AR110314A1 - Procesos para la purificación, recuperación, y conversión de sales de clorofenol y preparación y recuperación de productos preparados a partir de las mismas - Google Patents
Procesos para la purificación, recuperación, y conversión de sales de clorofenol y preparación y recuperación de productos preparados a partir de las mismasInfo
- Publication number
- AR110314A1 AR110314A1 ARP170103401A ARP170103401A AR110314A1 AR 110314 A1 AR110314 A1 AR 110314A1 AR P170103401 A ARP170103401 A AR P170103401A AR P170103401 A ARP170103401 A AR P170103401A AR 110314 A1 AR110314 A1 AR 110314A1
- Authority
- AR
- Argentina
- Prior art keywords
- recovery
- salts
- chlorophenol
- processes
- purification
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 12
- ISPYQTSUDJAMAB-UHFFFAOYSA-N 2-chlorophenol Chemical class OC1=CC=CC=C1Cl ISPYQTSUDJAMAB-UHFFFAOYSA-N 0.000 title abstract 8
- 238000011084 recovery Methods 0.000 title abstract 5
- 238000006243 chemical reaction Methods 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 3
- 238000000746 purification Methods 0.000 title abstract 3
- RANCECPPZPIPNO-UHFFFAOYSA-N 2,5-dichlorophenol Chemical compound OC1=CC(Cl)=CC=C1Cl RANCECPPZPIPNO-UHFFFAOYSA-N 0.000 abstract 3
- IWEDIXLBFLAXBO-UHFFFAOYSA-N dicamba Chemical compound COC1=C(Cl)C=CC(Cl)=C1C(O)=O IWEDIXLBFLAXBO-UHFFFAOYSA-N 0.000 abstract 3
- 150000003839 salts Chemical class 0.000 abstract 3
- 239000005504 Dicamba Substances 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 2
- 239000000543 intermediate Substances 0.000 abstract 2
- 239000005631 2,4-Dichlorophenoxyacetic acid Substances 0.000 abstract 1
- FKIKPQHMWFZFEB-UHFFFAOYSA-N 3,6-dichloro-2-hydroxybenzoic acid Chemical compound OC(=O)C1=C(O)C(Cl)=CC=C1Cl FKIKPQHMWFZFEB-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/04—Monocyclic monocarboxylic acids
- C07C63/06—Benzoic acid
- C07C63/10—Halides thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/64—Preparation of O-metal compounds with O-metal group bound to a carbon atom belonging to a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/685—Processes comprising at least two steps in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/72—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/74—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
- C07C37/78—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/74—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
- C07C37/80—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/15—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction of organic compounds with carbon dioxide, e.g. Kolbe-Schmitt synthesis
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procesos para la purificación, recuperación, y conversión de sales de clorofenol (por ejemplo, 2,5-diclorofenol y sales del mismo). En diversos aspectos, la presente se relaciona con la eliminación de una o más impurezas de corrientes de proceso que contienen sales de clorofenol y/o la recuperación de sales de clorofenol de corrientes de proceso para utilizar el clorofenol recuperado en cualquier otra parte de un proceso integrado. Las corrientes de proceso que se pueden tratar de acuerdo con la presente incluyen a aquellas que incorporan una o más sales de clorofenol en una mezcla de alimentación y también a aquellas donde hay presentes una o más sales de clorofenol en una corriente de producto o subproducto de un proceso integrado. Por ejemplo, los procesos de conversión de la presente son apropiados para usar como parte de un proceso integrado para producir ácido 3,6-dicloro-2-metoxibenzoico (dicamba) o una sal o un éster del mismo o un proceso para producir ácido 2,4-diclorofenoxiacético (2,4-D) o una sal o un éster del mismo. Además, procesos para la preparación, purificación, y recuperación de los intermediarios que se forman en procesos integrados en los que se utilizan como materia prima sales de clorofenol tales como 2,5-diclorofenol, incluyendo al intermediario ácido 3,6-diclorosalicílico (3,6-DCSA) que se forma durante la preparación del dicamba a partir de 2,5-diclorofenol.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201662431205P | 2016-12-07 | 2016-12-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR110314A1 true AR110314A1 (es) | 2019-03-20 |
Family
ID=62491613
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP170103401A AR110314A1 (es) | 2016-12-07 | 2017-12-04 | Procesos para la purificación, recuperación, y conversión de sales de clorofenol y preparación y recuperación de productos preparados a partir de las mismas |
| ARP220100706A AR125593A2 (es) | 2016-12-07 | 2022-03-25 | Procesos para la purificación, recuperación, y conversión de sales de clorofenol y preparación y recuperación de productos preparados a partir de las mismas |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP220100706A AR125593A2 (es) | 2016-12-07 | 2022-03-25 | Procesos para la purificación, recuperación, y conversión de sales de clorofenol y preparación y recuperación de productos preparados a partir de las mismas |
Country Status (7)
| Country | Link |
|---|---|
| US (3) | US10913701B2 (es) |
| EP (1) | EP3551601B1 (es) |
| JP (4) | JP7010944B2 (es) |
| CN (2) | CN110248919B (es) |
| AR (2) | AR110314A1 (es) |
| BR (1) | BR112019011557B1 (es) |
| WO (1) | WO2018106564A1 (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR112019011557B1 (pt) * | 2016-12-07 | 2022-10-18 | Monsanto Technology Llc | Processos de purificação, recuperação e conversão de sais de clorofenol e preparação e recuperação de produtos preparados dos mesmos |
| CN117438123B (zh) * | 2023-12-22 | 2024-05-07 | 中国核电工程有限公司 | 确定萃取柱中铀萃取区的方法、装置、控制其位置的方法 |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2480817A (en) | 1947-06-17 | 1949-08-30 | Us Rubber Co | Preparation of polychlorophenoxyacetic acids useful as plant growth regulators |
| GB651670A (en) * | 1947-08-13 | 1951-04-04 | Us Rubber Co | Improvements in preparation of polychlorophenoxy-aliphatic acids |
| US2651659A (en) | 1952-01-31 | 1953-09-08 | Us Rubber Co | Preparation of 2, 4-dichlorophenoxyacetic acid |
| US3013054A (en) | 1958-08-04 | 1961-12-12 | Velsicol Chemical Corp | 2-methoxy-3, 6-dichlorobenzoates |
| US4001341A (en) * | 1964-01-24 | 1977-01-04 | General Electric Company | Extraction separation |
| US3335177A (en) * | 1964-05-28 | 1967-08-08 | Velsicol Chemical Corp | Process for preparing 2-methoxy-3, 6-dichlorobenzoic acid |
| GB1221019A (en) | 1968-02-09 | 1971-02-03 | Coalite Chem Prod Ltd | Process for the production of dihalophenols |
| US4067913A (en) | 1972-03-20 | 1978-01-10 | Velsicol Chemical Corporation | Process for the production of 2,5-dichloro-4-bromophenol |
| PL85546B1 (es) | 1973-04-11 | 1976-04-30 | ||
| US4559109A (en) * | 1983-03-31 | 1985-12-17 | Phillips Petroleum Company | Dehydration of alcohol with extractive distillation |
| JPH04149150A (ja) * | 1990-10-08 | 1992-05-22 | Mitsui Toatsu Chem Inc | パラヒドロキシ安息香酸の分離方法 |
| US5648562A (en) | 1994-08-03 | 1997-07-15 | Sandoz Ltd. | Oxidation process |
| JP3739543B2 (ja) * | 1996-10-02 | 2006-01-25 | 三井化学株式会社 | ヒドロキシ安息香酸類の製造方法 |
| US7049435B2 (en) | 2002-03-08 | 2006-05-23 | Tate & Lyle Public Limited Company | Extractive methods for purifying sucralose |
| ITMI20021187A1 (it) | 2002-05-31 | 2003-12-01 | Polimeri Europa Spa | Procedimento per il recupero di fenolo e difenoli |
| JP5023618B2 (ja) | 2005-09-01 | 2012-09-12 | 住友化学株式会社 | 加水分解反応混合物の脱水方法 |
| JP5064690B2 (ja) | 2006-01-27 | 2012-10-31 | 出光興産株式会社 | フェノール含有水の処理方法及び処理設備 |
| ATE519726T1 (de) * | 2006-05-04 | 2011-08-15 | Badger Licensing Llc | Verbessertes verfahren zur herstellung von polyphenolen |
| CN101659586B (zh) * | 2009-09-21 | 2013-04-10 | 浙江升华拜克生物股份有限公司 | 水杨酸衍生物和相应苯酚衍生物的萃取分离方法 |
| CN101863744B (zh) * | 2010-07-10 | 2013-02-13 | 南京师范大学 | 一种错流离解萃取分离二氯苯酚混合物的方法 |
| CN102838482B (zh) * | 2012-09-20 | 2015-02-04 | 山东潍坊润丰化工股份有限公司 | 一种3,6-二氯水杨酸的制备方法 |
| CN102942474B (zh) | 2012-11-26 | 2015-07-08 | 江苏优嘉化学有限公司 | 一种除草剂麦草畏的合成工艺 |
| CN103012123B (zh) * | 2012-12-20 | 2014-11-26 | 浙江大学 | 3,6-二氯-2-羟基苯甲酸的合成方法 |
| CN103012124B (zh) * | 2012-12-26 | 2015-03-25 | 浙江大学 | 3,6-二氯-2-羟基苯甲酸的制备方法 |
| EP3083555B1 (en) | 2013-12-18 | 2018-10-03 | Monsanto Technology LLC | Processes for the diazotization of 2,5-dichloroanilines |
| AR100506A1 (es) | 2014-05-19 | 2016-10-12 | Basf Se | Proceso de obtención del herbicida dicamba |
| CN107848840B (zh) * | 2015-06-03 | 2021-07-06 | 孟山都技术公司 | 二氯苯酚的分离 |
| CN105884582A (zh) * | 2016-04-29 | 2016-08-24 | 四川福思达生物技术开发有限责任公司 | 一种2,5-二氯苯酚的合成工艺 |
| CN105859508B (zh) | 2016-05-06 | 2019-03-05 | 四川福思达生物技术开发有限责任公司 | 一种制备麦草畏的工艺 |
| BR112019011557B1 (pt) | 2016-12-07 | 2022-10-18 | Monsanto Technology Llc | Processos de purificação, recuperação e conversão de sais de clorofenol e preparação e recuperação de produtos preparados dos mesmos |
-
2017
- 2017-12-04 BR BR112019011557-9A patent/BR112019011557B1/pt active IP Right Grant
- 2017-12-04 JP JP2019530431A patent/JP7010944B2/ja active Active
- 2017-12-04 CN CN201780081778.1A patent/CN110248919B/zh active Active
- 2017-12-04 US US16/467,622 patent/US10913701B2/en active Active
- 2017-12-04 CN CN202310824430.4A patent/CN116854579A/zh active Pending
- 2017-12-04 AR ARP170103401A patent/AR110314A1/es active IP Right Grant
- 2017-12-04 WO PCT/US2017/064424 patent/WO2018106564A1/en not_active Ceased
- 2017-12-04 EP EP17878493.0A patent/EP3551601B1/en active Active
-
2020
- 2020-12-29 US US17/136,341 patent/US11629114B2/en active Active
-
2022
- 2022-01-13 JP JP2022003452A patent/JP2022050607A/ja active Pending
- 2022-03-25 AR ARP220100706A patent/AR125593A2/es not_active Application Discontinuation
-
2023
- 2023-02-28 US US18/115,127 patent/US12240807B2/en active Active
- 2023-05-02 JP JP2023075995A patent/JP2023099168A/ja active Pending
-
2024
- 2024-01-17 JP JP2024005113A patent/JP2024041948A/ja not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| JP7010944B2 (ja) | 2022-02-10 |
| US10913701B2 (en) | 2021-02-09 |
| JP2023099168A (ja) | 2023-07-11 |
| US20190322612A1 (en) | 2019-10-24 |
| EP3551601A1 (en) | 2019-10-16 |
| JP2019536807A (ja) | 2019-12-19 |
| JP2022050607A (ja) | 2022-03-30 |
| US12240807B2 (en) | 2025-03-04 |
| EP3551601B1 (en) | 2024-06-19 |
| BR112019011557A2 (pt) | 2019-10-15 |
| US20230202961A1 (en) | 2023-06-29 |
| CN116854579A (zh) | 2023-10-10 |
| US20210163395A1 (en) | 2021-06-03 |
| EP3551601A4 (en) | 2020-08-05 |
| AR125593A2 (es) | 2023-08-02 |
| US11629114B2 (en) | 2023-04-18 |
| WO2018106564A1 (en) | 2018-06-14 |
| CN110248919B (zh) | 2023-07-14 |
| CN110248919A (zh) | 2019-09-17 |
| BR112019011557B1 (pt) | 2022-10-18 |
| JP2024041948A (ja) | 2024-03-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration |