WO2016179792A1 - 制备粒子能多功能活性水的复合材料、制备方法及装置 - Google Patents

制备粒子能多功能活性水的复合材料、制备方法及装置 Download PDF

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Publication number
WO2016179792A1
WO2016179792A1 PCT/CN2015/078758 CN2015078758W WO2016179792A1 WO 2016179792 A1 WO2016179792 A1 WO 2016179792A1 CN 2015078758 W CN2015078758 W CN 2015078758W WO 2016179792 A1 WO2016179792 A1 WO 2016179792A1
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Prior art keywords
water
steam
composite material
particles
particle
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PCT/CN2015/078758
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English (en)
French (fr)
Inventor
黄景焕
黄尧权
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Jinghuan Particle Energy Technology Development Co Ltd
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Jinghuan Particle Energy Technology Development Co Ltd
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Priority to PCT/CN2015/078758 priority Critical patent/WO2016179792A1/zh
Priority to US15/545,666 priority patent/US10266435B2/en
Priority to EP15891495.2A priority patent/EP3248943A4/en
Priority to JP2017555825A priority patent/JP6495482B2/ja
Priority to KR1020177019896A priority patent/KR101967725B1/ko
Priority to RU2017127702A priority patent/RU2017127702A/ru
Publication of WO2016179792A1 publication Critical patent/WO2016179792A1/zh
Anticipated expiration legal-status Critical
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    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/38—Other non-alcoholic beverages
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
    • B01D35/02—Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/005—Systems or processes based on supernatural or anthroposophic principles, cosmic or terrestrial radiation, geomancy or rhabdomancy
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2305/00—Use of specific compounds during water treatment
    • C02F2305/08—Nanoparticles or nanotubes

Definitions

  • the invention relates to a composite material, a preparation method and a device for preparing particles capable of multifunctional active water.
  • water In real life, water is the basic material that people are not familiar with. Every day we cannot do without water. When you leave the water, all creatures will be extinct. People know how to use water and know that water is an indispensable resource for human survival.
  • the basic structure of a water molecule is H 2 O, which consists of one oxygen atom and two hydrogen atoms. In nature, there are more than 1,300 kinds of water molecules. Most water molecules are rare in nature. There are no more than 20 common water molecules. About half of them are in nature for about 12 years and the other half. It is the water of eternal. How is water formed? Most authorities in the academic circles believe that water is the product of the big bang.
  • the big bang produced a large number of hydrogen and oxygen atoms, which were then bonded by hydrogen and oxygen atoms to produce water.
  • a single water molecule exists as a triangle with three atoms at an angle of 104.52 degrees.
  • water is agglomerated by more than 10 water molecules, which is academically called "macromolecule water.” Why does water hold a group? In theory, it is believed to be caused by water degradation and pollution. After the water is polluted for a long time, the structure of the water molecules changes, and the small molecule water becomes the disordered macromolecular water, which causes the water's dissolving power, penetration force and diffusion force to degrade. Therefore, the water that exists in the natural state is a large molecule of water.
  • the various trace elements contained in the water are the result of long-term mineralization of water.
  • the academic study found that the water molecules are angularly distributed, and the nonlinear distribution is due to the negative charge on one side of the oxygen, the positive charge on the hydrogen side, and the non-uniform distribution of the positive charge around the negative charge.
  • the positive electrode attracts the adjacent negative electrode, thereby causing the water molecules to stick together to form a macromolecular water.
  • the covalent bond between the hydrogen and oxygen atoms of water molecules is formed by sharing a pair of electrons.
  • the sharing of a pair of electrons in water is not uniform, and oxygen requires electrons more than hydrogen.
  • the water molecules are agglomerated. Therefore, when the water is heated to 100 degrees, the force of the charge is overcome, and the water molecules are separated.
  • the conductivity of water gradually decreases during heating, and it is basically non-conductive when heated to 100 degrees.
  • macromolecular water can be dissociated into a single molecule state, but as the temperature decreases, the water molecules gradually Association and aggregation - macromolecular water. How to make water molecules no longer associate under normal temperature is one of the important topics in the study of basic materials.
  • Magnetized water and electrolytic ionized water use magnetization and electrolysis technology to dissociate macromolecular water into small molecular water; reverse osmosis membrane purifies water by reacting magnetic force and pressure to the permeable membrane, releasing hydrogen and oxygen atoms, and also obtaining A small molecule of water. Under normal temperature conditions, this small molecule water gradually aggregates and forms macromolecular water. Under normal circumstances, the time of keeping the small molecule state is within 72 hours, and the sealed state can reach 15 days under the action of temperature. Will immediately form a large molecule of water. This indicates that its stability and activity are defective.
  • the prior art fails to obtain stable, special-active small molecule water.
  • the invention is firstly prepared to obtain a particle multifunctional active water, which has special activity and energy effects, and can be used for food, health care, medicine, biology, environment, disease control, agriculture, military, machinery, energy, daily life. Life and so on.
  • the present invention provides a composite material for preparing a particle-multifunctional active water comprising the following components: Si, Re, Pt, Ge, Nb, Ni, Se and Mg.
  • the composite material contains components and parts by weight of the components as follows:
  • the composite material consists of the following parts by weight:
  • the composite material is spherical, has a spherical shape with a through hole at the center, a sheet shape or an eggshell shape with one end open.
  • the invention also provides a preparation method of the composite material, comprising the following steps:
  • step 2) The mixture obtained in the step 1) is placed in a magnetizing furnace for magnetization, the magnetization is 5-10 A/m, and the magnetization is 100-200 h;
  • step 2) placing the magnetized material in step 2) in a molding die and vacuum sintering;
  • the material obtained in the step 3) is placed in a magnetizing furnace for magnetization, the magnetization is 80-100 A/m, and the magnetization is 100-300 h to obtain the composite material.
  • the silicon, germanium, platinum, rhodium, iridium, nickel, selenium and magnesium described in the step 1) are all nano-sized particles.
  • the magnetization intensity in step 2) is 7 A/m, and the magnetization time is 120 to 125 h.
  • the sintering temperature in step 3 is from 800 to 1000 °C.
  • the vacuum sintering in step 3) is low-temperature transformation sintering: step 1) the magnetized material is placed in a molding die, and under vacuum, first sintered at a temperature of 800 to 850 ° C for 1 to 3 hours, and then 900 to 1000. The temperature of °C is sintered for 10 to 15 hours.
  • the magnetization intensity in step 4) is 95 to 100 A/m, and the magnetization time is 200 to 250 h.
  • the invention also discloses the above composite material for preparing a particle capable multifunctional active water, comprising:
  • a steam boiler for heating water to high pressure steam
  • a high-pressure sub-cylinder connected to a steam boiler through a pipe;
  • a particle energy reaction kettle comprising a tank body and the composite material filled in the tank body, the tank body is provided with a steam inlet and a steam outlet, and the steam inlet is connected to the high pressure sub-cylinder through the pipeline;
  • the vacuum heat exchanger comprises a tank body and the composite material filled in the tank body, wherein the tank body is provided with a steam inlet communicating with the steam outlet of the particle energy reaction kettle through the pipeline, and the steam outlet of the tank top is connected to the steam boiler through the pipeline , the bottom of the tank is provided with a water outlet;
  • An interactive particle energy water purification reactor comprising a can body and the composite material filled in the can body, the tank body being provided with a water input port and a water outlet, the water inlet port passing through the pipe and the vacuum heat exchanger The water outlet is connected.
  • the particle energy reactor comprises:
  • a tank body having a steam inlet and a steam outlet at the top of the tank;
  • a support net which is a mesh structure having the same shape as the cross section of the tank, is disposed at a lower portion of the tank body, and partitions the interior of the tank body into an upper loading area and a lower venting area;
  • the blocking portion is composed of an integrally formed vertical blocking plate and a horizontal blocking plate.
  • the upper bottom edge of the vertical blocking plate is integrally formed with the horizontal blocking plate, the two sides of the vertical blocking plate are attached to the tank wall, and the bottom edge is erected on the support net;
  • One side of the blocking plate is integrally formed with the vertical blocking plate, and the other side is attached to the tank wall; thus, the blocking portion divides the upper loading area in the tank into the air inlet area and the bypass area, wherein the steam inlet is correspondingly arranged on the tank body Position in the intake area;
  • the composite material is filled with a filling area.
  • the tank body is provided with two steam inlets, the upper steam inlet corresponding to the top of the inlet zone, and the lower steam inlet corresponding to the bottom of the inlet zone.
  • the vacuum heat exchanger includes:
  • a tank body a steam outlet at the top of the tank, a water outlet at the bottom of the tank, and a steam inlet at the tank body;
  • the first support net is a mesh structure having the same shape as the cross section of the can body, and is disposed at a lower portion of the can body.
  • the first support net is filled with the spherical composite material to form a first heat exchange area, and the steam inlet corresponds to Located below the first support net;
  • the second support net is a mesh structure having the same shape as the cross section of the can body, and is erected on the upper part of the can body, and the first support net is filled with the sheet-shaped composite material to form a second heat exchange area;
  • a filtration device is provided on the conduit connecting the vacuum heat exchanger and the interactive particle energy water purification reactor.
  • the apparatus comprises a plurality of the vacuum heat exchangers, wherein the steam inlets of the vacuum heat exchangers are respectively connected to the steam outlets of the particle energy reactor, and the steam outlets of the vacuum heat exchangers are respectively connected to the steam boiler The entrance is connected.
  • the apparatus comprises a plurality of said interactive particle energy water purification reactors connected in series by a conduit.
  • the conduit to which the water outlet of the interactive particle energy water purification reactor is connected is provided with a filtering device.
  • the invention also provides a method for preparing a particle capable multifunctional active water, comprising:
  • the steam in contact with the composite material, and the temperature of the steam in the reactor can be maintained at 150-190 ° C;
  • the water outputted by the vacuum heat exchanger enters the interactive particle energy water purification reactor, and heat exchange is performed after contact with the composite material until the water temperature is lower than 60 ° C, and then output and filtered to obtain particles capable of multifunctional active water.
  • the temperature of the steam in the step 1) and the step 2) is 145 to 155 °C.
  • the present invention provides the particle-multifunctional active water prepared by the above method.
  • the inventive preparation of the present invention obtains a multi-functional active water of particles, and the structure thereof is less than that of small molecule water, and the specific gravity is 1.002 to 1.004 g/cm 3 at normal temperature.
  • the particles prepared by the invention can be multi-functional active water as sterile water.
  • the particles prepared by the invention have the stability and activity of the multifunctional active water far exceeding the small molecular group water, and the shelf life is long.
  • the bottled water has three years, and the diameter, the decomposition force, the penetrating power and the active force have not changed. And still sterile water.
  • the particles prepared by the invention can be used for food, health care, medicine, biology, environment, disease control, agriculture, military, machinery, energy, daily life, etc. due to their special activities and energy effects.
  • Various industries can be used for food, health care, medicine, biology, environment, disease control, agriculture, military, machinery, energy, daily life, etc. due to their special activities and energy effects.
  • FIG. 1 is a schematic view showing the structure of a device for preparing particles capable of multifunctional active water according to the present invention.
  • FIG. 2 is a schematic view showing the structure of a particle energy reactor in the apparatus for preparing a particle-multifunctional active water of the present invention.
  • Fig. 3 is a schematic view showing the structure of a vacuum heat exchanger in the apparatus for preparing a particle-multifunctional active water of the present invention.
  • FIG. 4 is a schematic view showing the structure of a transfer type particle energy water purification reactor in the apparatus for preparing a particle capable multifunctional active water of the present invention.
  • the composite material of the present invention for preparing particles capable of multifunctional active water contains the following components: Si, Re, Pt, Ge, Nb, Ni, Se and Mg.
  • the composite was prepared by the following method:
  • step 2) The mixture obtained in the step 1) is placed in a magnetizing furnace for magnetization, the magnetization is 5-10 A/m, and the magnetization is 100-200 h;
  • step 2) placing the magnetized material in step 2) in a molding die and vacuum sintering;
  • the material obtained in the step 3) is placed in a magnetizing furnace for magnetization, the magnetization is 80-100 A/m, and the magnetization is 100-300 h to obtain the composite material.
