ATE143652T1 - Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmedium - Google Patents

Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmedium

Info

Publication number: ATE143652T1
Authority: AT; Austria
Prior art keywords: growth medium; fluordic; crystalline microporous; essentially non; microporous solids
Prior art date: 1991-11-20

Application number

AT92925310T

Other languages

English (en)

Inventor

Geoffrey A Ozin

Alex Kuperman

Susan Nadimi

Original Assignee

Dow Chemical Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1991-11-20

Filing date

1992-11-13

Publication date

1996-10-15

1992-11-13 Application filed by Dow Chemical Co filed Critical Dow Chemical Co

1996-10-15 Application granted granted Critical

1996-10-15 Publication of ATE143652T1 publication Critical patent/ATE143652T1/de

Links

239000007787 solid Substances 0.000 title abstract 4
239000001963 growth medium Substances 0.000 title abstract 2
238000000034 method Methods 0.000 title abstract 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 4
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
239000000203 mixture Substances 0.000 abstract 2
239000000377 silicon dioxide Substances 0.000 abstract 2
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 1
KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
229910000323 aluminium silicate Inorganic materials 0.000 abstract 1
239000012736 aqueous medium Substances 0.000 abstract 1
239000003795 chemical substances by application Substances 0.000 abstract 1
239000013078 crystal Substances 0.000 abstract 1
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
238000010438 heat treatment Methods 0.000 abstract 1
229910000040 hydrogen fluoride Inorganic materials 0.000 abstract 1
239000002808 molecular sieve Substances 0.000 abstract 1
-1 nitrogen-containing organic base Chemical class 0.000 abstract 1
235000015097 nutrients Nutrition 0.000 abstract 1
239000003960 organic solvent Substances 0.000 abstract 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 1
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
239000010457 zeolite Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
- C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/44—Ferrierite type, e.g. types ZSM-21, ZSM-35 or ZSM-38
- C01B39/445—Ferrierite type, e.g. types ZSM-21, ZSM-35 or ZSM-38 using at least one organic template directing agent

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
General Life Sciences & Earth Sciences (AREA)
Geology (AREA)
Inorganic Chemistry (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Materials Engineering (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

AT92925310T 1991-11-20 1992-11-13 Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmedium ATE143652T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US79535491A	1991-11-20	1991-11-20

Publications (1)

Publication Number	Publication Date
ATE143652T1 true ATE143652T1 (de)	1996-10-15

Family

ID=25165320

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT92925310T ATE143652T1 (de)	1991-11-20	1992-11-13	Verfahren zur züchtung von kristallinen, mikroporösen feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen wachstumsmedium

Country Status (6)

Country	Link
US (1)	US5320822A (de)
EP (1)	EP0613450B1 (de)
JP (1)	JPH07503693A (de)
AT (1)	ATE143652T1 (de)
DE (1)	DE69214294T2 (de)
WO (1)	WO1993010044A1 (de)

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US5853691A (en) *	1993-08-10	1998-12-29	State Of Oregon Acting By And Through The Oregon State Board Of Higher Education On The Behalf Of The University Of Oregon	Silver halides of altered crystal habit or morphology and methods for producing same
US5853686A (en) *	1993-08-10	1998-12-29	State Of Oregon Acting By And Through The Oregon State Board Of Higher Education On Behalf Of The University Of Oregon	Calcium carbonates of altered crystal habit or morphology and methods for producing same
US5545394A (en) *	1993-08-10	1996-08-13	The State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of The University Of Oregon	Complexation-mediated crystal-forming reactions using complexing agents
DE4407872C2 (de) *	1994-03-04	2003-10-23	Alsi Penta Zeolithe Gmbh	Verfahren zur Herstellung von hochsiliciumhaltigen Zeolithen
WO1995030625A1 (en) *	1994-05-10	1995-11-16	Shell Internationale Research Maatschappij B.V.	Process for preparing a large pore molecular sieve
US5599520A (en) *	1994-11-03	1997-02-04	Garces; Juan M.	Synthesis of crystalline porous solids in ammonia
IN192774B (de) *	1995-06-07	2004-05-15	Sheel Oil Company
US5840271A (en) *	1996-02-09	1998-11-24	Intevep, S.A.	Synthetic material with high void volume associated with mesoporous tortuous channels having a narrow size distribution
US5800799A (en) *	1996-05-02	1998-09-01	Board Of Trustees Operating Michigan State University	Porous inorganic oxide materials prepared by non-ionic surfactant and fluoride ion
US5849258A (en) *	1996-06-06	1998-12-15	Intevep, S.A.	Material with microporous crystalline walls defining a narrow size distribution of mesopores, and process for preparing same
US5688484A (en) *	1996-07-29	1997-11-18	Arco Chemical Technology, L.P.	Non-hydrothermal method of making a titanium-containing zeolite
US5716593A (en) *	1996-07-31	1998-02-10	Chevron U.S.A. Inc.	Preparation of Y-type faujasite using an organic template
US6071614A (en) *	1997-07-14	2000-06-06	3M Innovative Properties Company	Microporous fluorinated silica agglomerate and method of preparing and using same
US6521198B2 (en)	2000-05-17	2003-02-18	The Regents Of The University Of California	Metal surfaces coated with molecular sieve for corrosion resistance
US6284926B1 (en)	2000-06-06	2001-09-04	Richmond, Hitchcock, Fish & Dollar	Process and apparatus for producing organic polysulfides
US6723421B2 (en) *	2001-10-05	2004-04-20	Energy Conversion Devices, Inc.	Semiconductor with coordinatively irregular structures
US20050100493A1 (en) *	2003-11-06	2005-05-12	George Yaluris	Ferrierite compositions for reducing NOx emissions during fluid catalytic cracking
US20050100494A1 (en)	2003-11-06	2005-05-12	George Yaluris	Ferrierite compositions for reducing NOx emissions during fluid catalytic cracking
US7985400B2 (en) *	2004-01-26	2011-07-26	Lummus Technology Inc.	Method for making mesoporous or combined mesoporous and microporous inorganic oxides
US7304011B2 (en) *	2004-04-15	2007-12-04	W.R. Grace & Co. -Conn.	Compositions and processes for reducing NOx emissions during fluid catalytic cracking
US20050232839A1 (en)	2004-04-15	2005-10-20	George Yaluris	Compositions and processes for reducing NOx emissions during fluid catalytic cracking
EP1661859A1 (de) *	2004-11-26	2006-05-31	Total France	Zeolitenzusammensetzungen sowie Verfahren zu derer Herstellung; Verwendung dergleichen
KR101382014B1 (ko)	2005-04-27	2014-04-04	더블유.알. 그레이스 앤드 캄파니-콘.	유동상 접촉 분해 중의 ＮＯｘ 방출 감소를 위한 조성물 및공정
ES2304308B1 (es) *	2007-03-23	2009-08-07	Consejo Superior Investg.Cientificas	Procedimiento de preparacion de un aluminosilicato con estructura tipo ferrierita a partir de geles que contienen tetrametilamonio y bencil-metilpirrolidinio,y sus aplicaciones.
US20130005564A1 (en) *	2011-06-30	2013-01-03	Uop Llc	Synthesis of crystalline long-ranged ordered materials from preformed amorphous solids
EP2817262B1 (de) *	2012-02-21	2017-11-15	ExxonMobil Chemical Patents Inc.	Molekulares siebmaterial, synthese und verwendung davon
CN102627288B (zh) *	2012-04-23	2013-07-24	大连多相触媒有限公司	一种fer拓扑结构分子筛的制备方法
US9156706B2 (en) *	2012-07-03	2015-10-13	Chevron U.S.A. Inc.	Method for preparing high-silica LEV-type zeolites
CN103933871B (zh) *	2014-04-15	2016-02-10	南京工业大学	一种高稳定性全硅mfi型分子筛膜的制备方法
CN110759357B (zh) *	2018-07-25	2021-08-27	中国石油天然气股份有限公司	一种zsm-35/zsm-5共晶分子筛的合成方法
CN112939003B (zh) *	2021-02-11	2022-10-14	贵州大学	一种利用含氟硅渣制备sba-15分子筛并回收氟的方法
US11180376B1 (en) *	2021-03-19	2021-11-23	Chevron U.S.A. Inc.	Synthesis of zeolites having the ferrierite structure

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US4073865A (en) *	1976-09-27	1978-02-14	Union Carbide Corporation	Silica polymorph and process for preparing same
US4375458A (en) *	1977-08-17	1983-03-01	Mobil Oil Corporation	Synthesis of large crystallite zeolites
US4296083A (en) *	1977-04-22	1981-10-20	Mobil Oil Corporation	Zeolite synthesis
US4650656A (en) *	1977-05-25	1987-03-17	Mobil Oil Corporation	Large crystal ZSM-5 from template addition to the gel
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US4647442A (en) *	1983-12-19	1987-03-03	Mobil Oil Corporation	Crystalline silicophosphoaluminate from a two phase medium
US4664897A (en) *	1983-12-19	1987-05-12	Mobil Oil Corporation	Crystalline silicophosphoaluminate MCM-4
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US4705675A (en) *	1984-11-16	1987-11-10	The Standard Oil Company	Synthesis of molecular sieving metallosilicates using silica-transition metal oxide sols
GB2167052B (en) *	1984-11-17	1988-09-07	Laporte Industries Ltd	Synthetic crystalline molecular sieve materials and a method for their preparation
US4795623A (en) *	1986-08-05	1989-01-03	Shell Oil Company	Time effective method for preparing ferrierite
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FR2607128B1 (fr) *	1986-11-21	1989-04-28	Inst Francais Du Petrole	Nouvelles ferrierites, leur procede de preparation et leur utilisation
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FR2631621B1 (fr) *	1988-05-19	1990-09-07	Inst Francais Du Petrole	Nouvelles zeolithes de type structural ton, leur preparation et leur utilisation
FR2632943B1 (fr) *	1988-06-15	1990-09-28	Inst Francais Du Petrole	Nouveau procede de synthese de zeolites de type structural mtt
FR2652347B1 (fr) *	1989-09-22	1992-01-10	Inst Francais Du Petrole	Zeolithe de type beta et son procede de preparation invention de philippe caullet, jean-louis guth, anne-catherine faust, francis raatz, jean-francois joly et jean-marie deves.

1992
- 1992-11-13 DE DE69214294T patent/DE69214294T2/de not_active Expired - Fee Related
- 1992-11-13 AT AT92925310T patent/ATE143652T1/de not_active IP Right Cessation
- 1992-11-13 WO PCT/US1992/009947 patent/WO1993010044A1/en not_active Ceased
- 1992-11-13 JP JP5509497A patent/JPH07503693A/ja active Pending
- 1992-11-13 EP EP92925310A patent/EP0613450B1/de not_active Expired - Lifetime
1993
- 1993-01-29 US US08/011,059 patent/US5320822A/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
DE69214294D1 (de)	1996-11-07
EP0613450A1 (de)	1994-09-07
US5320822A (en)	1994-06-14
EP0613450B1 (de)	1996-10-02
DE69214294T2 (de)	1997-02-27
JPH07503693A (ja)	1995-04-20
WO1993010044A1 (en)	1993-05-27

Legal Events

Date	Code	Title	Description
1997-04-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties

Publication	Publication Date	Title
DE69214294D1 (de)	1996-11-07	Verfahren zur Züchtung von Kristallinen, mikroporösen Feststoffen in einem fluordaufweisenden, wesentlich nichtwässrigen Wachstumsmedium
DE69204850D1 (de)	1995-10-19	Verfahren zur herstellung von gleichmaessigen zeolithkristallen des mfi-typs.
DE69104864D1 (de)	1994-12-08	Verfahren zur gesteuerten Züchtung von nadelförmigen Kristallen und ihre Verwendung zur Herstellung spitzenförmiger Mikrokathoden.
ATE141186T1 (de)	1996-08-15	Verfahren zum züchten von gemischten zeolithen auf einem substrat
DE69508801D1 (de)	1999-05-12	Verfahren zur Kristallzüchtung von III-V Halbleiterverbindungen
DE3689196D1 (de)	1993-12-02	Verfahren zur Herstellung von Amiden unter Verwendung von Mikroorganismen.
DE69123944D1 (de)	1997-02-13	Verfahren zur Herstellung von Hydrogengas unter Verwendung von Mikroorganismen
GB8805478D0 (en)	1988-04-07	Method & apparatus for growing semi-conductor crystalline materials
DE3881478D1 (de)	1993-07-08	Substituierte carbonsaeure-derivate, verfahren zu ihrer herstellung und diese enthaltende fungizide fuer acker- und gartenbau.
DE69924137D1 (de)	2005-04-14	Verfahren zur herstellung einer übersättigten kalziumphosphatlösung und dünner film aus kalziumphosphatkristallen unter verwendung derselben
FI972315L (fi)	1997-05-30	Menetelmä ja laite piikarbidi-yksikiteiden valmistamiseksi sublimaatiokasvatuksen avulla
DE69022743D1 (de)	1995-11-02	Verfahren zur hydrothermalen herstellung von einkristallen mit optischer qualität.
DE3575136D1 (de)	1990-02-08	Cyclohexenonderivate, verfahren zu ihrer herstellung und ihre verwendung zur bekaempfung unerwuenschten pflanzenwuchses.
DE60114860D1 (de)	2005-12-15	Verfahren zur herstellung von aufgereinigtem anthocyanin und kristallines anthocyanin
DE3881064D1 (de)	1993-06-24	Verfahren zur herstellung von kristallinen komplexen perovskit-verbindungen.
DE3878382D1 (de)	1993-03-25	Verfahren zur herstellung von isomerisierten hopfenpellets.
DE58901829D1 (de)	1992-08-20	Verfahren zur herstellung von zeolithen.
ATE128447T1 (de)	1995-10-15	Verfahren zur herstellung von äthanderivaten.
DE3853084D1 (de)	1995-03-23	Verfahren und vorrichtung zur züchtung von kristallen nach der czochralski-methode.
DE3686612D1 (de)	1992-10-08	Verfahren zur herstellung von einkristallen aus kalziumkarbonat.
ATE168720T1 (de)	1998-08-15	Sukrosephosphatsynthase (sps), verfahren zu ihrer herstellung, ihre c-dns, und verwendung der c-dns zur modifizierung der sps-expression in pflanzenzellen
DE68919688D1 (de)	1995-01-12	Verfahren zur kristallisation von subtilisin.
DE3482971D1 (de)	1990-09-20	Landwirtschaftliche zusammensetzungen, verfahren zur herstellung von landwirtschaftlichen zusammensetzungen und verfahren zur verwendung von landwirtschaftlichen zusammensetzungen.
IL72217A0 (en)	1984-10-31	Compositions containing certain benzamide derivatives and method for regulating plant growth,some such novel compounds and their preparation
DE3869383D1 (de)	1992-04-23	Verfahren um hortensien das ganze jahr zum bluehen zu bringen.