ATE193998T1 - Verfahren zur herstellung von wasserstoffsuperoxyd und ein reaktor für dieses verfahren - Google Patents

Verfahren zur herstellung von wasserstoffsuperoxyd und ein reaktor für dieses verfahren

Info

Publication number: ATE193998T1
Authority: AT; Austria
Prior art keywords: reactor; working solution; top part; fixed bed; catalyst bed
Prior art date: 1994-03-15

Application number

AT95103745T

Other languages

English (en)

Inventor

Ilkka Turunen

Original Assignee

Kemira Chemicals Oy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1994-03-15

Filing date

1995-03-15

Publication date

2000-07-15

1995-03-15 Application filed by Kemira Chemicals Oy filed Critical Kemira Chemicals Oy

2000-07-15 Application granted granted Critical

2000-07-15 Publication of ATE193998T1 publication Critical patent/ATE193998T1/de

Links

238000000034 method Methods 0.000 title abstract 3
239000001257 hydrogen Substances 0.000 title abstract 2
229910052739 hydrogen Inorganic materials 0.000 title abstract 2
238000004519 manufacturing process Methods 0.000 title abstract 2
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title 1
OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 title 1
239000012224 working solution Substances 0.000 abstract 4
239000003054 catalyst Substances 0.000 abstract 3
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 2
PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 abstract 2
150000004056 anthraquinones Chemical class 0.000 abstract 2
239000006185 dispersion Substances 0.000 abstract 2
239000007789 gas Substances 0.000 abstract 2
RZVHIXYEVGDQDX-UHFFFAOYSA-N 9,10-anthraquinone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 abstract 1
125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
229940090441 infed Drugs 0.000 abstract 1
239000003960 organic solvent Substances 0.000 abstract 1
239000000126 substance Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/30—Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00026—Controlling or regulating the heat exchange system
- B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
- B01J2208/0007—Pressure measurement
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00539—Pressure
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00548—Flow

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Physics & Mathematics (AREA)
Thermal Sciences (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Catalysts (AREA)
Hydrogen, Water And Hydrids (AREA)

AT95103745T 1994-03-15 1995-03-15 Verfahren zur herstellung von wasserstoffsuperoxyd und ein reaktor für dieses verfahren ATE193998T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FI941217A FI95457C (fi)	1994-03-15	1994-03-15	Menetelmä vetyperoksidin valmistamiseksi ja siinä käytettävä reaktori

Publications (1)

Publication Number	Publication Date
ATE193998T1 true ATE193998T1 (de)	2000-07-15

Family

ID=8540316

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT95103745T ATE193998T1 (de)	1994-03-15	1995-03-15	Verfahren zur herstellung von wasserstoffsuperoxyd und ein reaktor für dieses verfahren

Country Status (6)

Country	Link
US (1)	US5637286A (de)
EP (1)	EP0672617B1 (de)
JP (1)	JPH07300303A (de)
AT (1)	ATE193998T1 (de)
DE (1)	DE69517542T2 (de)
FI (1)	FI95457C (de)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE19747407A1 (de) *	1997-10-27	1999-04-29	Basf Ag	Verfahren zur Hydrierung einer Anthrachinon-Verbindung in Gegenwart eines mindestens ein Metall der VIII. Nebengruppe des Periodensystems als Aktivmetall enthaltenden Katalysators
GB2334028A (en) *	1998-02-04	1999-08-11	Solvay	Making hydrogen peroxide by the anthraquinone process
DE19808385A1 (de) *	1998-02-27	1999-09-02	Basf Ag	Verfahren zur Suspensionshydrierung einer Anthrachinon-Verbindung in einem speziellen Reaktor zur Herstellung von Wasserstoffperoxid
ES2192883T3 (es) *	1998-09-12	2003-10-16	Degussa	Procedimiento para la realizacion de reacciones gas-liquido y reactor de circulacion para el mismo.
DE19841843A1 (de) *	1998-09-12	2000-03-30	Degussa	Verfahren zur Durchführung von Gas-Flüssig-Reaktionen und Durchflußreaktor hierfür
DE19953185A1 (de)	1999-11-05	2001-05-23	Degussa	Verfahren zur Herstellung von Wasserstoffperoxid
US6455023B1 (en) *	2000-10-11	2002-09-24	Corning Incorporated	Metallic catalysts for non-neutral liquid media
DE10052323A1 (de) *	2000-10-21	2002-05-02	Degussa	Kontinierliches Verfahren zur Hydrierung
WO2002051778A1 (en)	2000-12-27	2002-07-04	Corning Incorporated	Flow control in a three-phase monolithic catalyst reactor
FI110427B (fi)	2001-03-28	2003-01-31	Kemira Chemicals Oy	Työliuoksen hydraus vetyperoksidin valmistusprosessissa
US7147833B2 (en)	2002-03-25	2006-12-12	Huckins Harold A	Method for producing hydrogen peroxide from hydrogen and oxygen
ES2380231T3 (es) *	2005-08-31	2012-05-09	Fmc Corporation	Producción por autooxidación de peróxido de hidrógeno mediante oxidación de un microreactor
CN101296860B (zh) *	2005-08-31	2012-08-29	Fmc有限公司	在微反应器中通过加氢自动氧化生产过氧化氢
CN102009960A (zh) *	2010-11-18	2011-04-13	清华大学	一种蒽醌法生产过氧化氢的加氢方法
US8474240B1 (en) *	2012-08-10	2013-07-02	NW Licensing Company LLC	Regenerative gas generator
CN104418307B (zh) *	2013-08-22	2016-06-22	中国石油化工股份有限公司	一种蒽醌法生产双氧水多段氢化工艺
CN104418309B (zh) *	2013-09-05	2016-08-17	中国石油化工股份有限公司	一种过氧化氢的制备方法
CN107055481A (zh) *	2016-10-18	2017-08-18	上海睿思化工科技有限公司	一种过氧化氢的制备方法
CN106395755B (zh) *	2016-11-02	2019-12-10	上海睿思化工科技有限公司	一种蒽醌法制备过氧化氢的方法
CN109678120B (zh) *	2017-10-19	2020-06-09	中国石油化工股份有限公司	一种蒽醌法生产双氧水的氢化反应器及氢化方法
CN114644321A (zh) *	2020-12-21	2022-06-21	大连理工江苏研究院有限公司	一种基于蒽醌法制备过氧化氢的改进系统及工艺

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US1227047A (en) *	1916-06-13	1917-05-22	William P Gray	Brush.
IT509938A (de) *	1952-04-28
US2837411A (en) *	1952-11-25	1958-06-03	Olin Mathieson	Process for production of hydrogen peroxide
US2966398A (en) *	1958-03-12	1960-12-27	Fmc Corp	Production of hydrogen peroxide by slurrying the anthraquinone working soulution
US3009782A (en) *	1958-05-22	1961-11-21	Fmc Corp	Production of hydrogen peroxide by anthraquinone process in the presence of a fixed bed catalyst
NL139013B (nl) *	1965-12-04	1973-06-15	Degussa	Werkwijze voor het bereiden van waterstofperoxyde volgens het antrachinonkringloopprocede.
US3565581A (en) *	1968-05-16	1971-02-23	Fmc Corp	Production of hydrogen peroxide in the anthraquinone process using a novel catalytic fixed bed
DE2042522C3 (de) *	1970-08-27	1979-01-25	Deutsche Gold- U. Silber-Scheideanstalt, Vormals Roessler, 6000 Frankfurt	Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen
US3755552A (en) *	1970-10-21	1973-08-28	Fmc Corp	Process for producing hydrogen peroxide
ATE17026T1 (de) *	1982-02-19	1986-01-15	Pierre Zurkinden	Sportplatzbelag.
US4428922A (en) *	1982-05-14	1984-01-31	Fmc Corporation	Process for manufacturing hydrogen peroxide
SE431532B (sv) *	1982-09-08	1984-02-13	Eka Ab	Forfarande vid framstellning av veteperoxid
US4428923A (en) *	1982-11-09	1984-01-31	Degussa Aktiengesellschaft	Continuous process for the production of hydrogen peroxide according to the anthraquinone process
FI77633B (fi) *	1986-12-05	1988-12-30	Kemira Oy	Foerfarande foer framstaellning av vaeteperoxid.
FI82669C (fi) *	1989-01-27	1991-04-10	Kemira Oy	Foerfarande foer framstaellning av vaeteperoxid.
SE464867B (sv) *	1989-02-23	1991-06-24	Eka Nobel Ab	Foerfarande vid framstaellning av vaeteperoxid enligt antrakinonprocessen

1994
- 1994-03-15 FI FI941217A patent/FI95457C/fi not_active IP Right Cessation
1995
- 1995-03-14 US US08/404,170 patent/US5637286A/en not_active Expired - Fee Related
- 1995-03-15 AT AT95103745T patent/ATE193998T1/de not_active IP Right Cessation
- 1995-03-15 JP JP7055615A patent/JPH07300303A/ja not_active Withdrawn
- 1995-03-15 DE DE69517542T patent/DE69517542T2/de not_active Expired - Fee Related
- 1995-03-15 EP EP95103745A patent/EP0672617B1/de not_active Expired - Lifetime

Also Published As

Publication number	Publication date
US5637286A (en)	1997-06-10
FI95457C (fi)	1996-02-12
JPH07300303A (ja)	1995-11-14
DE69517542D1 (de)	2000-07-27
DE69517542T2 (de)	2000-11-16
EP0672617B1 (de)	2000-06-21
FI95457B (fi)	1995-10-31
EP0672617A1 (de)	1995-09-20
FI941217A0 (fi)	1994-03-15

Legal Events

Date	Code	Title	Description
2004-10-15	EEIH	Change in the person of patent owner
2005-12-15	REN	Ceased due to non-payment of the annual fee

Publication	Publication Date	Title
ATE193998T1 (de)	2000-07-15	Verfahren zur herstellung von wasserstoffsuperoxyd und ein reaktor für dieses verfahren
DE69817653D1 (de)	2003-10-09	Verfahren zur Umwandlung von Kohlenwasserstoffeinsätzen, katalytische Emulsion und Verfahren zu ihren Herstellung
ATE235963T1 (de)	2003-04-15	Neuer katalysator, verfahren für die herstellung von wasserstoffperoxid und seine verwendung für oxidierungsverfahren
ATE240262T1 (de)	2003-05-15	Verfahren zur herstellung von wasserstoffperoxid durch direktsynthese
BR9502610A (pt)	1996-01-02	Processo para separação de solução de trabalho isenta de catalisador do ciclo de hidrogenação do processo de antraquinona para preparação de peróxido de hidrogênio
ATE273238T1 (de)	2004-08-15	Katalysator für die herstellung von synthesegas und verfahren zur herstellung von kohlenmonoxid
BR8807760A (pt)	1990-08-07	Catalisador e processo para a producao de hidrocarbonetos a partir de gas de sintese
FR2412514A1 (fr)	1979-07-20	Procede d'hydrogenation catalytique
ATE168969T1 (de)	1998-08-15	Verfahren zur herstellung von kohlenmonoxid und wasserstoff
SE9000228D0 (sv)	1990-01-23	A process for the preparation of hydrogen peroxide
MY113319A (en)	2002-01-31	Process for preparing 1, 3-alkanediols and 3-hydroxyaldehydes
DE69714554D1 (de)	2002-09-12	Verfahren III zur Herstellung von Essigsäure
ATE25839T1 (de)	1987-03-15	Verfahren zur katalytischen herstellung von wasserstoffperoxid aus sauerstoff und wasserstoff.
ATE175411T1 (de)	1999-01-15	Verfahren zur herstellung von gamma-butyrolacton
ATE183493T1 (de)	1999-09-15	Verfahren zur herstellung von 3.3.5- trimethylcyclohexanon
SE9000227D0 (sv)	1990-01-23	A process for the preparation of hydrogen peroxide
DE69506573D1 (de)	1999-01-21	Verfahren zur herstellung von 1,3-alkandiolen und 3-hydroxyaldehyden
DE59807245D1 (de)	2003-03-27	Verfahren zur reinigung von stoffströmen
DE69506580D1 (de)	1999-01-21	Verfahren zur herstellung von 1,3-alkandiolen und 3-hydroxyaldehyden
DK0458675T3 (da)	1994-12-12	Fremgangsmåde til regenerering af en brugt katalysator med en vandig opløsning af hydrogenperoxid stabiliseret med en organisk forbindelse
KR830003392A (ko)	1983-06-20	싸이크로 헥산올 및/또는 싸이크로 헥사논의 제조방법
ATE141249T1 (de)	1996-08-15	Herstellung von 8-hydroxy-p-cymol durch dehydrogenierung
ATE150445T1 (de)	1997-04-15	Kontinuierliche herstellung von oxamid durch die katalytische oxydation von hcn
ES2167447T3 (es)	2002-05-16	Procedimiento para la produccion de aminoazabicicloalcanos a partir de oximas.
AR006821A1 (es)	1999-09-29	Un procedimiento para producir uno o mas alcoholes no saturados substituidos o no substituidos, una composicion asi producida, una mezcla dereaccion asi preparada y derivados de alcoholes no saturados substituidos o no substituidos asi preparados.