AT45026B - Process for the preparation of acidic wool dyes of the anthracene series. - Google Patents
Process for the preparation of acidic wool dyes of the anthracene series.Info
- Publication number
- AT45026B AT45026B AT45026DA AT45026B AT 45026 B AT45026 B AT 45026B AT 45026D A AT45026D A AT 45026DA AT 45026 B AT45026 B AT 45026B
- Authority
- AT
- Austria
- Prior art keywords
- sep
- yellow
- preparation
- acidic
- wool dyes
- Prior art date
Links
- 230000002378 acidificating effect Effects 0.000 title claims description 6
- 210000002268 wool Anatomy 0.000 title claims description 3
- 150000001454 anthracenes Chemical class 0.000 title claims 2
- 239000000975 dye Substances 0.000 title claims 2
- KHUFHLFHOQVFGB-UHFFFAOYSA-N 1-aminoanthracene-9,10-dione Chemical class O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2N KHUFHLFHOQVFGB-UHFFFAOYSA-N 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 150000003460 sulfonic acids Chemical class 0.000 claims 1
- 239000002253 acid Substances 0.000 description 6
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 description 6
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 244000172533 Viola sororia Species 0.000 description 3
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 2
- QOIXLGYJPBDQSK-UHFFFAOYSA-N 3,6-dioxocyclohexa-1,4-diene-1-sulfonic acid Chemical compound OS(=O)(=O)C1=CC(=O)C=CC1=O QOIXLGYJPBDQSK-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 2
- KXOGXZAXERYOTC-UHFFFAOYSA-N 1-amino-4-methoxyanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C(N)=CC=C2OC KXOGXZAXERYOTC-UHFFFAOYSA-N 0.000 description 1
- -1 Benzoyl- Chemical group 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 235000005811 Viola adunca Nutrition 0.000 description 1
- 240000009038 Viola odorata Species 0.000 description 1
- 235000013487 Viola odorata Nutrition 0.000 description 1
- 235000002254 Viola papilionacea Nutrition 0.000 description 1
- WETWJCDKMRHUPV-UHFFFAOYSA-N acetyl chloride Chemical compound CC(Cl)=O WETWJCDKMRHUPV-UHFFFAOYSA-N 0.000 description 1
- 239000012346 acetyl chloride Substances 0.000 description 1
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<Desc/Clms Page number 1>
EMI1.1
EMI1.2
<Desc/Clms Page number 2>
EMI2.1
EMI2.2
<tb>
<tb> Farbe <SEP> der <SEP> Lösung <SEP> in
<tb> konzentrierter <SEP> Färbung <SEP> auf <SEP> Wolle
<tb> Schwefeisäure <SEP> heiss@m <SEP> Wasser
<tb> 1-Aminoanthrachinon-6-sulfo-
<tb> 1 <SEP> zitronengelb <SEP> gelb <SEP> gelb
<tb> saure <SEP> + <SEP> Essigsäureanhydrid
<tb> 1-Aminoanthracinon-6-sulfo-
<tb> 2 <SEP> gelb <SEP> gelb <SEP> rötlich <SEP> gelb
<tb> säure <SEP> @xals@ure
<tb> 1 <SEP> Aminoanthrachinon <SEP> 6-sulfo-
<tb> 3. <SEP> orangegelb <SEP> gelb <SEP> gelb
<tb> säure <SEP> Benzoylchlorid
<tb> 1 <SEP> Aminoanthrachinon-ti-sulfo-
<tb> 4. <SEP> orange <SEP> gelb <SEP> grünstichig <SEP> gelb
<tb> süure <SEP> Salicylsäure
<tb> 1 <SEP> Aminoanthrachinon-6-sulfo-
<tb> 5.
<SEP> grünstichig <SEP> gelb <SEP> gelb <SEP> gelb
<tb> saure <SEP> + <SEP> Zimmtsäure
<tb> 1-Aminoanthrachinon-6-sulto-
<tb> 6. <SEP> gelb <SEP> gelb <SEP> grünstichig <SEP> gelb
<tb> saure <SEP> Suceinylchlorid.
<tb>
1-AMinoanthrachinon <SEP> 5-sulfo-
<tb> 7. <SEP> grunstichig <SEP> gelb <SEP> gelb <SEP> orangegelb
<tb> saure <SEP> Benzoylchlorid.
<tb>
1-Aminoanthrachinon <SEP> 8-sulfo
<tb> 8. <SEP> gelb <SEP> gelb <SEP> gelb
<tb> säure <SEP> benzoylchlorid.
<tb>
1.4-Diaminoanthrachinon-6-sulfo
<tb> 9. <SEP> gelb <SEP> rot <SEP> rot
<tb> säure <SEP> Bezoylchlorid
<tb> 1.5 <SEP> Diaminoanthrachinon-2.6-
<tb> 10. <SEP> orangegelb <SEP> orange <SEP> bräunlich <SEP> gelb
<tb> disulfosaure <SEP> Benzoylchlorid
<tb> 1-Amino-4-methylaminoanthra-
<tb> 11. <SEP> schwach <SEP> gefärbt <SEP> violett <SEP> violett
<tb> chinonsulfosäure <SEP> - <SEP> Acetylchlorid
<tb> 1-Amino-4 <SEP> methylaminoanthra-
<tb> 12. <SEP> chinonsulfosäure <SEP> + <SEP> Benzoyl- <SEP> schwach <SEP> gefärbt <SEP> violettblan <SEP> blauviolett
<tb> chlorid. <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> . <SEP> .
<tb>
1-Amino-4-methoxyanthrachinon-
<tb> 13. <SEP> orangerot <SEP> orange <SEP> orange
<tb> 7-sulfosäure <SEP> + <SEP> Benzoylchlorid
<tb> 1-Amino <SEP> 4 <SEP> p-tolylaminoanthra-
<tb> 14. <SEP> chinonsulfosäure <SEP> + <SEP> Benzoyl <SEP> violett <SEP> blan <SEP> blan
<tb> chlorid
<tb>
<Desc / Clms Page number 1>
EMI1.1
EMI1.2
<Desc / Clms Page number 2>
EMI2.1
EMI2.2
<tb>
<tb> Color <SEP> of the <SEP> solution <SEP> in
<tb> concentrated <SEP> dyeing <SEP> on <SEP> wool
<tb> sulfuric acid <SEP> hot @ m <SEP> water
<tb> 1-aminoanthraquinone-6-sulfo-
<tb> 1 <SEP> lemon yellow <SEP> yellow <SEP> yellow
<tb> acidic <SEP> + <SEP> acetic anhydride
<tb> 1-aminoanthracinone-6-sulfo-
<tb> 2 <SEP> yellow <SEP> yellow <SEP> reddish <SEP> yellow
<tb> acid <SEP> @ xals @ ure
<tb> 1 <SEP> Aminoanthraquinone <SEP> 6-sulfo-
<tb> 3. <SEP> orange-yellow <SEP> yellow <SEP> yellow
<tb> acid <SEP> benzoyl chloride
<tb> 1 <SEP> aminoanthraquinone-ti-sulfo-
<tb> 4. <SEP> orange <SEP> yellow <SEP> greenish <SEP> yellow
<tb> sour <SEP> salicylic acid
<tb> 1 <SEP> aminoanthraquinone-6-sulfo-
<tb> 5.
<SEP> greenish <SEP> yellow <SEP> yellow <SEP> yellow
<tb> acidic <SEP> + <SEP> room acid
<tb> 1-aminoanthraquinone-6-sulto-
<tb> 6. <SEP> yellow <SEP> yellow <SEP> greenish <SEP> yellow
<tb> acidic <SEP> suceinyl chloride.
<tb>
1-AMinoanthraquinone <SEP> 5-sulfo-
<tb> 7. <SEP> greenish <SEP> yellow <SEP> yellow <SEP> orange-yellow
<tb> acidic <SEP> benzoyl chloride.
<tb>
1-Aminoanthraquinone <SEP> 8-sulfo
<tb> 8. <SEP> yellow <SEP> yellow <SEP> yellow
<tb> acid <SEP> benzoyl chloride.
<tb>
1,4-diaminoanthraquinone-6-sulfo
<tb> 9. <SEP> yellow <SEP> red <SEP> red
<tb> acid <SEP> bezoyl chloride
<tb> 1.5 <SEP> diaminoanthraquinone-2.6-
<tb> 10. <SEP> orange-yellow <SEP> orange <SEP> brownish <SEP> yellow
<tb> disulfonic acid <SEP> benzoyl chloride
<tb> 1-Amino-4-methylaminoanthra-
<tb> 11. <SEP> weakly <SEP> colored <SEP> violet <SEP> violet
<tb> quinonsulfonic acid <SEP> - <SEP> acetyl chloride
<tb> 1-Amino-4 <SEP> methylaminoanthra-
<tb> 12. <SEP> quinonsulfonic acid <SEP> + <SEP> Benzoyl- <SEP> weakly <SEP> colored <SEP> violet-blan <SEP> blue-violet
<tb> chloride. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>. <SEP>.
<tb>
1-amino-4-methoxyanthraquinone
<tb> 13. <SEP> orange-red <SEP> orange <SEP> orange
<tb> 7-sulfonic acid <SEP> + <SEP> benzoyl chloride
<tb> 1-Amino <SEP> 4 <SEP> p-tolylaminoanthra-
<tb> 14. <SEP> quinone sulfonic acid <SEP> + <SEP> Benzoyl <SEP> violet <SEP> blan <SEP> blan
<tb> chloride
<tb>
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE45026X | 1909-03-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AT45026B true AT45026B (en) | 1910-11-25 |
Family
ID=5624865
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT45026D AT45026B (en) | 1909-03-16 | 1910-02-05 | Process for the preparation of acidic wool dyes of the anthracene series. |
Country Status (1)
| Country | Link |
|---|---|
| AT (1) | AT45026B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4770183A (en) * | 1986-07-03 | 1988-09-13 | Advanced Magnetics Incorporated | Biologically degradable superparamagnetic particles for use as nuclear magnetic resonance imaging agents |
-
1910
- 1910-02-05 AT AT45026D patent/AT45026B/en active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4770183A (en) * | 1986-07-03 | 1988-09-13 | Advanced Magnetics Incorporated | Biologically degradable superparamagnetic particles for use as nuclear magnetic resonance imaging agents |
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