 EP EP11722730.6A patent/EP2569257B1/de active Active
- 2011-05-04 CN CN201180022944.3A patent/CN102884012B/zh active Active
- 2011-05-04 RU RU2012153197/03A patent/RU2520208C1/ru active
- 2011-05-04 US US13/695,650 patent/US9856162B2/en active Active
- 2011-05-04 WO PCT/EP2011/002217 patent/WO2011141136A1/de not_active Ceased
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE8304858U1 (de) * | 1983-07-14 | Nikolaus Sorg GmbH & Co KG, 8770 Lohr a. Main | Einlegevorrichtung für einen Glasschmelzofen | |
| GB406577A (en) * | 1933-08-01 | 1934-03-01 | United Glass Bottle Mfg Ltd | Improvements in or relating to methods of and means for feeding raw material to glass melting furnaces |
| US2890547A (en) * | 1951-11-10 | 1959-06-16 | Emhart Mfg Co | Apparatus for and method of making glass |
| GB1067240A (en) * | 1964-12-21 | 1967-05-03 | Libbey Owens Ford Glass Co | Method and apparatus for feeding glass making materials to a glass melting tank furnace |
| GB1425461A (en) * | 1972-02-09 | 1976-02-18 | Glass Works Equipment Ltd | Charging of glass furnaces |
| EP0580048A1 (de) * | 1992-07-22 | 1994-01-26 | BETEILIGUNGEN SORG GMBH & CO. KG | Vorrichtung zum Einlegen von Chargiermaterial in Glasschmelzöfen |
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| Title |
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| ARGENT R D: "THE DOUGHOUSE SYSTEM", GLASS TECHNOLOGY, SOCIETY OF GLASS TECHNOLOGY, SHEFFIELD, GB, vol. 35, no. 2, 1 April 1994 (1994-04-01), pages 61 - 65, XP000439146, ISSN: 0017-1050 * |
| TOOLEY, F.V.: "The Handbook of Glass Manufacture", vol. 1, 1 January 1984, ASHLEE PUBLISHING CO,INC., New York, ISBN: 0 911993-20-7, XP002648008 * |
Also Published As
| Publication number | Publication date |
|---|---|
| RU2520208C1 (ru) | 2014-06-20 |
| EP2569257A1 (de) | 2013-03-20 |
| US20130114638A1 (en) | 2013-05-09 |
| CN102884012B (zh) | 2015-09-09 |
| JP2013526473A (ja) | 2013-06-24 |
| US9856162B2 (en) | 2018-01-02 |
| DE202010017541U1 (de) | 2012-02-27 |
| DE102010020176A1 (de) | 2011-11-17 |
| EP2569257B1 (de) | 2015-09-23 |
| CN102884012A (zh) | 2013-01-16 |
| RU2012153197A (ru) | 2014-06-20 |
| PL2569257T3 (pl) | 2016-03-31 |
| JP5717844B2 (ja) | 2015-05-13 |
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