ATE143652T1 - Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmedium - Google Patents
Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmediumInfo
- Publication number
- ATE143652T1 ATE143652T1 AT92925310T AT92925310T ATE143652T1 AT E143652 T1 ATE143652 T1 AT E143652T1 AT 92925310 T AT92925310 T AT 92925310T AT 92925310 T AT92925310 T AT 92925310T AT E143652 T1 ATE143652 T1 AT E143652T1
- Authority
- AT
- Austria
- Prior art keywords
- growth medium
- fluordic
- crystalline microporous
- essentially non
- microporous solids
- Prior art date
Links
- 239000007787 solid Substances 0.000 title abstract 4
- 239000001963 growth medium Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 4
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000000377 silicon dioxide Substances 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 1
- 239000012736 aqueous medium Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 abstract 1
- 239000002808 molecular sieve Substances 0.000 abstract 1
- -1 nitrogen-containing organic base Chemical class 0.000 abstract 1
- 235000015097 nutrients Nutrition 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
- C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/44—Ferrierite type, e.g. types ZSM-21, ZSM-35 or ZSM-38
- C01B39/445—Ferrierite type, e.g. types ZSM-21, ZSM-35 or ZSM-38 using at least one organic template directing agent
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US79535491A | 1991-11-20 | 1991-11-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE143652T1 true ATE143652T1 (de) | 1996-10-15 |
Family
ID=25165320
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT92925310T ATE143652T1 (de) | 1991-11-20 | 1992-11-13 | Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmedium |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5320822A (de) |
| EP (1) | EP0613450B1 (de) |
| JP (1) | JPH07503693A (de) |
| AT (1) | ATE143652T1 (de) |
| DE (1) | DE69214294T2 (de) |
| WO (1) | WO1993010044A1 (de) |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6042797A (en) | 1997-07-02 | 2000-03-28 | Tosoh Corporation | Adsorbent for ethylene, method for adsorbing and removing ethylene and method for purifying an exhaust gas |
| US5545394A (en) * | 1993-08-10 | 1996-08-13 | The State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of The University Of Oregon | Complexation-mediated crystal-forming reactions using complexing agents |
| US5853691A (en) * | 1993-08-10 | 1998-12-29 | State Of Oregon Acting By And Through The Oregon State Board Of Higher Education On The Behalf Of The University Of Oregon | Silver halides of altered crystal habit or morphology and methods for producing same |
| US5853686A (en) * | 1993-08-10 | 1998-12-29 | State Of Oregon Acting By And Through The Oregon State Board Of Higher Education On Behalf Of The University Of Oregon | Calcium carbonates of altered crystal habit or morphology and methods for producing same |
| DE4407872C2 (de) * | 1994-03-04 | 2003-10-23 | Alsi Penta Zeolithe Gmbh | Verfahren zur Herstellung von hochsiliciumhaltigen Zeolithen |
| CN1147800A (zh) * | 1994-05-10 | 1997-04-16 | 国际壳牌研究有限公司 | 制备大孔分子筛的方法 |
| US5599520A (en) * | 1994-11-03 | 1997-02-04 | Garces; Juan M. | Synthesis of crystalline porous solids in ammonia |
| TW380133B (en) * | 1995-06-07 | 2000-01-21 | Shell Oil Co | Process for preparing ferrierite |
| US5840271A (en) * | 1996-02-09 | 1998-11-24 | Intevep, S.A. | Synthetic material with high void volume associated with mesoporous tortuous channels having a narrow size distribution |
