ATE148102T1 - Verfahren zur reinigung von acetonitril - Google Patents
Verfahren zur reinigung von acetonitrilInfo
- Publication number
- ATE148102T1 ATE148102T1 AT93913980T AT93913980T ATE148102T1 AT E148102 T1 ATE148102 T1 AT E148102T1 AT 93913980 T AT93913980 T AT 93913980T AT 93913980 T AT93913980 T AT 93913980T AT E148102 T1 ATE148102 T1 AT E148102T1
- Authority
- AT
- Austria
- Prior art keywords
- acetonitrile
- acetonetrile
- purifying
- ozone
- treatment
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 9
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000003610 charcoal Substances 0.000 abstract 1
- 239000002808 molecular sieve Substances 0.000 abstract 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/32—Separation; Purification; Stabilisation; Use of additives
- C07C253/34—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Steroid Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US88674592A | 1992-05-21 | 1992-05-21 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE148102T1 true ATE148102T1 (de) | 1997-02-15 |
Family
ID=25389676
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT93913980T ATE148102T1 (de) | 1992-05-21 | 1993-05-18 | Verfahren zur reinigung von acetonitril |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5292919A (de) |
| EP (1) | EP0641314B1 (de) |
| AT (1) | ATE148102T1 (de) |
| CA (1) | CA2136235C (de) |
| DE (1) | DE69307701T2 (de) |
| WO (1) | WO1993023366A1 (de) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5426208A (en) * | 1992-05-21 | 1995-06-20 | Cryodyne Technologies, Inc. | Method of purification of acetonitrile |
| DE4397378T1 (de) * | 1993-05-14 | 1995-05-11 | Asahi Chemical Ind | Hochgereinigtes Acetonitril und Verfahren zur Reinigung von rohem Acetonitril |
| KR0171245B1 (ko) * | 1993-05-14 | 1999-03-30 | 유미꾸라 레이이찌 | 고 순도 아세토니트릴 및 미정제 아세토니트릴의 정제 방법 |
| WO1994026698A1 (fr) * | 1993-05-14 | 1994-11-24 | Asahi Kasei Kogyo Kabushiki Kaisha | Acetonitrile de grande purete et purification d'acetonitrile brut |
| US5629443A (en) * | 1993-05-14 | 1997-05-13 | Asahi Kasei Kogyo Kabushiki Kaisha | Highly purified acetonitrile and process for purifying crude acetonitrile |
| US5440068A (en) * | 1993-12-30 | 1995-08-08 | The Standard Oil Company | Acetonitrile purification via an adsorption-based process |
| ES2131269T3 (es) * | 1995-01-25 | 1999-07-16 | Standard Oil Co Ohio | Purificacion de acetonitrilo por medio de un proceso basado en la adsorcion. |
| ZA95629B (en) * | 1995-01-26 | 1995-10-05 | Standard Oil Co Ohio | Acetonitrile purification via an adsorption-based process |
| RU2149867C1 (ru) * | 1995-03-13 | 2000-05-27 | Дзе Стэндард Оил Компани | Способ очистки ацетонитрила |
| TR28966A (tr) * | 1995-03-14 | 1997-07-21 | Standard Oil Co Ohio | Adsorpsiyona dayali islem vasitasiyla asetonitrilin saflastirilmasi. |
| ES2197578T3 (es) * | 1998-02-23 | 2004-01-01 | The Standard Oil Company | Purificacion y recuperacion mejoradas de acetonitrilo. |
| US6395142B1 (en) | 1999-10-14 | 2002-05-28 | Chemcycles, Inc. | Method and apparatus for purifying low grade acetonitrile and other constituents from hazardous waste |
| JP4970276B2 (ja) | 2005-10-07 | 2012-07-04 | 三井化学株式会社 | アミド化合物の製造方法 |
| CN101597241B (zh) * | 2008-06-06 | 2012-11-21 | 上海星可高纯溶剂有限公司 | 一种提纯超净高纯度乙腈的方法 |
| CN101570498B (zh) * | 2009-05-27 | 2013-07-17 | 安徽时联特种溶剂股份有限公司 | 一种多级反应—精馏法生产hplc乙腈的方法 |
| CN104584164B (zh) * | 2012-09-04 | 2017-09-05 | 大金工业株式会社 | 电解液以及电化学器件 |
| CN104744300A (zh) * | 2013-12-31 | 2015-07-01 | 上海星可高纯溶剂有限公司 | 液相色谱-质谱联用仪用乙腈的提纯方法 |
| CN107778197B (zh) * | 2016-08-29 | 2020-07-10 | 中国石油化工股份有限公司 | 一种丙烯腈的提纯方法 |
| CN107778198A (zh) * | 2016-08-29 | 2018-03-09 | 中国石油化工股份有限公司 | 适用于生物法制备丙烯酰胺的丙烯腈的处理方法 |
| CN116987009A (zh) * | 2023-08-14 | 2023-11-03 | 西陇科学股份有限公司 | 一种梯度级乙腈及其制备方法 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2107904A (en) * | 1936-09-14 | 1938-02-08 | Armour & Co | Process of separating nitrile-hydrocarbon mixtures |
| US2351157A (en) * | 1943-10-30 | 1944-06-13 | Goodrich Co B F | Purification of nitriles |
| US3201451A (en) * | 1962-03-23 | 1965-08-17 | Standard Oil Co | Purification of acetonitrile |
| US3328458A (en) * | 1964-09-10 | 1967-06-27 | Universal Oil Prod Co | Purification of nitriles |
| US3322814A (en) * | 1964-09-10 | 1967-05-30 | Universal Oil Prod Co | Purification of nitriles |
| DE2102886B2 (de) * | 1971-01-22 | 1974-03-14 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zur Gewinnung von reinem Acetonitril |
| JPS5382722A (en) * | 1976-12-13 | 1978-07-21 | Nitto Chem Ind Co Ltd | Purification of crude acetonitrile |
| US4141826A (en) * | 1977-03-30 | 1979-02-27 | The Standard Oil Company | Treatment of acrylonitrile waste water with activated carbon |
| SU749828A1 (ru) * | 1977-05-10 | 1980-07-23 | Предприятие П/Я В-8873 | Способ регенерации ацетонитрила |
| US4308108A (en) * | 1979-03-28 | 1981-12-29 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for purification of crude acetonitrile |
| US4328075A (en) * | 1979-12-10 | 1982-05-04 | Standard Oil Company | Removal of cyanides from acetonitrile |
| US4287134A (en) * | 1980-06-26 | 1981-09-01 | E. I. Du Pont De Nemours And Company | Purification of acetonitrile by caustic extraction |
| US4362603A (en) * | 1981-01-02 | 1982-12-07 | The Standard Oil Company | Continuous acetonitrile recovery process |
| US4474709A (en) * | 1982-06-28 | 1984-10-02 | E. I. Du Pont De Nemours And Company | Removal of oxazole from acetonitrile |
| DD217212A1 (de) * | 1983-05-10 | 1985-01-09 | Petrolchemisches Kombinat | Verfahren zur reinigung von acetonitril |
| US4575434A (en) * | 1984-09-28 | 1986-03-11 | Akzona Incorporated | Process for the separation of amides from nitriles |
| SU1318588A1 (ru) * | 1985-08-26 | 1987-06-23 | Всесоюзный Научно-Исследовательский Институт Химических Реактивов И Особо Чистых Химических Веществ | Способ очистки ацетонитрила |
| US4730215A (en) * | 1986-05-30 | 1988-03-08 | Rca Corporation | Compatible wide screen television system with variable image compression/expansion |
| US5120881A (en) * | 1988-11-22 | 1992-06-09 | Exxon Chemical Patents Inc | Removal of nitrogenous components of a hydrocarbon feedstream |
| FR2655973B1 (fr) * | 1989-12-18 | 1992-03-20 | Elf Aquitaine | Procede catalytique de degradation oxydative d'effluents aqueux contenant des composes hydrocarbones toxiques. |
-
1993
- 1993-05-18 CA CA002136235A patent/CA2136235C/en not_active Expired - Fee Related
- 1993-05-18 AT AT93913980T patent/ATE148102T1/de not_active IP Right Cessation
- 1993-05-18 DE DE69307701T patent/DE69307701T2/de not_active Expired - Lifetime
- 1993-05-18 WO PCT/US1993/004731 patent/WO1993023366A1/en not_active Ceased
- 1993-05-18 EP EP93913980A patent/EP0641314B1/de not_active Expired - Lifetime
- 1993-05-21 US US08/064,972 patent/US5292919A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CA2136235C (en) | 2004-04-20 |
| DE69307701D1 (de) | 1997-03-06 |
| EP0641314B1 (de) | 1997-01-22 |
| EP0641314A4 (en) | 1995-03-22 |
| EP0641314A1 (de) | 1995-03-08 |
| CA2136235A1 (en) | 1993-11-25 |
| DE69307701T2 (de) | 1997-05-15 |
| WO1993023366A1 (en) | 1993-11-25 |
| US5292919A (en) | 1994-03-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |