WO2014016751A2 - Efficient seed coat composition - Google Patents

Efficient seed coat composition Download PDF

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Publication number
WO2014016751A2
WO2014016751A2 PCT/IB2013/055993 IB2013055993W WO2014016751A2 WO 2014016751 A2 WO2014016751 A2 WO 2014016751A2 IB 2013055993 W IB2013055993 W IB 2013055993W WO 2014016751 A2 WO2014016751 A2 WO 2014016751A2
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WIPO (PCT)
Prior art keywords
coating composition
seed coating
acid
agro
bijam
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PCT/IB2013/055993
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French (fr)
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WO2014016751A3 (en
Inventor
Yandapalli Durga Prasad
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Rudraram Research Institute Of Agriculture & Sciences
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Rudraram Research Institute Of Agriculture & Sciences
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    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/02—Fertilisers containing urea or urea compounds containing urea-formaldehyde condensates
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C05D9/02—Other inorganic fertilisers containing trace elements
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00—Other organic fertilisers
    • C05F11/10—Fertilisers containing plant vitamins or hormones
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/30—Layered or coated, e.g. dust-preventing coatings
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/30—Layered or coated, e.g. dust-preventing coatings
    • C05G5/37—Layered or coated, e.g. dust-preventing coatings layered or coated with a polymer
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/40—Fertilisers incorporated into a matrix

Definitions

  • This invention in general relates to the field of agricultural sciences.
  • this invention pertains to seed coating composition.
  • This invention also relates to a method of manufacturing precision, customized, control release fertilizers having applications in the field of agriculture.
  • Controlled release fertilizers are coated or encapsulated fertilizers and slow, release fertilizers have a chemically reduced or low solubility, the latter being mainly derivatives of urea.
  • An ideal synchronized fertilizer would release its nutrients according to the plant growth curve.
  • the objective of the present invention is to invent seed coating composition of providing an accurately controlled quantity of nutrient and to develop precision fertilization customized technology with better specifications for individual crops and environments with a holistic approach to agricultural management for better economics.
  • the primary object of this invention is to provide seed coat composition for precision customized control release fertilizers production using single layer or multilayer technology.
  • Another objective of this invention is to provide seed coat composition and a method of producing crop specific novel precision customized control release fertilizers to coat seeds or to treat the roots of seedlings at the time of sowing or for soil application or for foliar application.
  • Still another object of the invention is to provide necessary method for production of materials needed for accurate application of fertilizers.
  • Table 1 shows the preparation of saturated urea solutions.
  • Table 2 shows the preparation of MSM solution.
  • Table 3 shows the examples of seed coat composition in accordance with present invention.
  • Table 4 shows the examples of seed coat composition with pesticide in accordance with present invention.
  • the seed coat material comprising macronutrients (NPK), micronutrients, hormones, organic acids, lower molecular organic acids was formulated by using structurally modified agro polymer, urea resins ( formaldehyde, furfuraldehyde and Iso- butyraldehyde) along with mixing selected resins of Functional transition metal silicate immobilized on modified agro polymer structure.
  • NPK macronutrients
  • urea resins formaldehyde, furfuraldehyde and Iso- butyraldehyde
  • the materials comprising - modified structured urea resins composition were selected after screening of various ratios of urea, aldehyde [1 : 1 to .01 : 1 v/v] and tested for sustained nutrient release pattern along with seed priming ability.
  • An optimum desired composition for making nitrogenous supply in a sustained pattern was selected and used in the formulation of seed coat composition.
  • the seed coat materials along with insecticide, microbicides are formulated along with hormones. When tested the product shows enhanced priming, growth and vigor of seed.
  • main aspect of the present invention is to prepare a seed coating composition
  • a seed coating composition comprising agro-polymer with nitrogen containing fertilizers and / or urea aldehydes, and /or macro and micronutrients, and /or with hormone solution and / or with MSM solution and/or phosphates and/or functional transition metal silicates (FTMS) and / or solution mixture of poly vinyl alcohol (BIJAM+) and/or low molecular weight organic acids and /or potassium nitrate in a predetermined proportions, wherein seed optionally coated with pesticide mixture, the said composition comprising agro-polymer, organic acid and BIJAM+ is in the ratio of 1.0:0.01 :0.01 to 1 :3:5.
  • the nitrogen containing fertilizers are amide based fertilizers.
  • the nitrogen containing fertilizers are urea or derivatives of urea.
  • the aldehydes are selected from the group comprising formaldehyde (FA), isobutraladehyde (IBA), furfuraladehyde (FFA) or any combination thereof.
  • the ratio of agro polymer, amide and aldehyde varies from 1 : 0.3: 0.3 to 1 : 30: 30 w/w/v.
  • the solution mixture of poly vinyl alcohol comprising of polyvinyl alcohol, water, carboxy methylcellulose powder, paraffin oil, glycerol, and sodium alginate.
  • the BIJAM+ is in the range 0.05 to 3 ml per gram of agro polymer.
  • the BIJAM+ is preferably in the range 1.5 to 2 ml per gram of agro polymer.
  • the hormone solution comprising Gibberllic acid or Indole acetic acid or any combination thereof.
  • the hormone solution is in the range 50 to 1000 ⁇ per gram of agro polymer, more preferably in the range 100 to 900 ⁇ per gram of agro polymer.
  • the seed coating composition as claimed in claim 1 wherein the MSM solution is in the range 0.05 to 6 ml per gram of agro polymer, more preferably in the range 0.15 to 4 ml per gram of agro polymer.
  • the FTMS or immobilized FTMS is in the range of 30 to 400 mg per gram of agro polymer, more preferably in the range of 50 to 300 mg per gram of agro polymer.
  • the low molecular weight organic molecules are fulvic acid and is preferably in the range of 50 to 300 mg per gram of agro polymer.
  • the phosphates are selected from the group comprising ortho-phosphates or poly phosphates or potassium phosphates or any combination thereof and / or chelation with citric acid ranging from 0.001 to 0.3 gram per gram seed coat composition.
  • the micronutrients are salts of Zn, Cu, Mn, Mg, Fe, Boron, molybdenum or combination thereof, wherein, zinc, copper, manganese, molybdenum iron salts at ratios of 5-20; 1-5; 0.01-1; 0.05-3 : 0.1-3 combined (25 ml to 50 ml) and added to potassium silicate 10 to 30 grams, (with or without agro polymer of 5-50 grams) to obtain varied combinations suitable for various crop seed coats.
  • the macro nutrients are nitrogen, phosphorous and potassium, or combination thereof.
  • Yet another aspect of the invention further comprising vitamins such as ascorbic acid in the range 0.01 -0.3 grams per grams of agro polymer.
  • Step-1 100 g of Rice husk was washed with water, added 400 ml of 25% hydrochloric acid and kept for soaking for 2 hours. It was washed with water to get neutral pH.
  • Step-2 Added 30 g NaOH and 400 ml water soaked for 2 hours and washed with water to get neutral pH.
  • Step-3 Added 300 ml of H 2 0 2 (1 :3), mixed well and kept for drying.
  • Step-4 After drying grinded and sieved (throughlOO mesh)
  • Step-1 100 g of Rice husk was washed with water, added 400 ml of 25% hydrochloric acid(v/v) and kept for soaking for 4-5 hours. It was washed with water to get neutral pH.
  • Step-2 Added 30 g NaOH mixed well and added 400 ml water, soaked for 4-5 hours, then washed with water to get neutral pH.
  • Step-3 Added HC1 to get pH 3-4
  • Step-4 Added 300 ml of H 2 0 2 (1 :3), mixed well and kept for soaking for 48 hours.
  • Step-5 After drying grinded and sieved (through 100 mesh)
  • step-2 after adding NaOH flakes temperature rose to 60-65 deg.
  • Step-1 10 g of agro polymer powder is added to 75 ml of saturated urea solution (0,6 g/ml) and 25 ml of formaldehyde (37%). pH is adjusted to 3 with dilute sulphuric acid.
  • Step-2 Material is dried, grinded and sieved (through 100 mesh)
  • IBAAP is prepared with various compositions and procedure is followed as described for UFAP.
  • FFUAP is prepared with the procedure as described for UFAP. 1) Agro polymer - 5 g
  • gibberellic acid 0.1 g is dissolved in 600 ⁇ ethanol, mixed well to dissolve. Then make up to 100 ml with distilled water and mixed well.
  • Ascorbic acid should be prepared freshly.
  • Fulvic acid should be free from moisture.
  • Seeds must be of uniform size and weight.
  • Seeds were coated with pesticides as a primary layer and for secondary layer coating of below composition was given:
  • Table 3 shows the examples of seed coat composition in accordance with present invention.
  • Example- 8 Mixture 4 100 60 40 2.5 Powder
  • Example-9 Mixture 4 1 100 60 40 2.5
  • Example- 11 UFAP 2 100 60 40 1.5 1
  • Example- 12 UFAP 2 1 100 60 40 1.5 1
  • Example- 13 IBAAP; 2 100 60 40 1.5 1
  • Example- 14 FFUAP 2 100 60 40 1.5 1
  • Example- 15 33% 0.15 100 0.75 60 40 1.5 UFAP; 1
  • Example- 16 33% 0.15 1 100 0.75 60 40 1.5 UFAP; 1
  • Example- 17 2.5% 0.15 100 0.75 60 40 1.5 UFAP; 1
  • Example- 18 25% 0.15 1 100 0.75 60 40 1.5 UFAP
  • Example- 19 25% 0.15 0.3 100 0.75 - - 50 1.5 UFAP;
  • Example-20 25% 0.15 0.3 100 0.75 55 55 50 1.5
  • Example-21 25% 0.15 0.3 100 0.75 110 110 50 1.5
  • Example-22 25% 0.15 0.3 100 0.75 225 225 50 1.5
  • Example-23 25% 0.15 0.3 100 0.75 450 450 50 1.5
  • Example-24 25% 0.30 0.3 100 0.75 50 1.5
  • Example-25 25% 0.30 0.3 100 225 225 50 1.5
  • Example-26 25% 0.90 0.3 100 50 1.5
  • Example-27 25% 0.90 0.3 100 225 225 50 1.5
  • Example-28 UFAP 0.15 50 0.75 60 40 50 1.5
  • Example-29 IBAAP; 0.15 50 0.75 60 40 50 1.5
  • Example-31 UFAP 0.15 50 0.75 110 110 50 1.5
  • Example-32 IBAAP; 0.15 50 0.75 110 110 50 1.5
  • Example-33 FFUAP; 0.15 50 0.75 110 110 50 1.5
  • Example-34 UFAP 0.15 50 0.75 225 225 50 1.5
  • Example-35 IBAAP; 0.15 50 0.75 225 225 50 1.5
  • Example-36 FFUAP; 0.15 50 0.1 225 225 50 1.5
  • Example-38 IBAAP; 0.15 50 450 450 50 1.5
  • Example-40 UFAP; 0.15 100 0.75 110 110 50 1.5
  • Example-41 UFAP 0.15 300 0.75 110 110 50 1.5
  • Example-42 UFAP; 0.15 100 0.75 225 225 50 1.5
  • Example-43 UFAP 0.15 300 0.75 225 225 50 1.5
  • Example-44 UFAP 0.15 100 450 450 50 1.5
  • Example-45 UFAP 0.15 300 450 450 50 1.5
  • Example-46 UFAP 0.15 50 225 225 50 1.5
  • Table 4 shows the examples of seed coat composition with pesticide in accordance with present invention.
  • Seed coating treatments of above explained resulted in early onset of seed germination Seedling growth[shoot growth and root growth] and with enhanced germination percentage significantly on variety of crop seeds tested such as cotton , green gram ,black gram, groundnut, rice and vegetables.
  • This seed coat composition gives an economical advantage of enhanced plant growth with precision supply of nutrients to the seeds for viable agriculture which involves multilayer technology also. It is observed that seedlings growth enhances 10 to 50 %.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pretreatment Of Seeds And Plants (AREA)
  • Fertilizers (AREA)

Description

"EFFICIENT SEED COAT COMPOSITION"
The following specification particularly describes the invention and the manner in which it is to be performed.
FIELD OF THE INVENTION
This invention in general relates to the field of agricultural sciences. In particular, this invention pertains to seed coating composition. This invention also relates to a method of manufacturing precision, customized, control release fertilizers having applications in the field of agriculture.
BACKGROUND OF THE INVENTION
The incorporation of nutrients in seed coatings provides a unique opportunity to supply each sown seed with an accurately controlled quantity of nutrient that may preferentially available to the sown species and less available to any neighbouring weed species. Controlled release fertilizers are coated or encapsulated fertilizers and slow, release fertilizers have a chemically reduced or low solubility, the latter being mainly derivatives of urea. An ideal synchronized fertilizer would release its nutrients according to the plant growth curve.
To correct the deficiencies in the plant nutrient application methods, requires development of precision fertilizer customized technology and therefore the objective of the present invention is to invent seed coating composition of providing an accurately controlled quantity of nutrient and to develop precision fertilization customized technology with better specifications for individual crops and environments with a holistic approach to agricultural management for better economics.
There is a need for developing effective seed coat compositions than existing to answer the need for precision farming. Supply of required nutrients, hormones, protectants in a precision way at the time germination of a crop seed with a sustained release pattern with natural plant based agro polymers [derived from seed coat of crops] to increase seed priming, vigour and growth and catalyzing the enhanced growth for increase in crop yield . OBJECTS OF THE INVENTION
Accordingly, the primary object of this invention is to provide seed coat composition for precision customized control release fertilizers production using single layer or multilayer technology.
Another objective of this invention is to provide seed coat composition and a method of producing crop specific novel precision customized control release fertilizers to coat seeds or to treat the roots of seedlings at the time of sowing or for soil application or for foliar application.
Still another object of the invention is to provide necessary method for production of materials needed for accurate application of fertilizers.
BRIEF DESCRIPTION OF TABLES
Table 1 shows the preparation of saturated urea solutions.
Table 2 shows the preparation of MSM solution.
Table 3 shows the examples of seed coat composition in accordance with present invention. Table 4 shows the examples of seed coat composition with pesticide in accordance with present invention.
DETAIL DESCRIPTION OF THE INVENTION
While the invention is susceptible to various modifications and alternative forms, specific aspects thereof has been shown by way of example in the illustrative examples and will be described in detail below. It should be understood, however that it is not intended to limit the invention to the particular forms disclosed, but on the contrary, the invention is to cover all modifications, equivalents, and alternative falling within the spirit and the scope of the invention as defined by the appended claims.
It is to be noted that a person skilled in the art can be motivated from the present invention and modify the various constituents of plant nutrient, which are varying from crop to crop. However, such modification should be construed within the scope and spirit of the invention. Accordingly, the examples are showing only those specific details that are pertinent to understanding the aspects of the present invention so as not to obscure the disclosure with details that will be readily apparent to those of ordinary skill in the art having benefit of the description herein.
The terms "comprises", "comprising", or any other variations thereof, are intended to cover a non-exclusive inclusion, such that a setup, device that comprises a list of components does not include only those components but may include other components not expressly listed or inherent to such setup or device. In other words, one or more elements in a fertilizer composition or method proceeded by "comprises... a" does not, without more constraints, preclude the existence of other elements or additional elements in the composition or method. The seed coat material (composition) comprising macronutrients (NPK), micronutrients, hormones, organic acids, lower molecular organic acids was formulated by using structurally modified agro polymer, urea resins ( formaldehyde, furfuraldehyde and Iso- butyraldehyde) along with mixing selected resins of Functional transition metal silicate immobilized on modified agro polymer structure.
This invention is described with below examples:
The materials comprising - modified structured urea resins composition were selected after screening of various ratios of urea, aldehyde [1 : 1 to .01 : 1 v/v] and tested for sustained nutrient release pattern along with seed priming ability. An optimum desired composition for making nitrogenous supply in a sustained pattern was selected and used in the formulation of seed coat composition. The seed coat materials along with insecticide, microbicides are formulated along with hormones. When tested the product shows enhanced priming, growth and vigor of seed.
Accordingly, main aspect of the present invention is to prepare a seed coating composition comprising agro-polymer with nitrogen containing fertilizers and / or urea aldehydes, and /or macro and micronutrients, and /or with hormone solution and / or with MSM solution and/or phosphates and/or functional transition metal silicates (FTMS) and / or solution mixture of poly vinyl alcohol (BIJAM+) and/or low molecular weight organic acids and /or potassium nitrate in a predetermined proportions, wherein seed optionally coated with pesticide mixture, the said composition comprising agro-polymer, organic acid and BIJAM+ is in the ratio of 1.0:0.01 :0.01 to 1 :3:5.
In other aspect of the invention the nitrogen containing fertilizers are amide based fertilizers. In another aspect of the invention the nitrogen containing fertilizers are urea or derivatives of urea. In yet another aspect of the invention the aldehydes are selected from the group comprising formaldehyde (FA), isobutraladehyde (IBA), furfuraladehyde (FFA) or any combination thereof.
In yet another aspect of the invention the ratio of agro polymer, amide and aldehyde varies from 1 : 0.3: 0.3 to 1 : 30: 30 w/w/v.
In yet another aspect of the invention the solution mixture of poly vinyl alcohol (BIJAM+) comprising of polyvinyl alcohol, water, carboxy methylcellulose powder, paraffin oil, glycerol, and sodium alginate.
In yet another aspect of the invention the BIJAM+ is in the range 0.05 to 3 ml per gram of agro polymer.
In yet another aspect of the invention the BIJAM+ is preferably in the range 1.5 to 2 ml per gram of agro polymer.
In yet another aspect of the invention the hormone solution comprising Gibberllic acid or Indole acetic acid or any combination thereof. In yet another aspect of the invention the hormone solution is in the range 50 to 1000 μΐ per gram of agro polymer, more preferably in the range 100 to 900 μΐ per gram of agro polymer.
In yet another aspect of the invention the seed coating composition as claimed in claim 1, wherein the MSM solution is in the range 0.05 to 6 ml per gram of agro polymer, more preferably in the range 0.15 to 4 ml per gram of agro polymer. In yet another aspect of the invention the FTMS or immobilized FTMS is in the range of 30 to 400 mg per gram of agro polymer, more preferably in the range of 50 to 300 mg per gram of agro polymer. The seed coating composition as claimed in claim 1, wherein the low molecular weight organic molecules are fulvic acid and is in the range of 30 to 400 mg per gram of agro polymer.
In yet another aspect of the invention the low molecular weight organic molecules are fulvic acid and is preferably in the range of 50 to 300 mg per gram of agro polymer.
Still another aspect of the invention the phosphates are selected from the group comprising ortho-phosphates or poly phosphates or potassium phosphates or any combination thereof and / or chelation with citric acid ranging from 0.001 to 0.3 gram per gram seed coat composition.
In yet another aspect of the invention the micronutrients are salts of Zn, Cu, Mn, Mg, Fe, Boron, molybdenum or combination thereof, wherein, zinc, copper, manganese, molybdenum iron salts at ratios of 5-20; 1-5; 0.01-1; 0.05-3 : 0.1-3 combined (25 ml to 50 ml) and added to potassium silicate 10 to 30 grams, (with or without agro polymer of 5-50 grams) to obtain varied combinations suitable for various crop seed coats.
In yet another aspect of the invention the macro nutrients are nitrogen, phosphorous and potassium, or combination thereof. Yet another aspect of the invention further comprising vitamins such as ascorbic acid in the range 0.01 -0.3 grams per grams of agro polymer.
PREPARATION OF STRUCTURALLY MODIFIED AGRO POLYMERS (AP) PROCEDURE - 1
Step-1 : 100 g of Rice husk was washed with water, added 400 ml of 25% hydrochloric acid and kept for soaking for 2 hours. It was washed with water to get neutral pH. Step-2: Added 30 g NaOH and 400 ml water soaked for 2 hours and washed with water to get neutral pH.
Step-3: Added 300 ml of H202 (1 :3), mixed well and kept for drying.
Step-4: After drying grinded and sieved (throughlOO mesh)
PROCEDURE-2
Step-1 : 100 g of Rice husk was washed with water, added 400 ml of 25% hydrochloric acid(v/v) and kept for soaking for 4-5 hours. It was washed with water to get neutral pH. Step-2: Added 30 g NaOH mixed well and added 400 ml water, soaked for 4-5 hours, then washed with water to get neutral pH.
Step-3: Added HC1 to get pH 3-4
Step-4: Added 300 ml of H202 (1 :3), mixed well and kept for soaking for 48 hours.
Step-5: After drying grinded and sieved (through 100 mesh)
CONDITIONS
1. In step-2 after adding NaOH flakes temperature rose to 60-65 deg.
2. Addition of H202 should be done at cold temperatures- 20 deg with ventilation and exhaust.
PREPARATION OF UREA FORMALDEHYDE AGRO POLYMER (UFAP) PROCEDURE
Step-1 : 10 g of agro polymer powder is added to 75 ml of saturated urea solution (0,6 g/ml) and 25 ml of formaldehyde (37%). pH is adjusted to 3 with dilute sulphuric acid.
Step-2: Material is dried, grinded and sieved (through 100 mesh)
PREAPARATION OF UREA ISOBUTERALDEHYDE WITH AGRO POLYMER
(IBAAP)
PROCEDURE
IBAAP is prepared with various compositions and procedure is followed as described for UFAP. SET-1
1) Urea solution - 50 ml IBA - 7.5 ml pH-3
(Slow precipitation)
2) Urea solution - 50 ml IBA -10 ml pH-3
3) Urea solution - 50 ml IBA - 15 ml pH-3
4) Urea solution -50 ml IBA -20 ml pH-3
(fast precipitation)
SET-2
1) Agro polymer - 5 g Urea solution - 25 ml IBA - 7.5 ml pH - 3
2) Agro polymer - 5 g Urea solution - 25 ml IBA -10 ml pH - 3
SET-3
1) Agro polymer - 5 g Urea solution ■50 ml
IBA 10 ml
pH-3 2) Agro polymer -5g
Urea solution ■50 ml
IBA 15 ml
pH-3 3) Agro polymer -5g
Urea solution -50 ml
IBA 20 ml
pH-3 PREAPARTION OF UREA FURFURALDEHYDE WITH AGRO POLYMER
(FFUAP)
PROCEDURE
FFUAP is prepared with the procedure as described for UFAP. 1) Agro polymer - 5 g
Urea solution - 50 ml
Furfur aldehyde -10 ml
pH-3 Keep at 120 °C for 20 minutes and dry at atmospheric temperature. PREAPARTION OF HARMONE SOLUTIONS
PREAPARTION OF GIBBERELLIC ACID
0.1 g of gibberellic acid is dissolved in 600 μΐ ethanol, mixed well to dissolve. Then make up to 100 ml with distilled water and mixed well.
PREAPARTION OF INDOLE ACETICACID 0.1 g of indole acetic acid is dissolved in 600 μΐ ethanol, mixed well to dissolve. Then make up to 100 ml with distilled water and mixed well.
CONDITIONS
Prepared solutions should be kept in cold place and keep away from light.
TABLEl: PREPARATION OF SATURATED UREA SOLUTIONS
S.No. Name g/ml
1 ZnS04.7H20 0.59
2 CuS04.5H20 0.23
3 MnS04.H20 0.40
4 FeS04.7H20 0.10
5 Boric Acid 0.50
6 L- Ascorbic acid 0.20
7 Ammonium Molybdate 0.10
8 Sodium Molybdate 0.85
9 Citric acid 0.23
10 KH2P04 0.2
11 Zn(N03)2.6H20 1.0
12 Cu(N03)2.3H20 0.38
13 Urea Solution 0.6
TABLE2: PREPARATION OF MSM SOLUTION
S.No Name ml
1 ZnS04.7H20 10
2 CuS04.5H20 1
3 MnS04.H20 1
4 FeS04.7H20 0.1
Figure imgf000011_0001
CONDITIONS
Ascorbic acid should be prepared freshly.
PREPARATION OF FUNCTIONAL TRANSITION METAL SILICATES POWDERS
(plain)
Zinc nitrate - 20 ml
Copper Nitrate - 5 ml
Manganous sulphate - 0.1 ml
Ammonium Molybdate - 0.5 ml
Ferrous Sulphate - 0.1 ml
Potassium Silicate - 15 g
CONDITIONS
Filter and dry the above mixture at atmospheric temperature. FUNCTIONAL TRANSITION METAL SILICATES WITH AGRO POLYMER
(Nitrate form)
Agro Polymer - 5 g
Zinc nitrate - 20 ml
Copper Nitrate - 5 ml
Manganous sulphate - 0.1 ml
Ammonium Molybdate - 0.5 ml
Ferrous Sulphate - 0.1 ml
Potassium Silicate - 15 g CONDITIONS
Filter and dry the above mixture at atmospheric temperature.
FUNCTIONAL TRANSITION METAL SILICATES WITH AGRO POLYMER
(Sulphate form)
Agro Polymer 7.5 g
Zinc Sulphate 100 ml
Copper Sulphate - 10 ml
Manganous sulphate - 10 ml
Ammonium Mo lybdate- 1 ml
Ferrous Sulphate - 1 ml
Potassium Silicate - 75 g
CONDITIONS
Filter and dry the above mixture at atmospheric temperature.
pH - 3
PREPARATION OF BIJAM+ COATING MATERIAL
10 g polyvinyl alcohol is taken and added 100 ml of water mixed well and added 250 mg of carboxy methylcellulose powder. To this mixture is added 450 μΐ paraffin oil and 450 μΐ glycerol and mixed well. Then added 3 g of sodium alginate and 25 ml of water and mixed by heating on water bath.
BIJAM + material are added to various compositions for coating, attachment to seed, for uniform single layering or multiple layering. EXAMPLES
The following examples are given by way of illustration and therefore should not be construed to limit the scope of the present invention.
EXAMPLE 1
Agropolymer -1 g
Potassium Nitrate - 300 mg
MSM solution - 2 ml
Fulvic acid - 100 mg Water - 1 ml
BIJAM+ - 3 g
Add 20 g of cottonseed or green gram to the above mixture . It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 2
Agropolymer -ig
Potassium Nitrate - 300 mg
MSM solution -2 ml
Fulvic acid - 100 mg
Water - 1 ml
Gibberellic acid -60 μΐ
Indole acetic acid -40 μΐ
BIJAM+ -3g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedling growth enhances 10 to 50 %.
EXAMPLE 3
Agropolymer -ig
Potassium Nitrate -ig
FTMS -O.lg
MSM solution -2 ml
Fulvic acid - 100 mg
Water - 1 ml
Gibberellic acid -60 μΐ
Indole aceticacid -40 μΐ
BIJAM + 3g
Add 20 g of cottonseed or green gram to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 4
25% UFAP -2 g
MSM solution - 300 μΐ Fulvic acid - 100 mg
Water - 1.5 ml
Gibberellic acid - 30 μΐ
Indole aceticacid - 20 μΐ
BIJAM+ - 2 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 5
25% UFAP -2 g
MSM solution - 300 μΐ
Potassium Nitrate - 1 g
Fulvic acid - 100 mg
Water - 1.5 ml
Gibberellic acid - 30 μΐ
Indole aceticacid - 20 μΐ
BIJAM+ - 2 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
TYPE-1
Agropolymer -10 g
MSM solution - 10 ml
Urea solution - 75 ml
Formaldehyde - 25 ml
It is observed that seedlings growth enhances 10 to 50 %.
TYPE-2
Agropo lymer - 10 g
MSM solution - 10 ml
FTMS - 0.5 g
Urea solution - 75 ml
Formaldehyde - 25 ml It is observed that seedlings growth enhances 10 to 50 %. Mixture Powder
Urea formaldehyde with agro polymer - 3 g
25ml urea solution+7.5 IBA+5gAP - 3 g
Urea furfuraldehyde with Agropolymer - 3 g
Mixed well and taken for different given below examples EXAMPLE 6
Mixed powder - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg
Gibberellic acid - 60 μΐ
Indole aceticacid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 7
Mixed powder - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole aceticacid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 8
Mixed powder - 1 g
MSM solution - 4 ml Fulvic acid - 100 mg
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 2.5 g
Add 20 g of cotton seed to the above mixture
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 9
Mixed powder - 1 g
MSM solution - 4 ml
Fulvic acid - 100 mg
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 2.5 g
Add 20 g of cottonseed or green gram to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 10
Mixed powder - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg
Gibberellic acid - 30 μΐ
Indole acetic acid - 20 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 11
UFAP l g
MSM solution - 2 ml
Fulvic acid 100 mg
Gibberellic acid 60 μΐ Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 12
UFAP - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 13
IBAAP - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 14
FFUAP - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g Add 20 g of cotton seed to the above mixture
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 15
33% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %
EXAMPLE 16
33% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 17
25% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 18
25% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
MSM WITH HARMONES BASED VARIATIONS
EXAMPLE 19: 25%UFAP treatment
25%UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
FTMS - 50 mg
Potassium Nitrate - 300 mg
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 20: 25% UFAP (GA. IAA-55uF)
25%UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg Water - 750 μΐ
FTMS - 50 mg
Potassium Nitrate - 300 mg
Gibberellic acid - 55 μΐ
Indole acetic acid - 55 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 21: 25% UFAP(GAJAA-1 ΙΟμΙ)
25%UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
FTMS - 50 mg
Potassium Nitrate - 300 mg
Gibberellic acid - 110 μΐ
Indole acetic acid - 110 μΐ
BIJAM+ - 1 -5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 22; 25°, /„ UFAP (GA. ΙΑΑ-225μ1)
25%UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
FTMS - 50 mg
Potassium Nitrate - 300 mg
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 23; 25%UFAP (ΟΑ,ΙΑΑ-450μΓ)
25%UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
FTMS - 50 mg
Potassium Nitrate - 300 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 24; 25% UFAP (Μ8Μ-300μΓ)
25%UFAP - 1 g
MSM solution - 300 μΐ
Fulvic acid - 100 mg
FTMS - 50 mg
Potassium Nitrate - 300 mg
Water - 750 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 25; 25% υΡΑΡ(βΑ.ΙΑΑ-225μ1.Μ5Μ-300μΓ) 25%UFAP - 1 g
MSM solution - 300 μΐ
Fulvic acid - 100 mg
FTMS - 50 mg
Potassium Nitrate - 300 mg Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 26; 25% UFAP (MSM-900ui)
25%UFAP - 1 g
MSM solution - 900 μΐ
Fulvic acid - lOO mg
FTMS - 50mg
Potassium Nitrate - 300 mg
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture. It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 27; 25%UFAP(GAJAA-225ul Μ8Μ-900μΓ)
25% UFAP - 1 g
MSM solution - 900 μΐ
Fulvic acid - 100 mg
FTMS - 50 mg
Potassium Nitrate - 300 mg
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g
Add 20 g of cottonseed or green gram to the above mixture It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 28; UFAP treatment
UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 29; IBAAP treatment
IBAAP - i g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 30; FFU treatment
FFUAP - i g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 31: UFAP - 110 μΐ hormones
UFAP - lg
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 110 μΐ
Indole acetic acid - Ι ΙΟ μΙ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 32: IBA - 110 μΐ hormones
IBAAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 1 10 μΐ
Indole acetic acid - 110 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 33: FFU - 110 μΐ hormones
FFUAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg Water - 750 μΐ
Gibberellic acid - 110 μΐ
Indole acetic acid - 110 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 34; UFAP - 225 μΐ hormones
UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 35; IBAAP - 225 μΐ .hormones
IBAAP - i g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other EXAMPLE 36; FFUAP - 225 ul .hormones)
FFUAP - i g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Water - 100 μΐ
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 37;UFAP - 450 μΐ hormones
UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 38; IBAAP - 450 μΐ hormones
IBAAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 1.5 g Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 39; FFUAP - 450 μΐ hormones
FFUAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %.
TREATMENTS: FULVIC ACID AND HARMONES VARIATION
EXAMPLE 40; Fulvicacid-O. lg.l 10- μΐ . hormones
UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 110 μΐ
Indole acetic acid - 110 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 41; Fulvic acid-0.3g, 110- μΐ hormones
UFAP - 1 g MSM solution - 150 μΐ
Fulvic acid - 300 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 110 μΐ
Indole acetic acid - 110 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %.
UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 43; Fulvicacid-0.3e, 225 ul hormones
UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 300 mg
FTMS - 50 mg
Water - 750 μΐ
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+ - 1.5 g Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 44; Fulvicacid-O. lg. 450- μΐ hormones
UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
FTMS - 50 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 1-5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 300 mg
FTMS - 50 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 1.5 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other
It is observed that seedlings growth enhances 10 to 50 %.
Conditions:
1. Fulvic acid should be free from moisture.
2. Mixing and coating should be uniform.
3. Seeds must be of uniform size and weight.
4. Place the seeds uniform positions EXAMPLE 46
UFAP l g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Gibberellic acid - 225 μΐ
Indole acetic acid - 225 μΐ
BIJAM+- 2.1 g
Total mixture added to 20 g Cottonseed.
It is observed that seedlings growth enhances 10 to 50 %
EXAMPLE 47
UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 50 mg
FTMS - 50 mg
Gibberellic acid - 450 μΐ
Indole acetic acid - 450 μΐ
BIJAM+ - 2.1 g
Separate this mixture into two halves and add 10 g of cottonseed to one and 10 g of green gram to other.
It is observed that seedlings growth enhances 10 to 50 %.
PESTICIDE COATING ON SEEDS
Seeds were coated with pesticides as a primary layer and for secondary layer coating of below composition was given:
EXAMPLE 48; UFAP Control:
UFAP - 1 g
MSM solution - 2 ml
Fulvic acid - 100 mg Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 49; 25% UFAP:
25% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 50: 25% UFAP:
25% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20g of cotton seed to the above mixture
It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 51: 33% UFAP (10-50-100)
33% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 52; 33% UFAPQ 0-50- 100)
33% UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Potassium Nitrate - 1 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %>.
EXAMPLE 53; 33% UFAPQ 0-50- 100) with FTMS
33% UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Potassium Nitrate - i g
FTMS - O. l g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %>
EXAMPLE 54; 33% UFAP (10-50-100) with FTMS 33% UFAP - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Potassium Nitrate - i g
FTMS - 0.3 g
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1-5 g
Add 20 g of cotton seed to the above mixture
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 55; IBAAP treatment
IBAAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 56; FFUP treatment
FUAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 57; Mixture treatment
Mixture - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 58; 25% UFAP treatment
25%UFAP - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %.
EXAMPLE 59; TYPE-1
Type- 1 material - 1 g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
It is observed that seedlings growth enhances 10 to 50 %. EXAMPLE 60; TYPE-2
Type-2 material - i g
MSM solution - 150 μΐ
Fulvic acid - 100 mg
Water - 750 μΐ
Gibberellic acid - 60 μΐ
Indole acetic acid - 40 μΐ
BIJAM+ - 1.5 g
Add 20 g of cotton seed to the above mixture.
0 It is observed that seedlings growth enhances 10 to 50 %.
Table 3 shows the examples of seed coat composition in accordance with present invention.
Figure imgf000035_0001
Example- 8 Mixture 4 100 60 40 2.5 Powder;
1
Example-9 Mixture 4 1 100 60 40 2.5
Powder;
1
Example- 10 Mixture 2 100 30 20 1.5
Powder;
1
Example- 11 UFAP; 2 100 60 40 1.5 1
Example- 12 UFAP; 2 1 100 60 40 1.5 1
Example- 13 IBAAP; 2 100 60 40 1.5 1
Example- 14 FFUAP; 2 100 60 40 1.5 1
Example- 15 33% 0.15 100 0.75 60 40 1.5 UFAP; 1
Example- 16 33% 0.15 1 100 0.75 60 40 1.5 UFAP; 1
Example- 17 2.5% 0.15 100 0.75 60 40 1.5 UFAP; 1
Example- 18 25% 0.15 1 100 0.75 60 40 1.5 UFAP
Example- 19 25% 0.15 0.3 100 0.75 - - 50 1.5 UFAP;
1
Example-20 25% 0.15 0.3 100 0.75 55 55 50 1.5
UFAP;
1
Example-21 25% 0.15 0.3 100 0.75 110 110 50 1.5
UFAP;
1
Example-22 25% 0.15 0.3 100 0.75 225 225 50 1.5
UFAP;
1
Example-23 25% 0.15 0.3 100 0.75 450 450 50 1.5
UFAP;
1
Example-24 25% 0.30 0.3 100 0.75 50 1.5
UFAP;
1
Example-25 25% 0.30 0.3 100 225 225 50 1.5
UFAP;
1
Example-26 25% 0.90 0.3 100 50 1.5
UFAP
Example-27 25% 0.90 0.3 100 225 225 50 1.5
UFAP; 1
Example-28 UFAP; 0.15 50 0.75 60 40 50 1.5
1
Example-29 IBAAP; 0.15 50 0.75 60 40 50 1.5
1
Example-30 FFUAP; 0.15 50 0.75 60 40 50 1.5
1
Example-31 UFAP; 0.15 50 0.75 110 110 50 1.5
1
Example-32 IBAAP; 0.15 50 0.75 110 110 50 1.5
1
Example-33 FFUAP; 0.15 50 0.75 110 110 50 1.5
1
Example-34 UFAP; 0.15 50 0.75 225 225 50 1.5
1
Example-35 IBAAP; 0.15 50 0.75 225 225 50 1.5
1
Example-36 FFUAP; 0.15 50 0.1 225 225 50 1.5
1
Example-37 UFAP; 0.15 50 450 450 50 1.5
1
Example-38 IBAAP; 0.15 50 450 450 50 1.5
1
Example-39 FFUAP; 0.15 - 50 - 450 450 50 1.5 1
Example-40 UFAP; 0.15 100 0.75 110 110 50 1.5
1
Example-41 UFAP; 0.15 300 0.75 110 110 50 1.5
1
Example-42 UFAP; 0.15 100 0.75 225 225 50 1.5
1
Example-43 UFAP; 0.15 300 0.75 225 225 50 1.5
1
Example-44 UFAP; 0.15 100 450 450 50 1.5
1
Example-45 UFAP; 0.15 300 450 450 50 1.5
1
Example-46 UFAP; 0.15 50 225 225 50 1.5
1
Example-47 UFAP; 0.15 50 450 450 50 2.1
1
Table 4 shows the examples of seed coat composition with pesticide in accordance with present invention.
Figure imgf000040_0001
OBSERVATIONS ON DIFFERENT VARIANTS OF SEED TREATMENTS
Seed coating treatments of above explained resulted in early onset of seed germination Seedling growth[shoot growth and root growth] and with enhanced germination percentage significantly on variety of crop seeds tested such as cotton , green gram ,black gram, groundnut, rice and vegetables. ADVANTAGE
This seed coat composition gives an economical advantage of enhanced plant growth with precision supply of nutrients to the seeds for viable agriculture which involves multilayer technology also. It is observed that seedlings growth enhances 10 to 50 %.
The inventors have been working to develop the invention, so that advantage can be achieved in an economical, practical, and facile manner. While preferred aspects and example configurations have been shown and described, it is to be understood that various further modifications and additional configurations will be apparent to those skilled in the art. It is intended that the specific embodiments and configurations herein disclosed are illustrative of the preferred nature of the invention, and should not be interpreted as limitations on the scope of the invention.

Claims

THE CLAIMS
1. A seed coating composition comprising agro-polymer with nitrogen containing fertilizers and / or urea aldehydes, and /or macro and micronutrients, and /or with hormone solution and / or with MSM solution and/or phosphates and/or functional transition metal silicates (FTMS) and / or solution mixture of poly vinyl alcohol (BIJAM+) and/or low molecular weight organic acids and /or potassium nitrate in a predetermined proportions, wherein seed optionally coated with pesticide mixture, the said composition comprising agro-polymer, organic acid and BIJAM+ is in the ratio of 1.0:0.01 :0.01 to 1 :3:5.
2. The seed coating composition as claimed in claim 1, wherein nitrogen containing fertilizers are amide based fertilizers.
3. The seed coating composition as claimed in claim 1 or 2, wherein nitrogen containing fertilizers are urea or derivatives of urea.
4. The seed coating composition as claimed in claim 1, wherein aldehydes are selected from the group comprising formaldehyde (FA), isobutraladehyde (IBA), furfuraladehyde (FFA) or any combination thereof.
5. The seed coating composition as claimed in claim 1, wherein the ratio of agro polymer, amide and aldehyde varies from 1 : 0.3: 0.3 to 1 : 30: 30 w/w/v.
6. The seed coating composition as claimed in claim 1, wherein the solution mixture of poly vinyl alcohol (BIJAM+) comprising of polyvinyl alcohol, water, carboxy methylcellulose powder, paraffin oil, glycerol, and sodium alginate.
7. The seed coating composition as claimed in claim 6, wherein the BIJAM+ is in the range 0.05 to 3 ml per gram of agro polymer.
8. The seed coating composition as claimed in claim 1, wherein the BIJAM+ is preferably in the range 1.5 to 2 ml per gram of agro polymer.
9. The seed coating composition as claimed in claim 1, wherein the hormone solution comprising Gibberllic acid or Indole acetic acid or any combination thereof.
10. The seed coating composition as claimed in claim 1, wherein the hormone solution is in the range 50 to 1000 μΐ per gram of agro polymer.
11. The seed coating composition as claimed in claim 1, wherein the hormone solution is preferably in the range 100 to 900 μΐ per gram of agro polymer.
12. The seed coating composition as claimed in claim 1, wherein the MSM solution is in the range 0.05 to 6 ml per gram of agro polymer.
13. The seed coating composition as claimed in claim 1, wherein the MSM solution is preferably in the range 0.15 to 4 ml per gram of agro polymer.
14. The seed coating composition as claimed in claim 1, wherein the FTMS or immobilised FTMS is in the range of 30 to 400 mg per gram of agro polymer.
15. The seed coating composition as claimed in claim 1, wherein the FTMS or immobilised FTMS is preferably in the range of 50 to 300 mg per gram of agro polymer.
16. The seed coating composition as claimed in claim 1, wherein the low molecular weight organic molecules are fulvic acid and is in the range of 30 to 400 mg per gram of agro polymer.
17. The seed coating composition as claimed in claim 1, wherein the low molecular weight organic molecules are fulvic acid and is preferably in the range of 50 to 300 mg per gram of agro polymer.
18. The seed coating composition as claimed in claim 1, wherein phosphates are selected from the group comprising ortho-phosphates or poly phosphates or potassium phosphates or any combination thereof and / or chelation with citric acid ranging from 0.001 to 0.3 gram per gram seed coat composition.
19. The seed coating composition as claimed in claim 1, wherein the micronutrients are salts of Zn, Cu, Mn, Mg, Fe, Boron, molybdenum or combination thereof.
20. The seed coating composition as claimed in claim 1, wherein the macro nutrients are nitrogen, phosphate, potassium or combination thereof.
21. The seed coating composition as claimed in claim 19, wherein zinc, copper, manganese, molybdenum iron salts at ratios of 5-20; 1-5; 0.01-1; 0.05-3 : 0.1-3 combined (25 ml to 50 ml) and added to potassium silicate 10 to 30 grams, (with or without agro polymer of 5-50 grams) to obtain varied combinations suitable for various crop seed coats.
22. The seed coating composition as claimed in claim 1, wherein composition further comprising vitamins such as ascorbic acid in the range 0.01 -0.3 grams per grams of agro polymer.
23. The seed coating composition as claimed in any preceding claims enhances seedling growth 10 to 50 %.
PCT/IB2013/055993 2012-07-22 2013-07-22 Efficient seed coat composition Ceased WO2014016751A2 (en)

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WO2016141485A1 (en) 2015-03-10 2016-09-15 Compass Minerals Manitoba Inc. Potassium-based starter fertilizer
EP3268333A4 (en) * 2015-03-10 2018-11-07 Compass Minerals Manitoba Inc. Potassium-based starter fertilizer
US10351481B2 (en) 2015-03-10 2019-07-16 Compass Minerals Manitoba Inc. Potassium-based starter fertilizer
WO2016186526A1 (en) * 2015-05-20 2016-11-24 Ballance Agri-Nutrients Limited Fertiliser composition
EP3483136A1 (en) * 2017-11-10 2019-05-15 Bio3G Biostimulating composition for stimulating soil microbial flora, fertiliser composition comprising the same, methods of preparation and application and uses thereof
FR3073515A1 (en) * 2017-11-10 2019-05-17 Bio3G BIOSTIMULANT COMPOSITION FOR STIMULATION OF MICROBIAL SOIL FLORA, FERTILIZING COMPOSITION COMPRISING SAME, METHODS OF PREPARATION AND APPLICATION AND USES THEREOF

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