| US5800799A (en) * | 1996-05-02 | 1998-09-01 | Board Of Trustees Operating Michigan State University | Porous inorganic oxide materials prepared by non-ionic surfactant and fluoride ion |
| US5849258A (en) * | 1996-06-06 | 1998-12-15 | Intevep, S.A. | Material with microporous crystalline walls defining a narrow size distribution of mesopores, and process for preparing same |
| US5688484A (en) * | 1996-07-29 | 1997-11-18 | Arco Chemical Technology, L.P. | Non-hydrothermal method of making a titanium-containing zeolite |
| US5716593A (en) * | 1996-07-31 | 1998-02-10 | Chevron U.S.A. Inc. | Preparation of Y-type faujasite using an organic template |
| US6071614A (en) * | 1997-07-14 | 2000-06-06 | 3M Innovative Properties Company | Microporous fluorinated silica agglomerate and method of preparing and using same |
| US6521198B2 (en) | 2000-05-17 | 2003-02-18 | The Regents Of The University Of California | Metal surfaces coated with molecular sieve for corrosion resistance |
| US6284926B1 (en) | 2000-06-06 | 2001-09-04 | Richmond, Hitchcock, Fish & Dollar | Process and apparatus for producing organic polysulfides |
| US6723421B2 (en) * | 2001-10-05 | 2004-04-20 | Energy Conversion Devices, Inc. | Semiconductor with coordinatively irregular structures |
| US20050100494A1 (en) * | 2003-11-06 | 2005-05-12 | George Yaluris | Ferrierite compositions for reducing NOx emissions during fluid catalytic cracking |
| US20050100493A1 (en) * | 2003-11-06 | 2005-05-12 | George Yaluris | Ferrierite compositions for reducing NOx emissions during fluid catalytic cracking |
| US7985400B2 (en) * | 2004-01-26 | 2011-07-26 | Lummus Technology Inc. | Method for making mesoporous or combined mesoporous and microporous inorganic oxides |
| US20050232839A1 (en) | 2004-04-15 | 2005-10-20 | George Yaluris | Compositions and processes for reducing NOx emissions during fluid catalytic cracking |
| US7304011B2 (en) * | 2004-04-15 | 2007-12-04 | W.R. Grace & Co. -Conn. | Compositions and processes for reducing NOx emissions during fluid catalytic cracking |
| EP1661859A1 (de) * | 2004-11-26 | 2006-05-31 | Total France | Zeolitenzusammensetzungen sowie Verfahren zu derer Herstellung; Verwendung dergleichen |
| BRPI0610326B1 (pt) | 2005-04-27 | 2015-07-21 | W. R. Grace & Co.- Conn | Composições e processos para reduzir emissões de nox durante o craqueamento catalítico de fluído. |
| ES2304308B1 (es) * | 2007-03-23 | 2009-08-07 | Consejo Superior Investg.Cientificas | Procedimiento de preparacion de un aluminosilicato con estructura tipo ferrierita a partir de geles que contienen tetrametilamonio y bencil-metilpirrolidinio,y sus aplicaciones. |
| US20130005564A1 (en) * | 2011-06-30 | 2013-01-03 | Uop Llc | Synthesis of crystalline long-ranged ordered materials from preformed amorphous solids |
| CN104159849B (zh) | 2012-02-21 | 2017-01-11 | 埃克森美孚化学专利公司 | 分子筛材料,其合成及用途 |
| CN102627288B (zh) * | 2012-04-23 | 2013-07-24 | 大连多相触媒有限公司 | 一种fer拓扑结构分子筛的制备方法 |
| US9156706B2 (en) * | 2012-07-03 | 2015-10-13 | Chevron U.S.A. Inc. | Method for preparing high-silica LEV-type zeolites |
| CN103933871B (zh) * | 2014-04-15 | 2016-02-10 | 南京工业大学 | 一种高稳定性全硅mfi型分子筛膜的制备方法 |
| CN110759357B (zh) * | 2018-07-25 | 2021-08-27 | 中国石油天然气股份有限公司 | 一种zsm-35/zsm-5共晶分子筛的合成方法 |
| CN112939003B (zh) * | 2021-02-11 | 2022-10-14 | 贵州大学 | 一种利用含氟硅渣制备sba-15分子筛并回收氟的方法 |
| US11180376B1 (en) * | 2021-03-19 | 2021-11-23 | Chevron U.S.A. Inc. | Synthesis of zeolites having the ferrierite structure |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4073865A (en) * | 1976-09-27 | 1978-02-14 | Union Carbide Corporation | Silica polymorph and process for preparing same |
| US4375458A (en) * | 1977-08-17 | 1983-03-01 | Mobil Oil Corporation | Synthesis of large crystallite zeolites |
| US4296083A (en) * | 1977-04-22 | 1981-10-20 | Mobil Oil Corporation | Zeolite synthesis |
| US4650656A (en) * | 1977-05-25 | 1987-03-17 | Mobil Oil Corporation | Large crystal ZSM-5 from template addition to the gel |
| DK84884A (da) * | 1983-03-07 | 1984-09-08 | Res Ass Petroleum Alternat Dev | Krystallinsk aluminiumsilicat og fremgangsmaade til fremstilling deraf |
| GB8321849D0 (en) * | 1983-08-13 | 1983-09-14 | British Petroleum Co Plc | Crystalline silicates |
| US4673559A (en) * | 1983-12-19 | 1987-06-16 | Mobil Oil Corporation | Silicoaluminophosphate crystallization using hydrolysis |
| US4664897A (en) * | 1983-12-19 | 1987-05-12 | Mobil Oil Corporation | Crystalline silicophosphoaluminate MCM-4 |
| US4639357A (en) * | 1983-12-19 | 1987-01-27 | Mobil Oil Corporation | Crystalline silicophosphoaluminate MCM-5 |
| US4647442A (en) * | 1983-12-19 | 1987-03-03 | Mobil Oil Corporation | Crystalline silicophosphoaluminate from a two phase medium |
| US4713227A (en) * | 1983-12-19 | 1987-12-15 | Mobil Oil Corporation | Method for the synthesis of metallophosphoaluminates |
| US4705675A (en) * | 1984-11-16 | 1987-11-10 | The Standard Oil Company | Synthesis of molecular sieving metallosilicates using silica-transition metal oxide sols |
| GB2167052B (en) * | 1984-11-17 | 1988-09-07 | Laporte Industries Ltd | Synthetic crystalline molecular sieve materials and a method for their preparation |
| US4795623A (en) * | 1986-08-05 | 1989-01-03 | Shell Oil Company | Time effective method for preparing ferrierite |
| US4942027A (en) * | 1986-08-05 | 1990-07-17 | Shell Oil Company | Method for preparing ferrierite |
| FR2607128B1 (fr) * | 1986-11-21 | 1989-04-28 | Inst Francais Du Petrole | Nouvelles ferrierites, leur procede de preparation et leur utilisation |
| FR2619319B1 (fr) * | 1987-08-14 | 1990-01-12 | Inst Francais Du Petrole | Catalyseur du type aluminosilicate renfermant au moins un metal noble et son utilisation en isomerisation d'une coupe c8 aromatique |
| CN1006696B (zh) * | 1988-01-18 | 1990-02-07 | 太原工业大学 | 非水体系中丝光沸石的合成方法 |
| DE3812592A1 (de) * | 1988-04-15 | 1989-10-26 | Deggendorfer Werft Eisenbau | Verfahren zur herstellung von zeolithen |
| FR2631621B1 (fr) * | 1988-05-19 | 1990-09-07 | Inst Francais Du Petrole | Nouvelles zeolithes de type structural ton, leur preparation et leur utilisation |
| FR2632943B1 (fr) * | 1988-06-15 | 1990-09-28 | Inst Francais Du Petrole | Nouveau procede de synthese de zeolites de type structural mtt |
| FR2652347B1 (fr) * | 1989-09-22 | 1992-01-10 | Inst Francais Du Petrole | Zeolithe de type beta et son procede de preparation invention de philippe caullet, jean-louis guth, anne-catherine faust, francis raatz, jean-francois joly et jean-marie deves. |
-
1992
- 1992-11-13 DE DE69214294T patent/DE69214294T2/de not_active Expired - Fee Related
- 1992-11-13 WO PCT/US1992/009947 patent/WO1993010044A1/en not_active Ceased
- 1992-11-13 AT AT92925310T patent/ATE143652T1/de not_active IP Right Cessation
- 1992-11-13 EP EP92925310A patent/EP0613450B1/de not_active Expired - Lifetime
- 1992-11-13 JP JP5509497A patent/JPH07503693A/ja active Pending
-
1993
- 1993-01-29 US US08/011,059 patent/US5320822A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| WO1993010044A1 (en) | 1993-05-27 |
| EP0613450A1 (de) | 1994-09-07 |
| DE69214294D1 (de) | 1996-11-07 |
| DE69214294T2 (de) | 1997-02-27 |
| EP0613450B1 (de) | 1996-10-02 |
| US5320822A (en) | 1994-06-14 |
| JPH07503693A (ja) | 1995-04-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |