AT33319B - Process for the representation of monochloro-monobromoindigo. - Google Patents
Process for the representation of monochloro-monobromoindigo.Info
- Publication number
- AT33319B AT33319B AT33319DA AT33319B AT 33319 B AT33319 B AT 33319B AT 33319D A AT33319D A AT 33319DA AT 33319 B AT33319 B AT 33319B
- Authority
- AT
- Austria
- Prior art keywords
- monochloro
- monobromoindigo
- representation
- desc
- indigo
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 235000000177 Indigofera tinctoria Nutrition 0.000 claims description 3
- 229940097275 indigo Drugs 0.000 claims description 3
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 claims description 3
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 2
- 229910052794 bromium Inorganic materials 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 125000003963 dichloro group Chemical group Cl* 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- ORFSSYGWXNGVFB-UHFFFAOYSA-N sodium 4-amino-6-[[4-[4-[(8-amino-1-hydroxy-5,7-disulfonaphthalen-2-yl)diazenyl]-3-methoxyphenyl]-2-methoxyphenyl]diazenyl]-5-hydroxynaphthalene-1,3-disulfonic acid Chemical compound COC1=C(C=CC(=C1)C2=CC(=C(C=C2)N=NC3=C(C4=C(C=C3)C(=CC(=C4N)S(=O)(=O)O)S(=O)(=O)O)O)OC)N=NC5=C(C6=C(C=C5)C(=CC(=C6N)S(=O)(=O)O)S(=O)(=O)O)O.[Na+] ORFSSYGWXNGVFB-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring (AREA)
- Indole Compounds (AREA)
Description
<Desc/Clms Page number 1>
Verfahren zur Darstellung von Monochlor-Monobromindigo.
In der Patentschrift Nr. 33318 (zweites Zusatz-Patent zum Patente Nr. 3220ï) ist die Darstellung von gemischten Tri- und Tetrahalogensubstitutionsprodukten des Indigos beschrieben worden, bestehend in der Einwirkung von entsprechenden Mengen Brom auf Mono- und Dichlorderivate des Indigos. Es wurde nun weiter gefunden, dass man in analoger Weise auch zu den gemischten Dihalogenderivaten, d. h. zu Monochlor-Monobromsubstitutions-
EMI1.1
in Nitrobenzol mit reinblauer Farbe.
Beim Behandeln mit alkalischen Reduktionsmitteln, namentlich Natronlauge und Natriumhydrosultit, wird eine klare hellagelbe Küpe erhalten, aus welcher ungebeizte Baumwolle in lebhaften rotstichig-blauen Nuancen von vorzüglicher Waschechtheit, sowie guter Chlor- und Lichtechtheit angefärbt wird.
**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
<Desc / Clms Page number 1>
Process for the representation of monochloro-monobromoindigo.
In patent specification No. 33318 (second additional patent to patent No. 3220ï) the preparation of mixed tri- and tetrahalogen substitution products of indigo has been described, consisting in the action of corresponding amounts of bromine on mono- and dichloro derivatives of indigo. It has now been found that in an analogous manner to the mixed dihalogen derivatives, ie. H. to monochloro monobromo substitution
EMI1.1
in nitrobenzene with a pure blue color.
When treating with alkaline reducing agents, namely sodium hydroxide solution and sodium hydrosultite, a clear, light yellow vat is obtained from which unstained cotton is dyed in vivid reddish-blue shades of excellent washfastness, as well as good chlorine and lightfastness.
** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT32207T | 1907-03-04 | ||
| AT33319T | 1907-06-06 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AT33319B true AT33319B (en) | 1908-06-10 |
Family
ID=25599732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT33319D AT33319B (en) | 1907-03-04 | 1907-06-06 | Process for the representation of monochloro-monobromoindigo. |
Country Status (1)
| Country | Link |
|---|---|
| AT (1) | AT33319B (en) |
-
1907
- 1907-06-06 AT AT33319D patent/AT33319B/en active
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