ATE120196T1 - Verfahren für die zurückgewinnung von trimethoxysilan aus einer mischung von trimethoxysilan und methanol. - Google Patents

Verfahren für die zurückgewinnung von trimethoxysilan aus einer mischung von trimethoxysilan und methanol.

Info

Publication number: ATE120196T1
Authority: AT; Austria
Prior art keywords: trimethoxysilane; recovering; methanol; mixture; extractive
Prior art date: 1987-09-28

Application number

AT88115897T

Other languages

English (en)

Inventor

Thomas Edgeworth Childress

George Michael Omietanski

Frank Dominic Mendicino

Original Assignee

Osi Specialties Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1987-09-28

Filing date

1988-09-27

Publication date

1995-04-15

1988-09-27 Application filed by Osi Specialties Inc filed Critical Osi Specialties Inc

1995-04-15 Application granted granted Critical

1995-04-15 Publication of ATE120196T1 publication Critical patent/ATE120196T1/de

Links

YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 title abstract 3
238000000034 method Methods 0.000 title abstract 2
239000000203 mixture Substances 0.000 title abstract 2
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title 3
PWKQWSBUJOHVID-UHFFFAOYSA-N OC.CO[SiH](OC)OC Chemical compound OC.CO[SiH](OC)OC PWKQWSBUJOHVID-UHFFFAOYSA-N 0.000 abstract 1
238000000895 extractive distillation Methods 0.000 abstract 1
239000002904 solvent Substances 0.000 abstract 1
LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/04—Esters of silicic acids

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Nitrogen Condensed Heterocyclic Rings (AREA)

AT88115897T 1987-09-28 1988-09-27 Verfahren für die zurückgewinnung von trimethoxysilan aus einer mischung von trimethoxysilan und methanol. ATE120196T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US07/101,408 US4761492A (en)	1987-09-28	1987-09-28	Process for recovering trimethoxysilane from a trimethoxysilane and methanol mixture

Publications (1)

Publication Number	Publication Date
ATE120196T1 true ATE120196T1 (de)	1995-04-15

Family

ID=22284495

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT88115897T ATE120196T1 (de)	1987-09-28	1988-09-27	Verfahren für die zurückgewinnung von trimethoxysilan aus einer mischung von trimethoxysilan und methanol.

Country Status (6)

Country	Link
US (1)	US4761492A (de)
EP (1)	EP0310920B1 (de)
AT (1)	ATE120196T1 (de)
BR (1)	BR8804985A (de)
CA (1)	CA1310934C (de)
DE (1)	DE3853394T2 (de)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4999446A (en) *	1990-06-21	1991-03-12	Union Carbide Chemicals And Plastics Company Inc.	Trimethoxysilane preparation via the methanol-silicon reaction with recycle
US5084590A (en) *	1991-06-24	1992-01-28	Union Carbide Chemicals & Plastics Technology Corporation	Trimethoxysilane preparation via the methanol-silicon reaction using a continuous process and multiple reactors
US5166384A (en) *	1992-04-07	1992-11-24	Union Carbide Chemicals & Plastics Technology Corporation	Method for the removal of siloxane dissolved in the solvent employed in the preparation of trimethoxysilane via methanol-silicon metal reaction
US5783720A (en)	1996-10-10	1998-07-21	Osi Specialties, Inc.	Surface-active additives in the direct synthesis of trialkoxysilanes
US6090965A (en) *	1998-04-02	2000-07-18	Osi Specialties, Inc.	Removal of dissolved silicates from alcohol-silicon direct synthesis solvents
DE19947591A1 (de)	1999-10-04	2001-04-12	Basf Ag	Verfahren zur Isolierung von Trimethoxysilan aus einer TMS-Methanol-Mischung
US7858818B2 (en) *	2001-01-31	2010-12-28	Momentive Performance Materials Inc.	Nanosized copper catalyst precursors for the direct synthesis of trialkoxysilanes
US7339068B2 (en)	2001-01-31	2008-03-04	Momentive Performance Materials Inc.	Nanosized copper catalyst precursors for the direct synthesis of trialkoxysilanes
US6580000B1 (en)	2002-06-06	2003-06-17	Ak Research Company	Process for the manufacture of alkoxysilanes and alkoxy orthosilicates
US7652164B2 (en) *	2005-09-13	2010-01-26	Momentive Performance Materials Inc.	Process for the direct synthesis of trialkoxysilane
US7365220B2 (en) *	2005-09-29	2008-04-29	Momentive Performance Materials Inc.	Process for the recovery of alkoxysilanes obtained from the direct reaction of silicon with alkanols
US7645894B2 (en) *	2006-04-22	2010-01-12	Bernard Kanner	Direct process for making cyclic dimethylsiloxane oligomers
US7429672B2 (en) *	2006-06-09	2008-09-30	Momentive Performance Materials Inc.	Process for the direct synthesis of trialkoxysilane
US8153566B2 (en) *	2008-09-30	2012-04-10	Cherron Oronite Company LLC	Lubricating oil compositions
US8901050B2 (en)	2010-03-31	2014-12-02	Chevron Oronite Company Llc	Method for improving copper corrosion performance
US8933001B2 (en)	2010-03-31	2015-01-13	Chevron Oronite Company Llc	Method for improving fluorocarbon elastomer seal compatibility
CN108864169A (zh) *	2018-06-09	2018-11-23	河北晟凯新材料科技有限公司	一种提高异氰酸酯基丙基三乙氧基硅烷收率的方法
KR20260002708A (ko)	2023-04-19	2026-01-06	모멘티브 퍼포먼스 머티리얼즈 인크.	구리-알루미늄 합금 촉매를 이용한 알콕시실란의 직접 합성

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2473260A (en) *	1946-06-26	1949-06-14	Gen Electric	Preparation of tetramethyl silicate
US3072700A (en) *	1959-08-07	1963-01-08	Union Carbide Corp	Process for producing silanes
DE1793222A1 (de) *	1968-08-17	1971-04-15	Dynamit Nobel Ag	Verfahren zur Herstellung von Orthokieselsaeuretetraalkylestern
US3641077A (en) *	1970-09-01	1972-02-08	Eugene G Rochow	Method for preparing alkoxy derivatives of silicon germanium tin thallium and arsenic
US3803197A (en) *	1971-05-04	1974-04-09	Anderson Dev Co	Method of preparation of alkyl and 2-alkoxy-ethyl silicates
BE789535A (fr) *	1971-09-30	1973-01-15	Tokyo Shibaura Electric Co	Procede de fabrication d'alkoxysilanes
US4185029A (en) *	1975-07-19	1980-01-22	Dynamit Nobel Aktiengesellschaft	Method of preparing orthosilicic acid alkyl esters
FR2318872A1 (fr) *	1975-07-19	1977-02-18	Dynamit Nobel Ag	Procede pou l'obtention d'esters alkyliques d'acide orthosilicique
JPS54163529A (en) *	1978-06-13	1979-12-26	Mitsubishi Chem Ind	Production of alkoxysilane
JPS552641A (en) *	1978-06-21	1980-01-10	Mitsubishi Chem Ind Ltd	Preparation of alkoxysilane
JPS5528928A (en) *	1978-08-21	1980-02-29	Mitsubishi Chem Ind Ltd	Preparation of methoxysilane
JPS5528929A (en) *	1978-08-21	1980-02-29	Mitsubishi Chem Ind Ltd	Preparation of ethoxysilane
JPS5533457A (en) *	1978-09-01	1980-03-08	Mitsubishi Chem Ind Ltd	Preparation of trialkoxysilane
JPS5572198A (en) *	1978-11-27	1980-05-30	Mitsubishi Chem Ind Ltd	Stabilization of trimethoxysilane
JPS5572197A (en) *	1978-11-27	1980-05-30	Mitsubishi Chem Ind Ltd	Stabilization of trimethoxysilane
JPS5584348A (en) *	1978-12-20	1980-06-25	Matsushita Electric Ind Co Ltd	Flame-retardant acetal resin composition
JPS5616492A (en) *	1979-07-20	1981-02-17	Mitsubishi Chem Ind Ltd	Preparation of tetraalkoxysilane
US4288604A (en) *	1980-05-19	1981-09-08	Stauffer Chemical Company	Method for the production of tetraalkyl silicates
US4289889A (en) *	1980-06-30	1981-09-15	Union Carbide Corporation	Preparation of tetraalkoxysilanes
US4323690A (en) *	1981-04-20	1982-04-06	Carboline Company	Method of making silicate esters
US4402797A (en) *	1982-09-20	1983-09-06	Dow Corning Corporation	Separation of chlorosilanes by extractive distillation
US4447632A (en) *	1983-04-18	1984-05-08	Union Carbide Corporation	Process for production of alkyl silicates from silicon metal
US4487949A (en) *	1983-11-22	1984-12-11	Union Carbide Corporation	Process for the preparation of alkyl silicates
JPS62114992A (ja) *	1985-11-14	1987-05-26	Toray Silicone Co Ltd	アルコキシシランの精製方法
US4727173A (en) *	1987-03-31	1988-02-23	Union Carbide Corporation	Process for producing trialkoxysilanes from the reaction of silicon metal and alcohol
US4911740A (en) *	1988-08-02	1990-03-27	Schieder Hans B	Pressure responsive valve in a temperature changing device

1987
- 1987-09-28 US US07/101,408 patent/US4761492A/en not_active Expired - Lifetime
1988
- 1988-09-27 BR BR8804985A patent/BR8804985A/pt not_active Application Discontinuation
- 1988-09-27 CA CA000578577A patent/CA1310934C/en not_active Expired - Lifetime
- 1988-09-27 EP EP88115897A patent/EP0310920B1/de not_active Expired - Lifetime
- 1988-09-27 AT AT88115897T patent/ATE120196T1/de active
- 1988-09-27 DE DE3853394T patent/DE3853394T2/de not_active Expired - Lifetime

Also Published As

Publication number	Publication date
EP0310920B1 (de)	1995-03-22
EP0310920A3 (en)	1990-08-22
BR8804985A (pt)	1989-05-02
CA1310934C (en)	1992-12-01
EP0310920A2 (de)	1989-04-12
US4761492A (en)	1988-08-02
DE3853394D1 (de)	1995-04-27
DE3853394T2 (de)	1995-07-27

Similar Documents

Publication	Publication Date	Title
ATE120196T1 (de)	1995-04-15	Verfahren für die zurückgewinnung von trimethoxysilan aus einer mischung von trimethoxysilan und methanol.
DE3580803D1 (de)	1991-01-17	Neue zwischenprodukte und verfahren zur herstellung von 3-acylamino-1-hydroxy-2-azetidinonen.
DE3773523D1 (de)	1991-11-14	Verfahren zum abscheiden von kohlenstoffmonoxid konstanter reinheit.
DE69328029D1 (de)	2000-04-13	Verfahren zur herstellung von hochreinem benzol durch extraktivdestillation
DE3789120D1 (de)	1994-03-31	Verfahren zur Trennung der Komponenten eines Flüssigkeitsgemisches voneinander.
DE58909847D1 (de)	1999-03-11	Verfahren zur Herstellung von Diorganodialkoxysilanen
ATE66447T1 (de)	1991-09-15	Verfahren zur gewinnung von 1,3-butadien.
ATE113057T1 (de)	1994-11-15	Verfahren zum destillativen abtrennen von alkoholen.
DE3582000D1 (de)	1991-04-11	Verfahren zur herstellung von kohlenwasserstoffenmischungen.
DE3854948D1 (de)	1996-03-14	Verfahren zur Herstellung von organobimetallischen Verbindungen
ATE150744T1 (de)	1997-04-15	Verfahren zur entfernung olefinischer verunreinigungen aus 1,1,1,2,3,3,3 - heptafluorpropan
AT388556B (de)	1989-07-25	Stereogesteuertes verfahren zur herstellung von neuen penem-verbindungen
DE59002673D1 (de)	1993-10-21	Verfahren zur Aufarbeitung des Raffinates einer Extraktivdestillation von Kohlenwasserstoffgemischen.
ATA71379A (de)	1980-07-15	Verfahren zur herstellung von neuen 9-substi- tuierten adeninen
AT365622B (de)	1982-02-10	Verfahren zur herstellung von klebemitteln
ATA221292A (de)	1995-05-15	Neues verfahren zur herstellung von 3-vinylcephalosporinverbindungen
ATA817779A (de)	1984-04-15	Verfahren zur herstellung von 7-chlor-2-methyl-3,3a-dihydro-2h,9h-isoxazol (3,2-b) (1,3)-benzoxazin-9-on
AT368508B (de)	1982-10-25	Verfahren zur herstellung von 3-carbamoyloxymethylcephalosporinverbindungen
IT1088100B (it)	1985-06-04	Processo per l'idrogenazione di bis(2-cianoetossi)composti
AT369758B (de)	1983-01-25	Verfahren zur herstellung von alkenungesaettigten oligourethanen
ATE9477T1 (de)	1984-10-15	Verfahren zur herstellung von 1,1'-diacetalen.
ATE6933T1 (de)	1984-04-15	Verfahren zur herstellung von 4aminobutters[ureamid.
ATE26254T1 (de)	1987-04-15	Verfahren zur herstellung von 2,2,2 trifluoraethanol.
AT357547B (de)	1980-07-10	Verfahren zur herstellung von 3-phenyl- pyridazon-(6)
AT373244B (de)	1983-12-27	Verfahren zur herstellung von n-tritylimidazolverbindungen