  • the composite material can be formed into, but not limited to, the following shapes:
  • the particle can be spherical material, 6-10 mm in diameter, solid spherical;
  • Particle energy egg-shaped ball material maximum diameter 43-82 mm, hollow, wall thickness 2-3 mm, open at one end;
  • the particle can be a disk-shaped material with a diameter of 30-120 mm and a thickness of 2-5 mm;
  • the particle can be a cube or a rectangular parallelepiped sheet material with a size of 40 ⁇ 60 to 200 ⁇ 220 mm and a thickness of 2-5 mm.
  • the above composite material for preparing a particle capable multifunctional active water comprises the following steps:
  • the steam in contact with the composite material, and the temperature of the steam in the reactor can be maintained at 150-190 ° C;
  • the water outputted by the vacuum heat exchanger enters the interactive particle energy water purification reactor, and heat exchange is performed after contact with the composite material until the water temperature is lower than 60 ° C, and then output and filtered to obtain particles capable of multifunctional active water.
  • the invention has found through a large number of experiments that the basic particle energy generated by the composite material can play a vital role in water, so that the macromolecular water can form a stable and special energy after contacting the composite material under specific conditions.
  • Small molecule water The principle is presumed as follows: the energy particles (ie, the composite material of the present invention) exerts the action of particle energy in the device, and the potential energy generated by the various particles inside the proton when the axial rotation motion changes the structure of the water molecules, so that the structure of the water molecules is changed. Single water molecule can be stable The presence. Since the structure of the water molecule is changed and the association force is lost, the macromolecular water is not recombined at normal temperature. (The prepared particles can be multi-functional active water, even if the water is repeatedly heated to 100 ° C or low temperature to -40 ° C frozen, it will not re-associate the macromolecular water)
  • the multi-functional water of the particles may pair the protons and neutrons inside the nucleus of the water molecule to a stable state, thereby maintaining the activity of the water molecules and having magnetic properties.
  • a single water molecule capable of multi-functional water based on the water molecule's basic structure H 2 O, with a hydrogen atom radius of 79 pm and an oxygen atom radius of 70 pm.
  • the hydrogen nucleus and the nucleus The bonding pitch was 96 pm, and the outer electron spacing of the hydrogen atom and the oxygen atom was 240 pm at room temperature.
  • a single water molecule can maintain a stable single molecule state for a long time at room temperature.
  • the particles thus produced can reduce the viscosity of the multifunctional water, and the solubility, permeability, and dispersibility can be improved, and the activity can be enhanced without being attenuated.
  • the composite material for preparing the particle-multifunctional active water of the present embodiment is formed by combining silicon nanoparticle particles as a substrate and mixing other seven nano-sized particles.
  • This nanoscale material has an average length of 1-2 nanometers.
  • the above-mentioned nano-sized particles of silicon, germanium, platinum, rhodium, ruthenium, nickel, selenium and magnesium are mixed in a vacuum environment, and after the materials are mixed, the particle energy magnetization is carried out in the magnetization furnace, and the magnetization during the magnetization process should reach 7 A/ m, and maintain the magnetization of 123.25h.
  • low-temperature transformation sintering was performed, and the material was placed in a molding die to be sintered at 823.7 ° C for 1.7 h, and then sintered at a constant temperature of 920 ° for 12 h. After sintering, it was magnetized again, and the magnetization was 97 A/m, and the magnetization was continued at room temperature for 235.5 hours.
  • the composite is shaped into the following shapes:
  • the particle can be a spherical material, 6-10 mm in diameter, solid spherical or hollow spherical;
  • the particles can open the egg-shaped ball material, the maximum diameter is 43-82 mm, hollow, and the wall thickness is 2-3 mm;
  • the particle can be a disk-shaped material with a diameter of 30-120 mm and a thickness of 2-5 mm;
  • the particle can be a cube or a rectangular parallelepiped sheet material with a size of 40 ⁇ 60 to 200 ⁇ 220 mm and a thickness of 2-5 mm.
  • the apparatus for preparing a particle capable multifunctional active water comprises:
  • the high-pressure partial cylinder 2 is connected to the steam boiler 1 through a pipe.
  • the particle energy reactor 3 (shown in Figure 2) includes:
  • the tank body 30 is provided with a steam inlet 301, the tank top is provided with a steam outlet 302, and the steam inlet 302 is connected to the high pressure sub-cylinder through a pipeline;
  • the support net 31 is a mesh structure having the same shape as the cross section of the can body 30, and is disposed at a lower portion of the can body 30 to partition the inside of the can body 30 into an upper loading area and a lower venting area;
  • the blocking portion 32 is composed of an integrally formed vertical blocking plate 321 and a horizontal blocking plate 322.
  • the upper bottom edge of the vertical blocking plate 321 is integrally formed with the horizontal blocking plate 322, and the sides of the vertical blocking plate 321 are adhered to the can wall to vertically block
  • the bottom edge of the plate 321 is erected on the support net 31; one side of the horizontal blocking plate 322 is integrally formed with the vertical blocking plate 321 and the other side is fitted to the tank wall; thus, the blocking portion 32 separates the upper loading area of the tank into the intake air.
  • a zone and a bypass zone wherein the steam inlet 301 is correspondingly disposed at the location of the inlet zone on the can body.
  • the canister is provided with two steam inlets 301, and the upper steam inlets are correspondingly located at the intake At the top of the zone, the lower steam inlet corresponds to the bottom of the intake zone;
  • a spherical or open eggshell composite that is packaged in a wire mesh pocket and filled with a filling area.
  • the vacuum heat exchanger 4 (shown in Figure 3) includes:
  • the tank body 40 is provided with a steam outlet 402 communicating with the steam boiler 1 through a pipeline, and the tank bottom is provided with a water outlet port 403, and the tank body is provided with a steam inlet 401 communicating with the steam outlet 302 of the particle energy reaction kettle through a pipeline;
  • the first support net 41 is a mesh structure having the same shape as the cross section of the can body, and is placed on the lower part of the can body.
  • the first support net 41 is filled with a spherical or open eggshell composite material (the composite material is encapsulated in the wire mesh pocket). Medium and rear loading), constituting a first heat exchange area, wherein the steam inlet is correspondingly disposed below the first support net;
  • the second support net 42 is a mesh structure having the same shape as the cross section of the can body, and is erected on the upper part of the can body.
  • the first support net is filled with a sheet-like composite material to form a second heat exchange area;
  • the apparatus includes a plurality of the vacuum heat exchangers 4, and the steam inlets 401 of the vacuum heat exchangers are respectively connected to the steam outlets 302 of the particle energy reactor, and each vacuum heat exchange The steam outlets 402 are in communication with the inlets of the steam boilers, respectively.
  • the interactive particle energy water purification reactor 5 includes a can body 50, a support net 51, and a composite material on the loading support net (which may not need to be filled), and the can body is provided with a water input port 501 and a setting. There is a water outlet 502 through which the water inlet 501 communicates with the water outlet 403 of the vacuum heat exchanger 4. As shown in Figure 1, the apparatus includes a plurality of said interactive particle energy water purification reactors 5 connected in series by a conduit.
  • a filter device 6 is provided on the pipe connecting the vacuum heat exchanger 4 and the interactive particle energy water purification reactor 5.
  • the present embodiment uses the above device to prepare a particle capable multifunctional active water, comprising:
  • the water is introduced into the steam boiler 1 through the pipeline, and the steam is heated to generate steam of 145-155 ° C, and the steam is supplied to the reactor 3 through the high-pressure partial cylinder 2 .
  • the selection of water high-quality river water, lake water, reservoir water can be used, and groundwater should be selected from non-limestone formations. Tap water can also be used after removing the scavenger.
  • the cited external water is filtered and stored for later use.
  • the particle energy reactor 3 steam is contacted with the composite material, and the temperature of the vapor in the reactor 3 is maintained at 145-155 °C.
  • the input high-temperature steam needs to pass through the cyclic thermal potential energy reaction of the particle energy reactor 3, and at a high temperature, the particle energy core material can perform high-magnetization of the vapor, that is, the high-temperature and high-pressure particle energy potential energy is used to change the vapor state.
  • the particle energy reactor has vacuum magnetization, which can stabilize the energy of the particles in the preparation process of the multi-functional water.
  • the structure of the water molecules changes, and the magnetic field of this strength can be maintained to achieve the magnetic field density required for the molecular separation process.
  • the water molecules magnetized by the potential energy of the particles enter the vacuum heat exchanger in a gaseous form.
  • the particle-reactive reactor 3 the magnetized vapor is supplied to the vacuum heat exchanger 4, and exchanges heat between the upper and lower particle energy fields.
  • the vapor is separated from the formed by the vacuum heat exchanger 4.
  • the magnetized well formed monomolecular water is split downward and fed into the interactive particle energy water purification reactor 5.
  • the gaseous water molecules (vapors), which are still in a vapor state and are not completely stable, are sent back to the steam boiler 1 through the pipeline for reheating.
  • the vacuum heat exchanger 4 performs a thermal interaction between water and steam through a vacuum exchange process, and achieves uniform distribution of water molecules under the action of particle energy potential energy.
  • the particles produced by the vacuum heat exchanger 4 can be multi-functionally active water and sent to the interactive particle energy water purification reactor 5.
  • This process is mainly to convert the temperature of water from high temperature to normal temperature water. The heat in the water is gradually dissipated through the water tank, and after less than 60 degrees Celsius, the water is initially filtered. The initially filtered water is transported to the storage tank, and after the water is cooled, it is subjected to fine filtration after normal temperature, and is then stored in the water tank of the finished water through the finely filtered water.
  • the interactive particle energy water purification reactor 5 sends the formed multi-function water from the vacuum heat exchanger to the apparatus, and the water gradually passes from the high temperature to the normal temperature. In this process, the structure of the water is stabilized at a certain low magnetic field strength, and the purification reaction is exchanged.
  • the composition of the multi-functional active water of the particles exhibits irregularly arranged small molecular clusters with a diameter of less than 1 nm, which is smaller than the existing small molecular water (composed of more than 10 water molecules).
  • the water molecule group is called macromolecular water, and its diameter is larger than 2.6 nm; the molecular water composed of 5-7 water molecules is called small molecule water, and its diameter is between 1.1 and 1.6 nm).
  • the particles Under the electron tunnel scanning microscope, the particles can be arranged in a single water molecule. Note: The resolution of a transmission electron microscope (ST) is one millionth of a millimeter, and the resolution of an electron tunneling microscope (STM) is one hundred millionth of a millimeter.
  • the particles prepared in the present embodiment can be multi-functional active water as completely sterile water, which is currently unachievable by the existing small molecule water.
  • Detection method Accurately measure 1m 3 of particles with multifunctional active water and weigh.
  • the particle capable multifunctional active water of the invention is sent to the Analytical Testing Research Center of the Beijing Institute of Geology of the nuclear industry for testing.
  • Test Method 1 DZ/T 0064, 80-1993 ⁇ Groundwater Test Method Plasma Mass Spectrometry for Determination of 39 Elements Such as Lithium>, Instrument Model: ELEMENT XR Plasma Mass Spectrometer
  • Test Method 2 DZ/T 0184-19-1997 "Determination of Hydrogen Isotope Zinc Reduction Method in Water", DZ/T 0184-21-1997 “Determination of Oxygen Isotope Carbon Dioxide-Water Balance Method in Natural Water”. Instrument model: MAT 253. The test results are as follows:
  • the particles of the present invention are capable of multifunctional active water and do not contain radioactive elements. This is not radioactive.
  • the particles prepared in this embodiment can be heated to 100 degrees by the multifunctional active water, and the functional characteristics and activities of the multifunctional active water of the particles are not changed, and the particles can be reduced to ordinary water by the multi-functional active water association. After 3 years of standing, it was verified by activity experiments that there was no deterioration in its activity.
  • the long-term storage property of the particles of the present invention can be kept unchanged by long-term storage, and it is speculated that it may be related to the activity characteristics of the multifunctional active water of the particles. Since the particles can be used as a multifunctional active water without a radioactive source, there is no radioactivity. There is no clear conclusion that the active energy source of the particles can be stored for a long time without any attenuation. Judging from the production process and other aspects, the active source of particles capable of multifunctional active water may be magnetic. A few small experiments are as follows:
  • the particles prepared in the present embodiment can be filled with a multifunctional active water into a glass, plastic or aluminum container (500 g container), and the beer or white wine or cigarette is placed on the side of the container, and the energy released by the water can be worn. After two hours of translucent packaging, the taste of the wine and the smoke changed significantly, and the taste was significantly improved.
  • the particles can be multi-functional active water people lying on the top for 30 to 45 minutes, the fatigue is eliminated; the cervical vertebrae pain only needs to be able to multi-function the particles of a plastic bottle before going to bed.
  • the water was placed under the neck, and the pain was significantly reduced or even disappeared after 2 hours.
  • the nuclear magnetic resonance is 48--50 Hz.
  • the molecular group water existing in the natural state the water molecule group composed of more than 10 water molecules is called macromolecular water, and its diameter is larger than 2.6 nm; the molecular water composed of 5-7 water molecules is called Small molecule water with a diameter between 1.1 and 1.6 nm.
  • the particle can be a single water molecule of multifunctional water.
  • the outer electron spacing of the hydrogen atom and the oxygen atom is 240 pm at room temperature and 390 pm in vapor state. Therefore, the particles can be multi-functional water, can directly enter each cell and red blood cells through the cell water channel; can meet the quantity of water molecules and growth factors required by each nucleus of the human body; can improve the body due to excessive water molecules Cell metabolism function.
  • German scientists discovered that there is a water channel on the human cell membrane that allows water and ionized nutrients to pass through the cell. It is called a cell water channel.
  • the small molecule water is easily passed through the cell membrane under the action of human body electrostatic force.
  • the water channel, and the water molecule group composed of more than 10 water molecules, is difficult to enter the interior of the cell.
  • the human cell's cellular water channel is a hexagonal channel surrounded by six protein subunits, in protein Under the action of electrostatic force, water molecules enter the cells one by one through the channel, perform hydration, and absorb and repel nutrients and metabolites.
  • the academic community has confirmed that water is the medium needed for human cells to absorb nutrients and physiological activities, while the water channel of the cell wall runs through, not a closed shell.
  • the academic community believes that the cause of atrophy and depletion of human cells is caused by "the body cells are blocked by water exchange.”
  • the particles prepared by the invention can be multi-functional water, which can easily enter the interior of the cell, thereby restoring the original functions of the human cells, promoting cell growth and antibacterial and antiviral effects.
  • the micro-mineral elements and trace metal elements contained in the multi-functional active water of the particles reach the ionic state, and the harmful substances are extremely low in content and sterilized, reaching the level of pure water, and can be applied to medical treatment. It is administered to a patient by intravenous drip, which can decompose and excrete blood lipids, blood sugar and other deposited substances in the blood, and the cells and genes are also repaired to some extent.
  • the trial was conducted by a 30-year-old woman with advanced breast cancer.
  • the trial method was as follows: the cancer treatment drug and the particle energy multifunctional active water were prepared as intravenous drip, and the patient was treated with intravenous drip.
  • the patients were genetically tested at any time during the treatment.
  • the results were as follows: Initially, the immunologically active genes CD4, PRF1 and the antioxidant capacity gene SOD-2 and the toxicant metabolic enzyme gene CYP1A2 were abnormally expressed. With the treatment, some gene expressions have returned to normal, SOD The -2 gene is also in recovery. It can be seen from the results of genetic testing that the patient's condition has been significantly improved.
  • the tester is a 40-year-old cancer patient, which is used by dissolving an anticancer drug in the particle-multifunctional active water of the present invention and intravenously instilling it. After 6 months of treatment, cancer cells were not detected after examination.
  • the trial is for hypertensive patients over 50 years old.
  • the trial method is intravenous drip, and the test dose is 250mL per day. After continuous infusion for 6 days, the amount was increased to 500 mL per day, and the blood pressure returned to normal after 9 to 10 days.
  • the trial was performed on a hypotensive patient.
  • the test dose was 500 mL per day for the intravenous infusion. There was no adverse reaction during the instillation. After several days of continuous infusion, the blood pressure returned to normal.
  • the patient was tested for allergic symptoms.
  • the trial method was intravenous drip. After the first day of instillation, the allergic symptoms were aggravated. The next day, allergic symptoms improved and alleviated. After 9 days of continuous infusion, allergic symptoms disappeared.
  • the multi-functional active water of the particles has a very obvious effect on softening and relieving cardiovascular and cerebrovascular diseases.
  • the blood viscosity of patients with cardiovascular and cerebrovascular diseases is greatly reduced, the obstructive state is obviously improved, and blood lipids are improved.
  • the sediment is decomposed and excreted through the urethra.
  • Cardiac premature beats trials of male premature beats in men, intravenous infusion of 500mL per day.
  • the second bottle was instilled, the symptoms of premature beats were alleviated.
  • the symptoms of premature beats have not occurred.
  • this patient has severe insomnia.
  • After instilling the fourth bottle he no longer loses sleep, and his calcified tuberculosis block many years ago has a narrow shadow on the lung after instillation treatment.
  • one person's urine is light blue (it works in lead-zinc mines, which may be lead and zinc exceeded), and one person's urine is light green (working in copper mines, which may be excessive copper).
  • the urine discharged by the diabetics has a yellowish appearance, some cola colors, but all have foam. After the instillation of the drug user, the urine is colored like soy sauce.
  • the multi-functional active water of the present invention has the above-mentioned principle: the particles can be multifunctional active water itself, and have no therapeutic effect on human diseases.
  • the remarkable effect after instillation is that this kind of water can act on genes in human cells and nucleus; it can input various proteins and substances required by cells into cells, repair and survive cell and cell tissues, Freshmen provide a material basis. Therefore, the original function of the human body is activated, and the function of the human body itself is restored.
  • the particles can multi-function water, in addition to the body's atrophy, diseased cell tissue, gene repair, but also metabolism of impurities and sediments in the blood.
  • the particles can be multi-functional water, which not only has good repair and growth promotion effects on human cells, but also has very good antibacterial and antiviral effects, and can decompose and remove germs and aging in the body and blood. Cells and sediments.
  • the multi-functional active water of particles can also be used for oral drinking and daily health care, which can gradually restore the original functions of human cells, promote cell growth and antibacterial and antiviral effects; the particles can not change the quality of the active water, and the function will not be caused by It lasts for a long time and decays.
  • eye function defects you can directly use the particles can be multi-functional active water drops, several times a day, drop again before going to bed.
  • the multi-functional active water of the particles can gradually repair the eye cells and restore the original function of the eye. No need to add any drugs. Usage, use a 10 or 20 ml syringe to inject water into the empty eye vial for instillation.
  • each particle contains multi-functional active water for half a time, 5 seconds, brushing teeth for 20-30 seconds, (ordinary toothpaste) slightly longer Better, it can immediately remove tartar and yellow tongue.
  • the use of particles can be multi-functional active water rubbing, the effect is obvious, if the particles can be multi-functional active water with a better effect.
  • For athletes with athlete's foot just use a few drops of multi-functional active water to clean the affected area, and immediately relieve itching. After one or two days, the athlete's foot will heal. Body odor, just spray or rub the particles with multifunctional active water Your armpit can stop the stench immediately.
  • the functional water can be heated into the hot water bottle, the temperature can be appropriate, placed at the cervical vertebra before going to bed. After that, the hot water bottle is placed in a pot and heated and reused with hot water. Women with dysmenorrhea can also use this method, put the hot water bottle on the lower abdomen. Do not mix functional water with other water. The water in the hot water bottle should not be drunk, but it can be used repeatedly for a long time.
  • the particle can be multi-functional active water also has the function of hangover, drink the particles can be multi-functional active water 150-200 ml after drunkenness, drink it and feel, about 15-20 minutes to wake up. After drinking the particles, the multi-functional active water will not feel any discomfort even if it has no alcohol.
  • the multi-functional active water of the particles has an excellent effect on the wine. Before drinking any white wine, it can be shaken by shaking with 3-5 grams of multifunctional active water (per bottle), and the particles can be multi-functional active water after 5 minutes. The liquor will become very mellow and sweet. The fake wine can be mixed with particles to be multi-functional active water, and the taste is bitter.
  • the original wine is as above. Two bottles of multi-functional active water can be used to sandwich a bottle of white wine. After 12 hours, the wine can also be mellow. The same is true for beer and wine.
  • the menstrual discomfort one can be heated by the particles of multi-functional active water, two particles can be multi-functional active water into the hot water bottle, the hot water is poured into the basin before use, the water bag is hot, placed Above the lower abdomen, it can significantly relieve dysmenorrhea.
  • the ability of particles can be multi-functional active water on burns, red wounds, burns than the existing drugs (users say), patients, only need to spray a small amount of multi-functional active water particles in the affected area, multiple times a day
  • the particles can multi-functional active water has a very good role in promoting cell growth; such as scratches, wounds, the use of particles can be used to wash the wound with multi-functional active water can immediately relieve pain, can be wrapped after washing. Due to the multi-functional active water of particles, it has an antibacterial effect.
  • the particles can be sterilized in multi-functional active water, see; China CDC test report.
  • particle energy water and photon have physical and chemical characteristics, the two can convert each other's energy, so the particles can have a good sun protection effect. But storage should be protected from light.
  • the other two distinguishing features of the multi-functional active water of the particles are: First, the storage will not deteriorate for a long time. Second, the function will not be attenuated due to long storage time.
  • the multi-functional active water of particles can be mainly in the form of intravenous drip in detoxification treatment.
  • the mechanism of action is generally that a single stable water molecule directly acts on different regions of the body through the blood circulation of the human body and directly enters the cells in the region, so the particles can be multifunctional.
  • Active water activates cells in the nervous system, promotes metabolic functions of cell damage, stimulates the self-metabolism of nerve cells, repairs irreversible brain cell damage, and restores normal brain function damage caused by drug use. Achieve drug treatment.
  • the main manifestations are the repair of receptors and neurotransmitters in the midbrain-edge dopamine system (nucleus accumbens, hippocampus, prefrontal cortex, ventral tegmental area, amygdala, etc.).
  • the symptoms of the brain reward system formed by drug abuse are alleviated, Under the reward mechanism, the recovery of addictive brain function caused by exogenous drug dependence achieves the purpose of detoxification.
  • Intravenous infusion of particles can be a clinical manifestation of dopaminergic nerve recovery caused by long-term drug abuse by drug users, so that drug users can achieve normal brain reward mechanism and return the normal amount of excitement and pleasure to dopamine.
  • dopamine tolerance caused by long-term drug use.
  • the accumulation of dopamine in the prominent posterior membrane was removed, and the excitatory symptoms of brain function beyond the normal range due to drug use were significantly alleviated.
  • the dopamine system achieves functional degradation under the action of multi-functional active water, and the enhanced activity of midbrain dopamine and serotonin transduction activity, thereby alleviating the aversion of the drug addicts during the withdrawal phase.
  • Anxiety
  • the multi-functional active water of particles can not only promote the growth of animal cells, but also the effect on plant cells.
  • the rapeseed After being immersed in the multi-functional active water, the rapeseed can not only grow faster after seeding, but also about twice as high as the growth height of rapeseed without soaking the seeds.
  • the potatoes were immersed for 12 hours after dicing, and grown to a height of 350 mm after only 13 days after sowing.
  • the particle can be multi-functional active water spray, which can more than double the flowering period.
  • the above-mentioned nano-sized particles of silicon, germanium, platinum, rhodium, ruthenium, nickel, selenium and magnesium are mixed in a vacuum environment, and after the materials are mixed, the particle energy magnetization is carried out in the magnetization furnace, and the magnetization during magnetization should reach 10 A/ m, and maintain the magnetization for 150h.
  • low-temperature transformation sintering was performed, and the material was placed in a molding die and sintered at 850 ° C for 2.1 h, and then sintered at a constant temperature of 950 ° for 12 h. After sintering, the magnetization was again performed, and the magnetization was 95 A/m, and the magnetization was continued at room temperature for 245.1 hours.
  • the composition of the particles capable of multifunctional active water of the present embodiment exhibits an irregular arrangement of small molecular clusters having a diameter of less than 1 nm, which is smaller than the existing small molecule water (by more than 10 waters).
  • Water molecule group It is called macromolecular water, and its diameter is larger than 2.6nm; the molecular water composed of 5-7 water molecules is called small molecule water, and its diameter is between 1.1-1.6nm).
  • the particles Under the electron tunnel scanning microscope, the particles can be arranged in a single water molecule. Note: The resolution of a transmission electron microscope (ST) is one millionth of a millimeter, and the resolution of an electron tunneling microscope (STM) is one hundred millionth of a millimeter.
  • the content of various minerals and ions in the multi-functional active water of the particles is far lower than the national standard, and basically belongs to the pure water category.
  • the multi-functional active water of the particles of the present embodiment contains only a small number of colonies and reaches the national standard, which is currently unachievable by the existing small molecule water.
  • Detection method Accurately measure 1m 3 of particles with multifunctional active water and weigh.
  • the particles prepared in this embodiment can be heated to 100 degrees by the multifunctional active water, and the functional characteristics and activities of the multifunctional active water of the particles are not changed, and the particles can be reduced to ordinary water by the multi-functional active water association. After 3 years of standing, it was verified by activity experiments that there was no deterioration in its activity.
  • the particles prepared in the present embodiment can be filled with a multifunctional active water into a glass, plastic, or aluminum container (500 g container), and the beer or white wine or cigarette is placed on the side of the container. After two hours, the wine and the smoke are The taste changed significantly and the taste was significantly improved. Particles can be used to penetrate the package to other objects. The energy action principle and energy source can not give a clear conclusion.
  • the particles can be multi-functional active water people lying on the top for 30 to 45 minutes, the fatigue is eliminated; the cervical vertebrae pain only needs to be able to multi-function the particles of a plastic bottle before going to bed.
  • the water is placed under the neck, and the pain is noticeable after 4-5 hours. Reduce or even disappear.
  • the NMR is 48-50 Hz.
  • the method for treating cancer, hypertension, hypotension, allergies, premature cardiac contracting, and the like and the daily health care of the particles which can be prepared by the present embodiment are the same as those of the first embodiment Relief and treatment effects.
  • the above-mentioned nano-sized particles of silicon, germanium, platinum, rhodium, ruthenium, nickel, selenium and magnesium are mixed in a vacuum environment, and after the materials are mixed, the particle energy magnetization is carried out in the magnetization furnace, and the magnetization during magnetization should reach 10 A/ m, and maintain the magnetization for 150h.
  • low-temperature transformation sintering was performed, and the material was placed in a molding die and sintered at 850 ° C for 2.1 h, and then sintered at a constant temperature of 950 ° for 12 h. After sintering, the magnetization was again performed, and the magnetization was 95 A/m, and the magnetization was continued at room temperature for 245.1 hours.
  • the composition of the multi-functional active water of the present embodiment exhibits an irregular arrangement of small molecules with a diameter of less than 1 nm, which is smaller than the existing small molecular water (by more than 10 water molecules).
  • the polymolecular group of water molecules is called macromolecular water, and its diameter is larger than 2.6 nm; the molecular water composed of 5-7 water molecules is called small molecule water, and its diameter is between 1.1 and 1.6 nm).
  • the particles Under the electron tunnel scanning microscope, the particles can be arranged in a single water molecule. Note: The resolution of a transmission electron microscope (ST) is one millionth of a millimeter, and the resolution of an electron tunneling microscope (STM) is one hundred millionth of a millimeter.
  • the content of various minerals and ions in the multi-functional active water of the particles is far lower than the national standard, and basically belongs to the pure water category.
  • the multi-functional active water of the particles of the present embodiment contains only a small amount of microbial colonies, which fully meets the national standard, which is currently unachievable by the existing small molecule water.
  • Detection method Accurately measure 1m 3 of particles with multifunctional active water and weigh.
  • the particles prepared in this embodiment can be heated to 100 degrees by the multifunctional active water, and the functional characteristics and activities of the multifunctional active water of the particles are not changed, and the particles can be reduced to ordinary water by the multifunctional active water.
  • the particles prepared in the present embodiment can be filled with a multifunctional active water into a glass, plastic, or aluminum container (500 g container), and the beer or white wine or cigarette is placed on the side of the container. Two hours later, the wine and the smoke The taste has changed significantly, and its taste has improved significantly.
  • the particles can be multi-functional active water people lying on the top for 30 to 45 minutes, the fatigue is eliminated; the cervical vertebrae pain only needs to be able to multi-function the particles of a plastic bottle before going to bed.
  • the water was placed under the neck, and the pain was significantly reduced or even disappeared after 2 hours.
  • the NMR is 48-50 Hz.
  • the method for treating cancer, hypertension, hypotension, allergies, premature cardiac contracting, and the like and the daily health care of the particles which can be prepared by the present embodiment are the same as those of the first embodiment Relief and treatment effects.

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Abstract

一种用于制备粒子能多功能活性水的复合材料、制备方法及装置。该复合材料含有如下成分：Si，Re，Pt，Ge，Nb，Ni，Se和Mg。该复合材料由上述成分的纳米颗粒经磁化、烧结和再磁化制成。该复合材料在本发明的装置中与水接触作用后，将水转化为粒子能多功能活性水。本发明的粒子能多功能活性水，小于小分子团水，在常温下，比重为1.002～1.004g/cm 3，为无菌水，其稳定性、活性远超小分子团水，且保质期长，瓶装水三年，其直径、分解力、渗透力、活性力未发生任何变化，且仍为无菌水。粒子能多功能活性水可用于食品、保健、医药、生物、环境、疾控、农业、军工、机械、能源、日常生活等等各行各业。

Description

制备粒子能多功能活性水的复合材料、制备方法及装置 技术领域
本发明涉及一种用于制备粒子能多功能活性水的复合材料、制备方法及装置。
背景技术
一、自然状态下的水
在现实生活中，水是人们再熟悉不过的基础物质，每一天我们都离不开水。离开了水，所有生物都将灭绝。人们知道如何使用水，也知道水是人类生存不可缺少的资源。水分子的基本结构是H2O，由一个氧原子和两个氢原子组成。在自然界，水分子的种类约有1300多个，多数水分子在自然界中十分少见，常见的水分子不超过20个，其中约一半的水分子，在自然界存在的时间约12年左右，另一半则是永恒之水。水是怎样形成的？学界多数权威认为水是大爆炸后的产物。大爆炸产生了大量的氢氧原子，后由氢氧原子键合而产生了水。单个水分子是以三个原子成104.52度角的三角形存在。水在自然状态下，是由10个以上的水分子抱团聚成的，在学术上称之为“大分子团水”。水为什么会抱团存在？在理论上认为是水的退化和污染造成的。水被长期污染后，使水分子的结构发生变化，由小分子团水变成排列无序的大分子团水，造成水的溶解力、渗透力、扩散力下降退化。故，自然状态存在的水，为大分子团水。水中含有的各种微量元素，是水被长期矿化的结果。
学界研究发现，水分子呈角分布，而非线性分布，是因氧的一侧带负电，氢的一侧带正电，在负电荷周围正电荷并不均匀分布，作用不能相互抵消，水分子的正极吸引邻近的负极，从而使水分子黏在一起，形成大分子团水。
二、大分子团水的成因
已知，水在常温时因正负电荷的不均衡作用，水分子聚成大分子团。水会形成大分子团是水分子缔合的一种物理过程，反之是离解。缔合是放热过程，离解是吸热过程。当水温升高，水的缔合程度降低，大分子团水随着水温度的升高而离解，将水加温到100度时，因温度作用使水分子有足够的能量克服氢键的强作用力而分开。当温度高于100度C时水呈气态，水分子主要由单分子组成。水分子的氢氧原子之间的共价键，是通过分享一对电子形成的，水的一对电子的共享程度不均衡，氧比氢更需要电子。在氢氧键合时，主要是因氢键的强作用力，使水分子成团状存在。故，水被加温到100度时克服了电荷的作用力，水分子被分开。(水在加热过程时电导力逐渐下降，加热到100度时基本不导电。)大分子团水在温度的作用下，虽然能够被离解成单分子状态，但随着温度的降低水分子又逐渐缔合聚成——大分子团水。如何能够使水分子在常温状态下不再缔合，是基本物质学界研究的重要课题之一。
三、离解成单分子水的可能性
学界认为自然界的水，以大分子团状态存在，是因水的退化和污染所致，将水分子从大分子团分开，认为是离解、还原水的最初形态。所以，众多基本物质学者长期致力于这方面的研 究。发达国家先后开发出了磁化水，(1945年比利时)；电解离子水，(1999年日本京都大学)；反渗透膜净化水，(1977年美国陶氏化学)。磁化水、电解离子水，利用磁化、电解技术将大分子团水离解成小分子团水；反渗透膜净化水，则是将磁力与压力反作用于渗透膜，释放过氢氧原子，同样也得到了小分子团水。在常温状态下，这种小分子团水又逐渐的聚集缔合成大分子团水，一般情况下其保持小分子状态的时间，在72小时以内，密封状态下可达15天，在温度作用下会立即缔合成大分子团水。这说明其稳定性与活性存在缺陷。
在自然界中，因地球表面的磁场强度不同，所呈现的物质结构也是不同的。在地球的一些强磁场地区，发现了一种天然小分子团水。这种小分子团水是由5-7个水分子聚合构成。如中国的广西巴马地区、新疆的昆仑山、俄罗斯的高加索地区就出产这种天然小分子团水。由于人们逐渐认识到小分子团水的广泛应用前景，所以在广西的巴马地区就聚集了十余万人开发利用这种小分子团水。天然小分子团水在封装后会在短时间内重新缔合，但水的保质期，在密封状态下达12-18个月。
技术问题
现有技术无法获得稳定的、具有特殊活性的小分子水。
技术解决方案
本发明首创性地制备得到了一种粒子能多功能活性水，其具有特殊的活性及能量作用，可用于食品、保健、医药、生物、环境、疾控、农业、军工、机械、能源、日常生活等等各行各业。
本发明提供了一种用于制备粒子能多功能活性水的复合材料，其含有如下成分：Si，Re，Pt，Ge，Nb，Ni，Se和Mg。
优选地，所述的复合材料含有的成分及各成分的重量份数如下：
Figure PCTCN2015078758-appb-000001
进一步优选地，所述复合材料由如下重量份数的成分构成：
Figure PCTCN2015078758-appb-000002
Figure PCTCN2015078758-appb-000003
其中，复合材料为球形、中心开有通孔的球形、片状或一端开口的蛋壳形。
本发明还提供了所述的复合材料的制备方法，包括如下步骤：
1)取硅、铼、铂、锗、铌、镍、硒和镁，真空下混合均匀；
2)将步骤1)所得混合物置于磁化炉中实施磁化，磁化强度为5～10A/m，磁化100～200h；
3)将步骤2)磁化后的材料置于成型模具中，真空烧结；
4)步骤3)得到的材料再置于磁化炉中实施磁化，磁化强度为80～100A/m，磁化100～300h，得到所述复合材料。
作为优选技术方案，步骤1)中所述的硅、铼、铂、锗、铌、镍、硒和镁均为纳米级颗粒。
作为优选技术方案，步骤2)中磁化强度为7A/m，磁化时间为120～125h。
优选地，步骤3)中烧结温度为800～1000℃。
进一步优选地，步骤3)中真空烧结为低高温转变烧结：步骤1)磁化后的材料置于成型模具中，真空下，先以800～850℃的温度烧结1～3h，再以900～1000℃的温度烧结10～15h。
作为优选技术方案，步骤4)磁化强度为95～100A/m，磁化时间为200～250h。
本发明还公开了上述的复合材料用于制备粒子能多功能活性水的装置，包括：
蒸汽锅炉，用于将水加热为高压蒸汽；
高压分气缸，通过管道与蒸汽锅炉连接；
粒子能反应釜，包括罐体和装填在罐体内的所述复合材料，罐体设有蒸汽入口和蒸汽出口，蒸汽入口通过管道与高压分气缸连通；
真空式热交换器，包括罐体和装填在罐体内的所述复合材料，罐体设有蒸汽入口通过管道与粒子能反应釜的蒸汽出口连通，罐顶设有蒸汽出口通过管道与蒸汽锅炉连通，罐底设有水输出口；
交互式粒子能量水净化反应器，包括罐体和装填在罐体内的所述复合材料，罐体设有水输入口和水输出口，所述水输入口通过管道与所述真空式热交换器的水输出口连通。
作为优选技术方案，所述粒子能反应釜包括:
罐体，罐身设有蒸汽入口，罐顶设有蒸汽出口；
支撑网，其为一形状与罐体横截面相同的网状结构，架设在罐体内的下部，将罐体内部分隔为上部装填区和下部通气区；
阻挡部，由一体成型的垂直阻挡板和水平阻挡板构成，垂直阻挡板的上底边与水平阻挡板一体成型，垂直阻挡板的两侧边贴合罐壁，底边架设在支撑网上；水平阻挡板的一边与垂直阻挡板一体成型，其余边贴合罐壁；以此，阻挡部将罐体内的上部装填区分隔为进气区和绕行区，其中，蒸汽入口在罐体上对应设于进气区的位置；
所述复合材料，装填满装填区。
优选地，所述罐体设有两个蒸汽入口，上蒸汽入口对应位于进气区的顶部，下蒸汽入口对应位于进气区的底部。
作为优选技术方案，所述真空式热交换器包括：
罐体，罐顶设有蒸汽出口，罐底设有水输出口，罐身设有蒸汽入口；
第一支撑网，为一形状与罐体横截面相同的网状结构，架设在罐体内的下部，第一支撑网上装填球形的所述复合材料，构成第一热交换区，所述蒸汽入口对应设于第一支撑网的下方；
第二支撑网，为一形状与罐体横截面相同的网状结构，架设在罐体内的上部，第一支撑网上装填片状的所述复合材料，构成第二热交换区；
其中，第一热交换区和第二热交换区之间还有无填充的缓冲区。
优选地，连通真空式热交换器和交互式粒子能量水净化反应器的管道上设有过滤装置。
优选地，所述装置包括多个所述真空式热交换器，各真空式热交换器的蒸汽入口分别与粒子能反应釜的蒸汽出口连通，各真空式热交换器的蒸汽出口分别与蒸汽锅炉的入口连通。
优选地，所述装置包括多个所述交互式粒子能量水净化反应器，通过管道串联连通。
优选地，所述交互式粒子能量水净化反应器的水输出口连接的管道设有过滤装置。
本发明还提供上述的装置用于制备粒子能多功能活性水的方法，包括：
1)水经管道引入蒸汽锅炉，加温致生成150-190℃的蒸汽，蒸汽通过高压分气缸输入粒子能反应釜；
2)在粒子能反应釜中，蒸汽与复合材料接触作用，粒子能反应釜中的蒸汽温度保持在150-190℃；
3)蒸汽自粒子能反应釜输出至真空式热交换器，与真空式热交换器中的复合材料接触及热交换后，水经水输出口输出，蒸汽经蒸汽出口回流至蒸汽锅炉；
4)真空式热交换器输出的水进入交互式粒子能量水净化反应器，与所述复合材料接触发生热交换至水温低于60℃后，输出，过滤，得粒子能多功能活性水。
作为优选技术方案，步骤1)和步骤2)中蒸汽的温度为145～155℃。
本发明提供上述方法制备的粒子能多功能活性水。
有益效果
本发明能够达到如下效果：
1、本发明首创性的制备得到了粒子能多功能活性水，经检测，其结构小于小分子团水，在常温下，比重为1.002～1.004g/cm3。
2、经检测，本发明制得的粒子能多功能活性水为无菌水。
3、本发明制得的粒子能多功能活性水的稳定性、活性远超小分子团水，且保质期长，瓶装水三年，其直径、分解力、渗透力、活性力未发生任何变化，且仍为无菌水。
4、本发明制得的粒子能多功能活性水由于其特殊的活性及能量作用，可用于食品、保健、医药、生物、环境、疾控、农业、军工、机械、能源、日常生活等等各行各业。
附图说明
图1为本发明的制备粒子能多功能活性水的装置结构示意图。
图2为本发明的制备粒子能多功能活性水的装置中粒子能反应釜的结构示意图。
图3为本发明的制备粒子能多功能活性水的装置中真空式热交换器的结构示意图。
图4为本发明的制备粒子能多功能活性水的装置中交护式粒子能量水净化反应器的结构示意图。
本发明的实施方式
下面结合附图和具体实施例对本发明作进一步说明，以使本领域的技术人员可以更好的理解本发明并能予以实施，但所举实施例不作为对本发明的限定。
本发明的用于制备粒子能多功能活性水的复合材料含有如下成分：Si，Re，Pt，Ge，Nb，Ni，Se和Mg。
该复合材料通过如下方法制备：
1)取硅、铼、铂、锗、铌、镍、硒和镁，真空下混合均匀；
2)将步骤1)所得混合物置于磁化炉中实施磁化，磁化强度为5～10A/m，磁化100～200h；
3)将步骤2)磁化后的材料置于成型模具中，真空烧结；
4)步骤3)得到的材料再置于磁化炉中实施磁化，磁化强度为80～100A/m，磁化100～300h，得到所述复合材料。
该复合材料可成型为(但不限于)如下形状：
粒子能球形材料，直径6-10毫米，实芯球状；
粒子能蛋形球材料，最大直径43-82毫米，中空，壁厚2-3毫米，一端开口；
粒子能圆片形材料，直径30-120毫米，厚度2-5毫米；
粒子能正方体、长方体片状材料，规格40×60至200×220毫米，厚度2-5毫米。
上述复合材料用于制备粒子能多功能活性水的方法包括如下步骤：
1)水经管道引入蒸汽锅炉，加温致生成150-190℃的蒸汽，蒸汽通过高压分气缸输入粒子能反应釜；
2)在粒子能反应釜中，蒸汽与复合材料接触作用，粒子能反应釜中的蒸汽温度保持在150-190℃；
3)蒸汽自粒子能反应釜输出至真空式热交换器，与真空式热交换器中的复合材料接触及热交换后，水经水输出口输出，蒸汽经蒸汽出口回流至蒸汽锅炉；
4)真空式热交换器输出的水进入交互式粒子能量水净化反应器，与所述复合材料接触发生热交换至水温低于60℃后，输出，过滤，得粒子能多功能活性水。
本发明经大量实验发现复合材料所产生的基本粒子能量，能够对水起到至关重要的作用，从而使得大分子水在特定条件下与复合材料接触后，生成稳定的、并具有特殊能量的小分子水。其原理推测如下：能量粒子(即本发明的复合材料)在设备中发挥粒子能量作用，使质子内部的各种粒子，作轴向旋转运动时所产生的势能，改变了水分子的结构，使得单个水分子能稳定 的存在。因水分子的结构被改变失去缔合的作用力，所以在常温下不会再缔合成大分子团水。(制成的粒子能多功能活性水，即使将水反复加温至100度C或低温至-40度C冷冻，也不会重新缔合成大分子团水)
理论上推测，粒子能多功能水可能将水分子的原子核内部的质子和中子配对达到稳定状态，从而保持水分子的活性，并具有磁性。粒子能多功能水的单个水分子，基于水分子的基础结构H2O，氢原子半径79pm，氧原子半径70pm，当两个氢原子和氧原子键合成一个分子时，氢核与氧核的键合间距为96pm，氢原子和氧原子的外层电子间距在室温状态下为240pm。经过复合材料的能量处理后，单个水分子在室温条件下能够长期保持稳定的单分子状态。由此制出的粒子能多功能水的粘度降低，溶解能力、通透能力、分散能力均得以提高，活性作用增强而不会衰减。
实施例1
本实施例的用于制备粒子能多功能活性水的复合材料，以硅纳米粒子颗粒为基材，在混合其它7种纳米级颗粒组合而成。这种纳米级材料的平均长度为1-2纳米。
(一)制备复合材料的原料及比例如下：
a、硅纳米级颗粒作为复合材料构成基础，质量占复合材料组成的33.13％；
b、铼纳米级颗粒，质量占复合材料组成的21.87％；
c、铂纳米级颗粒，质量占复合材料组成的16.65％；
d、纯度为97％的锗纳米级颗粒，质量占复合材料组成的12.75％；
e、铌纳米级颗粒，质量占复合材料组成的9.45％；
f、镍纳米级颗粒，质量占复合材料组成的2.25％；
g、硒纳米级颗粒，质量占复合材料组成的2.17％；
h、镁纳米级颗粒，质量占复合材料组成的1.73％。
(二)本实施例复合材料的制备方法：
取上述硅、铼、铂、锗、铌、镍、硒和镁的纳米级颗粒，于真空环境中混合，材料混合后，在磁化炉中实施粒子能量磁化，磁化过程中磁化强度应达7A/m，并维持磁化强度123.25h。磁化后进行低高温转变烧结，将材料置于成型模具中先以823.7℃进行烧结，1.7h，再以920度恒温烧结12h。烧结后，再次磁化，磁化强度为97A/m，进行235.5h的常温持续磁化。
根据模具的不同，复合材料成型为如下形状：
粒子能球形材料，直径6-10毫米，实芯球状或中空球形；
粒子能开口蛋形球材料，最大直径43-82毫米，中空，壁厚2-3毫米；
粒子能圆片形材料，直径30-120毫米，厚度2-5毫米；
粒子能正方体、长方体片状材料，规格40×60至200×220毫米，厚度2-5毫米。
(三)本实施例的复合材料在特定装置中用于制备粒子能多功能活性水的方法具体如下：
结合图1～3所示，本发明用于制备粒子能多功能活性水的装置，包括：
蒸汽锅炉1，用于将水加热为高压蒸汽。
高压分气缸2，通过管道与蒸汽锅炉1连接。
粒子能反应釜3(如图2所示)，包括：
罐体30，罐身设有蒸汽入口301，罐顶设有蒸汽出口302，蒸汽入口302通过管道与高压分气缸连通；
支撑网31，其为一形状与罐体30横截面相同的网状结构，架设在罐体30内的下部，将罐体30内部分隔为上部装填区和下部通气区；
阻挡部32，由一体成型的垂直阻挡板321和水平阻挡板322构成，垂直阻挡板321的上底边与水平阻挡板322一体成型，垂直阻挡板321的两侧边贴合罐壁，垂直阻挡板321的底边架设在支撑网31上；水平阻挡板322的一边与垂直阻挡板321一体成型，其余边贴合罐壁；以此，阻挡部32将罐体内的上部装填区分隔为进气区和绕行区，其中，蒸汽入口301在罐体上对应设于进气区的位置，在本发明的优选实施方式中，罐体设有两个蒸汽入口301，上蒸汽入口对应位于进气区的顶部，下蒸汽入口对应位于进气区的底部；
球形或开口蛋壳形的复合材料，封装在钢丝网兜中后装填满装填区。
真空式热交换器4(如图3所示)，包括：
罐体40，罐顶设有蒸汽出口402通过管道与蒸汽锅炉1连通，罐底设有水输出口403，罐身设有蒸汽入口401通过管道与粒子能反应釜的蒸汽出口302连通；
第一支撑网41，为一形状与罐体横截面相同的网状结构，架设在罐体内的下部，第一支撑网41上装填球形或开口蛋壳形的复合材料(复合材料封装在钢丝网兜中后装填)，构成第一热交换区，所述蒸汽入口对应设于第一支撑网的下方；
第二支撑网42，为一形状与罐体横截面相同的网状结构，架设在罐体内的上部，第一支撑网上装填片状的复合材料，构成第二热交换区；
其中，第一热交换区和第二热交换区之间还有无填充的缓冲区；
在本发明的优选实施方式中，本装置包括多个所述真空式热交换器4，各真空式热交换器的蒸汽入口401分别与粒子能反应釜的蒸汽出口302连通，各真空式热交换器的蒸汽出口402分别与蒸汽锅炉的入口连通。
如图4所示，交互式粒子能量水净化反应器5，包括罐体50、支撑网51和装填支撑网上所述复合材料(可不必装满)，其罐身设有水输入口501和设有水输出口502，水输入口501通过管道与所述真空式热交换器4的水输出口403连通。如图1所示，本装置包括多个所述交互式粒子能量水净化反应器5，通过管道串联连通。
本发明的装置中，连通真空式热交换器4和交互式粒子能量水净化反应器5的管道上设有过滤装置6。
本实施例利用上述装置制备粒子能多功能活性水的方法，包括：
1)水经管道引入蒸汽锅炉1，加温致生成145-155℃的蒸汽，蒸汽通过高压分气缸2输入粒子能反应釜3。水的选用；优质河水、湖水、水库水均可选用，地下水要选用非石灰岩地层的。自来水去掉净化剂后，亦可使用。引用的外源水，经过滤后，储备备用。
2)在粒子能反应釜3中，蒸汽与复合材料接触反应，粒子能反应釜3中的蒸汽温度保持在145-155℃。所输入的高温蒸气，需要经过粒子能反应釜3的循环热势能反应，在高温状态下，粒子能核心材料对蒸气进行高效磁化作用，即利用高温、高压的粒子能势能作用，改变处于蒸气状态下的水分子结构。粒子能反应釜具有真空磁化作用，能使粒子能量稳定的作用于粒子能多功能水的制备过程中。高温蒸气进入粒子能反应釜后，粒子能复合材料随着温度的升高，其粒子能量势能增强，并作用于蒸气。高温蒸气经过高强度粒子能复合材料稳定的粒子势能磁化过程后，水分子的结构发生变化，维持这种强度的磁场，能够达到分子分离过程所需的磁场密度。经过粒子势能磁化过的水分子以气态形式，进入真空式热交换器。
3)将粒子能反应釜3，磁化好的蒸气输入真空式热交换器4，经上下两层粒子能量场的热交换。由真空式热交换器4将蒸气与形成的分离。磁化好的已形成的单分子水向下分流，输入交互式粒子能量水净化反应器5。仍处于蒸气状态的尚不完全稳定的气态水分子(蒸气)，经管道送回蒸汽锅炉1再加热。真空式热交换器4通过真空交换过程，进行水与蒸气的热交互，在粒子能量势能的作用下，实现水分子的均匀分布。在粒子能量磁场强度和循环磁化交互过程中，水以单分子状态稳定存在，并通过下行管道进入交互式粒子能量水净化反应器。尚不稳定的水分子(气态)，则通过上行管道回入蒸汽锅炉1再加温。
4)经真空式热交换器4生产好的粒子能多功能活性水，输送至交互式粒子能量水净化反应器5。这一过程，主要是将水的温度，从高温向常温水转换。水中的热量通过水罐逐渐散发，在低于60摄氏度后，对水进行初期过滤。初期过滤好的水，输送致储水罐，待水冷却致常温后进行精滤，经过精滤的水，再输入成品水的水罐中储备。交互式粒子能量水净化反应器5将已形成的粒子能多功能水从真空式热交换器高，送入本设备后，水由高温逐渐过度到常温。在这一过程中，使水的结构在一定的低磁场强度下稳定下来，互换进行净化反应。
(四)本实施例制得的粒子能多功能活性水性质的检测与验证：
A、关于水分子的结构：
在电子透射显微镜下，粒子能多功能活性水的组成结构呈现不规则排列的小分子团状，直径在1nm以下，其小于现有的小分子团水(由10个以上的水分子聚组成的水分子团称为大分子团水，其直径大于2.6nm；由5-7个水分子组成的分子团水，称为小分子团水，其直径在1.1-1.6nm之间)。在电子隧道扫描显微镜下，粒子能多功能活性水呈单个水分子状排列。注：电子透射显微镜(ST)的分辨率为百万分之一毫米，电子隧道显微镜(STM)分辨率为亿分之一毫米。
B、关于粒子能多功能活性水的水质检验：
经中国疾病预防控制中心环境与健康相关产品安全所的检测，结果见下表：
理化指标
Figure PCTCN2015078758-appb-000004
Figure PCTCN2015078758-appb-000005
从上表中可看出，粒子能多功能活性水中各种矿物质和离子极有害物质的含量远远低于国家标准。
微生物指标
Figure PCTCN2015078758-appb-000006
从上表可看出，本实施例制得的粒子能多功能活性水为完全的无菌水，这是目前为止，现有的小分子水无法达到的。
C、关于粒子能多功能活性水的密度
检测方法：精确量取1m3的粒子能多功能活性水，称重。
经检测，常温下，密度为1.002～1.004g/cm3,属于目前为止唯一的密度超过1g/cm3的水(普通水在常温下密度为0.998g/cm3)。
D、关于放射性
将本发明的粒子能多功能活性水，送核工业北京地质研究院分析测试研究中心进行检测。
测试方法一：DZ/T 0064,80-1993<地下水检验方法等离子体质谱法测定锂等39个元素>，仪器型号：ELEMENT XR等离子体质谱分析仪
经检测，结果如下表(单位：μg/L)：
Figure PCTCN2015078758-appb-000007
测试方法二：DZ/T 0184-19-1997《水中氢同位素锌还原法测定》，DZ/T 0184-21-1997《天然水中氧同位素二氧化碳一水平衡法测定》。仪器型号：MAT 253.检测结果如下：
δDV-SMOW(‰)                δ18OV-SMOW(‰)
-30.7                        -6.2
从测试方法一和二的结果可看出，本发明的粒子能多功能活性水中并不含放射性元素，因 此不具有放射性。
E、稳定性
本实施例制得的粒子能多功能活性水加热到100度，也不会改变粒子能多功能活性水的功能特点与活性，也不能使粒子能多功能活性水缔合还原成普通水。在放置3年后，经活性实验验证，其活性并未出现任何衰退。
F、活性
本发明的粒子能多功能活性水经长期存放性质不变，推测可能与粒子能多功能活性水的活性特质有关。由于粒子能多功能活性水不含放射源，故，没有放射性。粒子能多功能活性水长期存放，且不衰减的活性源是什么，至今没有明确结论。从生产过程等方面判断，粒子能多功能活性水所存在的活性源，可能是磁性。几个小实验如下：
a.将本实施例制得的粒子能多功能活性水装入玻璃、塑料、铝制容器密封(500g容器)，将啤酒或白酒或香烟紧贴在容器边上，本水释放的能量可穿透包装物，两小时后，酒和烟的口味均发生明显变化，其口感，明显提高。
b.高分子材料制作的水床，装入粒子能多功能活性水人躺在上面30～45分钟后，疲劳顿消；颈椎痛者在睡前只需将一塑料瓶的粒子能多功能活性水置于颈下，2小时以后痛感即显著减轻甚至消失。
G、核磁共振
核磁共振为48--50赫兹。
(五)本实施例制得的粒子能多功能活性水的应用
1、粒子能多功能活性水与现代生物学
自然状态下存在的分子团水，由10个以上的水分子聚组成的水分子团称为大分子团水，其直径大于2.6nm；由5-7个水分子组成的分子团水，称为小分子团水，其直径在1.1-1.6nm之间。
现代生物学对人体细胞壁跨膜蛋白通道进行测定，人体细胞壁跨膜蛋白水通道为2nm。粒子能多功能水的单个水分子，氢原子和氧原子的外层电子间距在室温状态下为240pm，在蒸气状态下为390pm。因而粒子能多功能水，能够直接通过细胞水通道，进入每个细胞和红血球；能够满足人体每一个细胞核所需要的水分子和生长因子的数量进行代谢；能够改善人体因水分子过大而降低的细胞代谢功能。
1991年德国科学家，发现人的细胞膜上存在直径2nm能让水和离子化营养物质一同通过细胞的水通道，称为细胞水通道，小分子团水在人体蛋白质静电力的作用下，容易通过细胞膜的水通道，而10个以上水分子构成的水分子团，则很难进入细胞内部。
2000年美国科学家，用显微摄影拍到世界第一张细胞膜水通道蛋白的照片，再次证明了细胞水通道为2nm，大于2nm的水分子很难进入细胞内。且人体细胞最多可以进入10个水分子。
人体在发育时期，自身的蛋白质静电力作用极强，能将大分子团水分开使之进入细胞。在发育期过后随着年龄的增长，人体自身的作用能力逐渐减弱，其分解能力也程下降趋势。
科学证明，人体的细胞水通道，是由六个蛋白质亚单位包绕而成的六角形通道，在蛋白质 静电力的作用下，水分子一个一个穿过通道进入细胞，进行水合作用，对营养物质和代谢物进行吸收、排谢。
学界，证实了水是人体细胞吸收营养和生理活动需要的介质，而细胞壁的水通道是贯穿的，并非是一个封闭状的壳体。学界认为；人体细胞萎缩衰竭的原因是因为“人体细胞因水的交流受阻”所致。
从原理上讲，本发明制备的粒子能多功能活性水为单分子水，其能够很容易进入细胞内部，从而恢复人体细胞的原有功能，促进细胞增长和抗菌、抗病毒作用。
2、粒子能多功能活性水的医药用途
粒子能多功能活性水含有的微量矿物元素和微量金属元素全部达到了离子态，且有害物质含量极低并无菌，达到了纯水程度，可应用于医疗。其通过静脉滴注施用于病人，可将血液中的血脂、血糖和其它沉积物质分解并排出体外，并且细胞及基因也得到一定程度的修复。
A、癌症
河北某医院进行了癌症志愿临床试用，试用人为一30岁女性晚期乳腺癌症患者，试用方式为：癌症治疗药物与粒子能多功能活性水配制为静脉滴液后以静脉滴注对患者进行治疗，治疗过程中随时对患者进行基因检测，结果如下：最初，免疫活性基因CD4，PRF1和抗氧化能力基因SOD-2及毒物代谢酶基因CYP1A2表达异常，随治疗进行，部分基因表达已恢复正常，SOD-2基因也处于恢复中。从基因检测结果可看出，患者的病情已明显得到好转。
广州某医院进行了癌症志愿临床试用。试用人为一40岁癌症患者，使用方式为将抗癌注射药物溶解于本发明的粒子能多功能活性水中，静脉滴注。治疗6个月后经检查已查不到癌细胞。
B、高血压
试用人为50岁以上的高血压患者，试用方式为静脉滴注，试用量为每天250mL。连续滴注6天后，增加量至每天500mL，9～10天后血压恢复正常。
C、低血压
试用人为低血压患者，试用量为每天500mL试用方式为静脉滴注，滴注时无不良反应，连续滴注数日后，血压恢复到正常水平。
D、过敏
试用人为过敏症状患者，试用方式为静脉滴注，第一天滴注后，过敏症状加重，第二天开始过敏症状好转并减轻，连续滴注9天后，过敏症状消失。
E、心脑血管与心脏早搏
粒子能多功能活性水，对软化缓解心脑血管疾病的作用非常明显，每天经动脉滴注500毫升后，心脑血管患者的血液粘稠度大为降低，阻塞状态明显改善，血液中的血脂、沉积物质被分解后通过尿道排出体外。心脏早搏，试用人为男性心脏早搏患者，静脉滴注每天500mL。在滴注第二瓶后，早搏症状得到缓解，滴到第11瓶后，早搏症状至今未发生。另外，此患者有严重的失眠症，在滴注第4瓶后，不再失眠，而且他多年前已钙化的结核病块在滴注治疗后肺上阴影缩小。
F、其它
静脉滴注30分钟后，少数滴注者开始出现肠道蠕动、排气现象；滴注一小时后，有人出现尿意，大多数人出现尿意的时间在2小时以后。滴注期间或滴注后，第一次排尿，多数人的尿液呈可乐色，并伴有极细的微粒(经检测，多为代谢产生的废弃细胞组织)；少数人的尿液为粉红色，出现粉红色尿液的人，在第二次排尿，或数次滴注后，尿液有时也会呈可乐色。
目前为止，一人的尿液呈浅蓝色(其在铅锌矿工作，可能是铅锌超标)，一人的尿液呈浅绿色(在铜矿工作，可能是铜超标)。
糖尿病人滴注后排出的尿液有的发黄，有的可乐色，但都出现泡沫。吸毒病人滴注后尿液如酱油色。
推测本发明粒子能多功能活性水具有上述作用的原理：粒子能多功能活性水本身，对人体疾病没有任何治疗作用。而滴注后出现的显著效果，是因这种水，能够作用于人体细胞和细胞核内的基因；能够将细胞所需要的各种蛋白和物质输入细胞，为细胞与细胞组织的修复、存活、新生提供了物质基础。因而激活了人体自身的原有功能，使人体本身的功能作用得到恢复。粒子能多功能水，除了对人体萎缩、病变的细胞组织、基因产生修复作用外，还能对血液中的杂质和沉积物质进行代谢。尤其值得注意的是粒子能多功能水，不但对人体细胞具有较好的修复与促进生长的作用，也具有非常好的抗菌和抗病毒作用，并能够分解、清除体内、血液内的病菌、老化细胞和沉积物质。
3、粒子能多功能活性水的日常保健等用途
粒子能多功能活性水还可用于口服饮用和日常保健，其能够逐渐恢复人体细胞的原有功能，促进细胞增长和抗菌、抗病毒作用；粒子能多功能活性水不变质，功能亦不会因久存而衰减。
1)、每日早中晚三次，每次50-毫升饮用，能够增进肠道的蠕动、通气、调理肝脾、促进肠胃吸收与代谢作用。慢性便秘饮用5-7日后效果明显、排便通畅，且排气亦无臭味。对失眠、肠胃炎症、胃酸、胃痛、胃溃疡、过劳综合症(过度疲劳)等均有明显的改善作用。大部分肠胃病，在饮用粒子能多功能活性水15日后病症消失。热饮效果更佳，晚上最好在睡前饮用。
2)、高血压患者，每日饮用量1500-2000毫升，三日后效果显见，连续饮用五七日后，可降至每日三次，每次100毫升，可有效缓解血管的紧缩程度。
3)、眼功能缺陷者，可直接使用粒子能多功能活性水滴眼，一日数次不等，睡前再滴一次。粒子能多功能活性水能够逐渐修复眼细胞，恢复眼的原有功能。不必添加任何药物。用法，用10或20毫升的注射器，将水注入空眼药瓶，用于滴注即可。
4)、齿污、舌胎黄者，除按1项饮用外，每日早晚各一次含粒子能多功能活性水半口，时间5秒，刷牙20-30秒，(普通牙膏)稍长一点更好，能立即将牙垢、黄舌胎清除。过敏性鼻炎或鼻子不通，每个鼻孔各滴入两滴并吸一下气，鼻子能马上通气，亦能够立即缓解鼻炎。
5)、皮炎、粉刺、雀斑、花斑、皮癣等症，使用粒子能多功能活性水擦抺，效果明显，若在粒子能多功能活性水中配以药物效果更佳。脚气患者，只需用粒子能多功能活性水数滴，清洗患处，能够立即止痒，一、二日后脚气痊愈。狐臭，只需将粒子能多功能活性水喷于或擦于 腋下能立即止臭。
6)、美容，原用护肤、美白护肤品，兑入功能水搅匀，比例30-50％，1小时后能够自然溶合，即可使用；随时以功能水涂抹肌肤，皮感湿润；取水少量涂于发根处按摸30秒，能使头发柔顺、光亮，长期使用还有生发作用；睡前使用面膜，待干后用小水雾喷壶将面膜再度喷湿软。
7)、颈椎痛或病，可将功能水加热装入热水袋，温度适当即可，睡前置于颈椎处。此后用时，将热水袋放于盆中，以热水加热反复使用。女人痛经亦可用此法，将热水袋放于小腹即可。不可将功能水与其它水混用，装入热水袋中的水不可再喝，但可长期反复使用。
8)、粒子能多功能活性水还具有解酒作用，酒醉后喝粒子能多功能活性水150-200毫升，喝下即有感觉，约15-20分钟酒醒。喝下粒子能多功能活性水后，即使再出酒，也没有一点酒臭味儿，亦不会感到任何不适。
粒子能多功能活性水对酒的作用极好，任何白酒在饮用前，只要兑入粒子能多功能活性水3-5克摇动摇动(每瓶)，5分钟后兑入粒子能多功能活性水的白酒，会变的非常醇绵、甘香而不烈。假酒兑入粒子能多功能活性水，口感发苦，原酿酒则如上。以粒子能多功能活性水两瓶，中间夹一瓶白酒，12小时后同样能够使酒变的醇香甘绵。对啤酒、葡萄酒的作用亦是如此。
9)、伤风感冒，以热功能水冲感冒颗粒药一袋，一日三次，效果很好。
10)、女士经期不适，一可将粒子能多功能活性水加热饮用，二将粒子能多功能活性水装入热水袋中，用前将热水倒入盆中，将水袋焐热，置于小腹之上，可显著缓解痛经。
11)、蚊叮、虫咬、蜂蛰、皮肤搔痒，粒子能多功能活性水涂上后会立即止痒，红肿部位会逐渐消除。防晒的作用也非常好，将水涂裸露部分即可。
12)、粒子能多功能活性水对烧伤、红伤、烫伤的作用胜过现有药物(用者言)，患者，只需将粒子能多功能活性水少量喷在患处，一日多次效果极为明显，因为粒子能多功能活性水有非常好的促进细胞增长的作用；如划伤、创伤，使用粒子能多功能活性水清洗伤口能立即止痛，清洗后包扎即可。因粒子能多功能活性水具有抗菌作用。粒子能多功能活性水中无菌，见；中国疾控中心检测报告。
13)、粒子能水和光子(光量子)有理化性的作用特点，两者能互相转换各自的能量，故粒子能多功能活性水有很好的防晒作用。但存放，应避光。粒子能多功能活性水的另二个显著特点是，一、存放多久都不会变质，二、功能不会因存放时间长而衰减。
4、粒子能多功能活性水用于戒毒治疗
粒子能多功能活性水在戒毒治疗中主要通过静脉滴注形式，其作用机制一般是通过单个稳定的水分子经人体血液循环直接作用体内不同区域并直接进入该区域内细胞，因此粒子能多功能活性水对神经系统内细胞实现活化，促进细胞受损的代谢功能，刺激神经细胞的自我代谢能力，对不可逆的脑部细胞损伤进行修复，使因吸毒造成的脑部受损区域回复正常功能从而实现戒毒治疗。
临床上主要表现为对中脑-边缘多巴胺系统(伏隔核、海马、额前皮质、腹侧被盖区、杏仁核等)的受体、神经递质等进行修复作用。因吸毒形成的大脑奖赏系统变化症状得到缓解，是 奖赏机制下因外源性药物依赖而导致的成瘾性大脑功能恢复实现戒毒的目的。
粒子能多功能水静脉滴注临床表现为吸毒者因长期吸毒而导致的多巴胺神经恢复，使吸毒者实现正常的大脑奖赏机制令其对多巴胺所产生的兴奋感与愉悦感所需量回归正常范围，降低因长期吸食毒品而造成的多巴胺耐受现象。同时，在毒品使用后，突出后膜的多巴胺积累出现移除现象，使脑功能因毒品使用而超出正常范围的兴奋感症状得到明显缓解。
在戒断症状上表现为多巴胺系统在粒子能多功能活性水作用下实现功能退化恢复，中脑多巴胺和5-羟色胺转导活性的增强表现，从而缓解戒毒者在戒断阶段表现出的厌恶和焦虑现象。
基于目前应用粒子能多功能活性水对于戒毒的临床表现观察，基本未出现因常规药物治疗而产生的戒断症状和药物依赖症状，同时对因吸毒而造成的大脑损害有修复作用，吸毒者受损的空间知觉功能和听力等有一定程度恢复。
5、粒子能多功能活性水在农业上的应用
粒子能多功能活性水除了对动物细胞有很好的促进增长作用外，对植物细胞的作用，也非常明显。经过本粒子能多功能活性水浸泡过的油菜籽，播种后不但生长速度快，且比没有浸泡过种子的油菜的生长高度，高出约一倍。土豆，经切块后浸泡12小时，播种出芽后仅13天就生长致350毫米高。以粒子能多功能活性水喷花，能将花期延长一倍以上。
实施例2
本实施例的用于制备粒子能多功能活性水的复合材料，其原料及比例如下：
a、硅纳米级颗粒作为复合材料构成基础，质量占复合材料组成的21.03％；
b、铼纳米级颗粒，质量占复合材料组成的10.37％；
c、铂纳米级颗粒，质量占复合材料组成的29.05％；
d、纯度为97％的锗纳米级颗粒，质量占复合材料组成的10.15％；
e、铌纳米级颗粒，质量占复合材料组成的14.45％；
f、镍纳米级颗粒，质量占复合材料组成的9.05％；
g、硒纳米级颗粒，质量占复合材料组成的4.87％；
h、镁纳米级颗粒，质量占复合材料组成的1.03％。
(二)本实施例复合材料的制备方法：
取上述硅、铼、铂、锗、铌、镍、硒和镁的纳米级颗粒，于真空环境中混合，材料混合后，在磁化炉中实施粒子能量磁化，磁化过程中磁化强度应达10A/m，并维持磁化强度150h。磁化后进行低高温转变烧结，将材料置于成型模具中先以850℃进行烧结，2.1h，再以950度恒温烧结12h。烧结后，再次磁化，磁化强度为95A/m，进行245.1h的常温持续磁化。
(三)本实施例的复合材料在装置中用于制备粒子能多功能活性水的方法通实施例1。
(四)本实施例制得的粒子能多功能活性水性质的检测与验证：
A、关于水分子的结构：
在电子透射显微镜下，本实施例的粒子能多功能活性水的组成结构呈现不规则排列的小分子团状，直径在1nm以下，其小于现有的小分子团水(由10个以上的水分子聚组成的水分子团 称为大分子团水，其直径大于2.6nm；由5-7个水分子组成的分子团水，称为小分子团水，其直径在1.1-1.6nm之间)。在电子隧道扫描显微镜下，粒子能多功能活性水呈单个水分子状排列。注：电子透射显微镜(ST)的分辨率为百万分之一毫米，电子隧道显微镜(STM)分辨率为亿分之一毫米。
B、关于粒子能多功能活性水的水质检验：
经中国疾病预防控制中心环境与健康相关产品安全所的检测，结果见下表：
理化指标
Figure PCTCN2015078758-appb-000008
Figure PCTCN2015078758-appb-000009
从上表中可看出，粒子能多功能活性水中各种矿物质和离子的含量远远低于国家标准，基本属于纯水范畴。
微生物指标
Figure PCTCN2015078758-appb-000010
从上表可看出，本实施例的粒子能多功能活性水为仅含有少量菌落，达到国家标准，这是目前为止，现有的小分子水无法达到的。
C、关于粒子能多功能活性水的密度
检测方法：精确量取1m3的粒子能多功能活性水，称重。
经检测，常温下，密度为1.002～1.004g/cm3，属于目前为止唯一的密度超过1g/cm3的水(普通水在常温下密度为0.998g/cm3)。
E、稳定性
本实施例制得的粒子能多功能活性水加热到100度，也不会改变粒子能多功能活性水的功能特点与活性，也不能使粒子能多功能活性水缔合还原成普通水。在放置3年后，经活性实验验证，其活性并未出现任何衰退。
F、活性
本实施例的粒子能多功能活性水经长期存放性质不变：
a.将本实施例制得的粒子能多功能活性水装入玻璃、塑料、铝制容器密封(500g容器)，将啤酒或白酒或香烟紧贴在容器边上，两小时后酒和烟的口味发生明显改变，其口感明显提高。粒子能多功能活性水能够穿透包装物作用到其它物体，其能量作用原理和能量源目前尚无法给出明确结论。
b.高分子材料制作的水床，装入粒子能多功能活性水人躺在上面30～45分钟后，疲劳顿消；颈椎痛者在睡前只需将一塑料瓶的粒子能多功能活性水置于颈下，4-5小时以后痛感即显著 减轻甚至消失。
G、核磁共振
核磁共振为48—50赫兹。
(五)本实施例制得的粒子能多功能活性水的应用
本实施例制得的粒子能多功能活性水应用于治疗癌症、高血压、低血压、过敏、心脏早搏等的方法及日常保健的方法与实施例1相同，并取得了与实施例1相同的缓解和治疗效果。
实施例3
本实施例的用于制备粒子能多功能活性水的复合材料，其原料及比例如下：
a、硅纳米级颗粒作为复合材料构成基础，质量占复合材料组成的36.89％；
b、铼纳米级颗粒，质量占复合材料组成的25.37％；
c、铂纳米级颗粒，质量占复合材料组成的8.48％；
d、纯度为97％的锗纳米级颗粒，质量占复合材料组成的18.10％；
e、铌纳米级颗粒，质量占复合材料组成的5.05％；
f、镍纳米级颗粒，质量占复合材料组成的1.16％；
g、硒纳米级颗粒，质量占复合材料组成的1.12％；
h、镁纳米级颗粒，质量占复合材料组成的3.83％。
(二)本实施例复合材料的制备方法：
取上述硅、铼、铂、锗、铌、镍、硒和镁的纳米级颗粒，于真空环境中混合，材料混合后，在磁化炉中实施粒子能量磁化，磁化过程中磁化强度应达10A/m，并维持磁化强度150h。磁化后进行低高温转变烧结，将材料置于成型模具中先以850℃进行烧结，2.1h，再以950度恒温烧结12h。烧结后，再次磁化，磁化强度为95A/m，进行245.1h的常温持续磁化。
(三)本实施例的复合材料在装置中用于制备粒子能多功能活性水的方法通实施例1。
(四)本实施例制得的粒子能多功能活性水性质的检测与验证：
A、关于水分子的结构：
在电子透射显微镜下，本实施例的粒子能多功能活性水的组成结构呈现不规则排列的小分子状，直径在1nm以下，其小于现有的小分子团水(由10个以上的水分子聚组成的水分子团称为大分子团水，其直径大于2.6nm；由5-7个水分子组成的分子团水，称为小分子团水，其直径在1.1-1.6nm之间)。在电子隧道扫描显微镜下，粒子能多功能活性水呈单个水分子状排列。注：电子透射显微镜(ST)的分辨率为百万分之一毫米，电子隧道显微镜(STM)分辨率为亿分之一毫米。
B、关于粒子能多功能活性水的水质检验：
经中国疾病预防控制中心环境与健康相关产品安全所的检测，结果见下表1和表2：
经中国疾病预防控制中心环境与健康相关产品安全所的检测，结果见下表：
理化指标
Figure PCTCN2015078758-appb-000011
Figure PCTCN2015078758-appb-000012
从上表中可看出，粒子能多功能活性水中各种矿物质和离子的含量远远低于国家标准，基本属于纯水范畴。
微生物指标
Figure PCTCN2015078758-appb-000013
从上表可看出，本实施例的粒子能多功能活性水为仅含有少量微生物菌落，完全达到国家标准，这是目前为止，现有的小分子水无法达到的。
C、关于粒子能多功能活性水的密度
检测方法：精确量取1m3的粒子能多功能活性水，称重。
经检测，常温下，密度为1.002～1.004g/cm3，属于目前为止唯一的密度超过1g/cm3的水(普通水在常温下密度为0.998g/cm3)。
E、稳定性
本实施例制得的粒子能多功能活性水加热到100度，也不会改变粒子能多功能活性水的功能特点与活性，也不能使粒子能多功能活性水还原成普通水。
在放置3年后，经活性实验验证，其活性并未出现任何衰退。
F、活性
本实施例的粒子能多功能活性水经长期存放性质不变：
a.将本实施例制得的粒子能多功能活性水装入玻璃、塑料、铝制容器密封(500g容器)，将啤酒或白酒或香烟紧贴在容器边上，两小时后，酒和烟的口味均发生明显变化，其口感，明显提高。
b.高分子材料制作的水床，装入粒子能多功能活性水人躺在上面30～45分钟后，疲劳顿消；颈椎痛者在睡前只需将一塑料瓶的粒子能多功能活性水置于颈下，2小时以后痛感即显著减轻甚至消失。
G、核磁共振
核磁共振为48—50赫兹。
(五)本实施例制得的粒子能多功能活性水的应用
本实施例制得的粒子能多功能活性水应用于治疗癌症、高血压、低血压、过敏、心脏早搏等的方法及日常保健的方法与实施例1相同，并取得了与实施例1相同的缓解和治疗效果。
以上所述实施例仅是为充分说明本发明而所举的较佳的实施例，本发明的保护范围不限于此。本技术领域的技术人员在本发明基础上所作的等同替代或变换，均在本发明的保护范围之内。本发明的保护范围以权利要求书为准。

Claims (21)

  1. 一种用于制备粒子能多功能活性水的复合材料，其特征在于，其含有如下成分：Si，Re，Pt，Ge，Nb，Ni，Se和Mg。
  2. 根据权利要求1所述的复合材料，其特征在于，其含有的成分及各成分的重量份数如下：
    Figure PCTCN2015078758-appb-100001
  3. 根据权利要求2所述的复合材料，其特征在于，含有如下重量份数的成分：
    Figure PCTCN2015078758-appb-100002
  4. 根据权利要求1～3任一项所述的复合材料，其特征在于，所述复合材料为球形、中心开有通孔的球形、片状或一端开口的蛋壳形。
  5. 权利要求1～4任一项所述的复合材料的制备方法，其特征在于，包括如下步骤：
    1)取硅、铼、铂、锗、铌、镍、硒和镁，真空下混合均匀；
    2)将步骤1)所得混合物置于磁化炉中实施磁化，磁化强度为5～10A/m，磁化时间100～200h；
    3)将步骤2)磁化后的材料置于成型模具中，真空烧结；
    4)步骤3)得到的材料再置于磁化炉中实施磁化，磁化强度为80～100A/m， 磁化100～300h，得到所述复合材料。
  6. 根据权利要求5所述的复合材料的制备方法，其特征在于，步骤1)中所述的硅、铼、铂、锗、铌、镍、硒和镁均为纳米级颗粒。
  7. 根据权利要求5所述的复合材料的制备方法，其特征在于，步骤2)中磁化强度为7A/m，磁化时间为120～125h。
  8. 根据权利要求5所述的复合材料的制备方法，其特征在于，步骤3)中烧结温度为800～1000℃。
  9. 根据权利要求5所述的复合材料的制备方法，其特征在于，步骤3)中真空烧结为低高温转变烧结：步骤1)磁化后的材料置于成型模具中，真空下，先以800～850℃的温度烧结1～3h，再以900～1000℃的温度烧结10～15h。
  10. 根据权利要求5所述的复合材料的制备方法，其特征在于，步骤4)磁化强度为95～100A/m，磁化时间为200～250h。
  11. 权利要求1～4任一项所述的复合材料用于制备粒子能多功能活性水的装置，其特征在于，包括：
    蒸汽锅炉，用于将水加热为高压蒸汽；
    高压分气缸，通过管道与蒸汽锅炉连接；
    粒子能反应釜，包括罐体和装填在罐体内的所述复合材料，罐体设有蒸汽入口和蒸汽出口，蒸汽入口通过管道与高压分气缸连通；
    真空式热交换器，包括罐体和装填在罐体内的所述复合材料，罐体设有蒸汽入口通过管道与粒子能反应釜的蒸汽出口连通，罐顶设有蒸汽出口通过管道与蒸汽锅炉连通，罐底设有水输出口；
    交互式粒子能量水净化反应器，包括罐体和装填在罐体内的所述复合材料，罐体设有水输入口和水输出口，所述水输入口通过管道与所述真空式热交换器的水输出口连通。
  12. 根据权利要求11所述的装置，其特征在于，所述粒子能反应釜包括:
    罐体，罐身设有蒸汽入口，罐顶设有蒸汽出口；
    支撑网，其为一形状与罐体横截面相同的网状结构，架设在罐体内的下部，将罐体内部分隔为上部装填区和下部通气区；
    阻挡部，由一体成型的垂直阻挡板和水平阻挡板构成，垂直阻挡板的上底边与水平阻挡板一体成型，垂直阻挡板的两侧边贴合罐壁，底边架设在支撑网上；水平阻挡板的一边与垂直阻挡板一体成型，其余边贴合罐壁；以此，阻挡部将罐体内的上部装填区分隔为进气区和绕行区，其中，蒸汽入口在罐体上对应设于进气区的位置；所述复合材料，装填满装填区。
  13. 根据权利要求12所述的装置，其特征在于，所述罐体设有两个蒸汽入 口，上蒸汽入口对应位于进气区的顶部，下蒸汽入口对应位于进气区的底部。
  14. 根据权利要求11所述的装置，其特征在于，所述真空式热交换器包括：
    罐体，罐顶设有蒸汽出口，罐底设有水输出口，罐身设有蒸汽入口；
    第一支撑网，为一形状与罐体横截面相同的网状结构，架设在罐体内的下部，第一支撑网上装填球形或开口蛋壳形的所述复合材料，构成第一热交换区，所述蒸汽入口对应设于第一支撑网的下方；
    第二支撑网，为一形状与罐体横截面相同的网状结构，架设在罐体内的上部，第一支撑网上装填片状的所述复合材料，构成第二热交换区；
    其中，第一热交换区和第二热交换区之间还有无填充的缓冲区。
  15. 根据权利要求11所述的装置，其特征在于，连通真空式热交换器和交互式粒子能量水净化反应器的管道上设有过滤装置。
  16. 根据权利要求11所述的装置，其特征在于，所述装置包括多个所述真空式热交换器，各真空式热交换器的蒸汽入口分别与粒子能反应釜的蒸汽出口连通，各真空式热交换器的蒸汽出口分别与蒸汽锅炉的入口连通。
  17. 根据权利要求16所述的装置，其特征在于，所述装置包括多个所述交互式粒子能量水净化反应器，通过管道串联连通。
  18. 根据权利要求11所述的装置，其特征在于，所述交互式粒子能量水净化反应器的水输出口连接的管道设有过滤装置。
  19. 权利要求11～18所述的装置用于制备粒子能多功能活性水的方法，其特征在于，包括：
    1)水经管道引入蒸汽锅炉，加温致生成150-190℃的蒸汽，蒸汽通过高压分气缸输入粒子能反应釜；
    2)在粒子能反应釜中，高温蒸汽与复合材料接触产生的粒子势能作用于水分子，粒子能反应釜中的蒸汽温度保持在150-190℃；
    3)蒸汽自粒子能反应釜输出至真空式热交换器，与真空式热交换器中的复合材料二次接触及热交换后，水经水输出口输出，蒸汽经蒸汽出口回流至蒸汽锅炉；
    4)真空式热交换器输出的水进入交互式粒子能量水净化反应器，与所述复合材料接触发生热交换至水温低于60℃后，输出，过滤，得粒子能多功能活性水。
  20. 根据权利要求19所述的方法，其特征在于，步骤1)和步骤2)中蒸汽的温度为145～155℃。
  21. 权利要求19或20所述方法制备的粒子能多功能活性水。
PCT/CN2015/078758 2015-05-12 2015-05-12 制备粒子能多功能活性水的复合材料、制备方法及装置 Ceased WO2016179792A1 (zh)

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