ATE115548T1 - Verfahren zur herstellung von oxamid. - Google Patents
Verfahren zur herstellung von oxamid.Info
- Publication number
- ATE115548T1 ATE115548T1 AT91901586T AT91901586T ATE115548T1 AT E115548 T1 ATE115548 T1 AT E115548T1 AT 91901586 T AT91901586 T AT 91901586T AT 91901586 T AT91901586 T AT 91901586T AT E115548 T1 ATE115548 T1 AT E115548T1
- Authority
- AT
- Austria
- Prior art keywords
- oxamide
- vessels
- reaction
- solution
- crystallization
- Prior art date
Links
- YIKSCQDJHCMVMK-UHFFFAOYSA-N Oxamide Chemical compound NC(=O)C(N)=O YIKSCQDJHCMVMK-UHFFFAOYSA-N 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 6
- 229910021529 ammonia Inorganic materials 0.000 abstract 3
- 238000002425 crystallisation Methods 0.000 abstract 3
- 230000008025 crystallization Effects 0.000 abstract 3
- LOMVENUNSWAXEN-UHFFFAOYSA-N Methyl oxalate Chemical compound COC(=O)C(=O)OC LOMVENUNSWAXEN-UHFFFAOYSA-N 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 2
- 238000002156 mixing Methods 0.000 abstract 2
- 239000012452 mother liquor Substances 0.000 abstract 2
- 238000010924 continuous production Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Diaphragms For Electromechanical Transducers (AREA)
- Control Of El Displays (AREA)
- Ultra Sonic Daignosis Equipment (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI900105A FI85975C (fi) | 1990-01-09 | 1990-01-09 | Foerfarande foer framstaellning av oxamid. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE115548T1 true ATE115548T1 (de) | 1994-12-15 |
Family
ID=8529662
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT91901586T ATE115548T1 (de) | 1990-01-09 | 1991-01-08 | Verfahren zur herstellung von oxamid. |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0462247B1 (de) |
| AT (1) | ATE115548T1 (de) |
| DE (1) | DE69105828T2 (de) |
| FI (1) | FI85975C (de) |
| WO (1) | WO1991010643A1 (de) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2547127B2 (ja) * | 1991-03-15 | 1996-10-23 | 宇部興産株式会社 | オキサミドの製造法 |
| CN103242188A (zh) * | 2013-05-08 | 2013-08-14 | 天津大学 | 直接合成草酰胺颗粒的方法及装置 |
| CN109134258B (zh) * | 2017-06-28 | 2021-07-30 | 上海浦景化工技术股份有限公司 | 一种草酸二甲酯加氢制乙醇酸甲酯的产品分离工艺 |
| CN110862331B (zh) * | 2019-12-06 | 2021-05-11 | 东华工程科技股份有限公司 | 一种连续生成草酰胺的方法 |
| CN111153823B (zh) * | 2019-12-24 | 2023-05-26 | 上海戊正工程技术有限公司 | 一种草酸二甲酯制备草酰胺的方法 |
| CN115715962B (zh) * | 2022-11-30 | 2025-01-07 | 赛鼎工程有限公司 | 一种用于连续制备草酰胺的装置及方法 |
| CN119455855B (zh) * | 2025-01-16 | 2025-04-18 | 东华工程科技股份有限公司 | 一种生产草酰胺的装置及方法 |
-
1990
- 1990-01-09 FI FI900105A patent/FI85975C/fi not_active IP Right Cessation
-
1991
- 1991-01-08 DE DE69105828T patent/DE69105828T2/de not_active Expired - Fee Related
- 1991-01-08 WO PCT/FI1991/000006 patent/WO1991010643A1/en not_active Ceased
- 1991-01-08 AT AT91901586T patent/ATE115548T1/de not_active IP Right Cessation
- 1991-01-08 EP EP91901586A patent/EP0462247B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FI900105L (fi) | 1991-07-10 |
| FI85975B (fi) | 1992-03-13 |
| DE69105828T2 (de) | 1995-04-27 |
| FI900105A0 (fi) | 1990-01-09 |
| FI85975C (fi) | 1992-06-25 |
| DE69105828D1 (de) | 1995-01-26 |
| EP0462247B1 (de) | 1994-12-14 |
| EP0462247A1 (de) | 1991-12-27 |
| WO1991010643A1 (en) | 1991-07-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |