ATE220657T1 - Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure - Google Patents

Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure

Info

Publication number
ATE220657T1
ATE220657T1 AT99308376T AT99308376T ATE220657T1 AT E220657 T1 ATE220657 T1 AT E220657T1 AT 99308376 T AT99308376 T AT 99308376T AT 99308376 T AT99308376 T AT 99308376T AT E220657 T1 ATE220657 T1 AT E220657T1
Authority
AT
Austria
Prior art keywords
methacrylic acid
methyl methacrylate
high yield
producing high
yield methyl
Prior art date
Application number
AT99308376T
Other languages
English (en)
Inventor
Chorng-Shyuan Tsay
Makarand Dattatraya Phadke
Soc
Michael Stanley Decourcy
Abraham Benderly
I-Hwa Midey Chang-Mateu
Nicole Rendon Koegel
Heather Granzin Thompson
Diana Elaine Chase
Original Assignee
Rohm & Haas
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm & Haas filed Critical Rohm & Haas
Application granted granted Critical
Publication of ATE220657T1 publication Critical patent/ATE220657T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/08—Preparation of carboxylic acids or their salts, halides or anhydrides from nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/18—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group
    • C07C67/20—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group from amides or lactams
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B01J2219/029—Non-ferrous metals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
AT99308376T 1998-11-04 1999-10-22 Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure ATE220657T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10694798P 1998-11-04 1998-11-04

Publications (1)

Publication Number Publication Date
ATE220657T1 true ATE220657T1 (de) 2002-08-15

Family

ID=22314086

Family Applications (1)

Application Number Title Priority Date Filing Date
AT99308376T ATE220657T1 (de) 1998-11-04 1999-10-22 Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure

Country Status (10)

Country Link
US (2) US6545176B1 (de)
EP (1) EP0999200B1 (de)
JP (2) JP4553425B2 (de)
KR (1) KR100691647B1 (de)
CN (1) CN1173921C (de)
AT (1) ATE220657T1 (de)
BR (1) BR9904993B1 (de)
DE (1) DE69902137T2 (de)
ES (1) ES2179599T3 (de)
TW (1) TW505629B (de)

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FR2827279B1 (fr) * 2001-07-13 2004-06-18 Atofina Procede de preparation de methacrylamide sulfurique et dispositif pour sa mise en oeuvre
ZA200303241B (en) * 2002-05-01 2003-11-04 Rohm & Haas Improved process for methacrylic acid and methcrylic acid ester production.
US7128813B2 (en) 2002-05-01 2006-10-31 Rohm And Haas Company Process for manufacturing high purity methacrylic acid
BRPI0503134B1 (pt) 2004-08-02 2018-03-20 Rohm And Haas Company Método de formação de uma chapa de tubo laminada
US20110197556A1 (en) 2004-11-02 2011-08-18 Baldwin Filters, Inc. Filter element
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US9757676B2 (en) 2006-12-06 2017-09-12 Baldwin Filters, Inc. Method and apparatus for winding a filter element
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
DE102006058251A1 (de) * 2006-12-08 2008-06-12 Evonik Röhm Gmbh Verfahren und Vorrichtung zur Herstellung von Methacrylsäurealkylestern
US7892498B2 (en) * 2007-03-08 2011-02-22 Eastman Chemical Company Polyester production system employing an unagitated esterification reactor
US7863477B2 (en) 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7868129B2 (en) * 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7872090B2 (en) * 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7872089B2 (en) * 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7847053B2 (en) * 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7829653B2 (en) * 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7868130B2 (en) * 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
US7858730B2 (en) * 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
US7842777B2 (en) * 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US9545593B2 (en) 2007-11-01 2017-01-17 Baldwin Filters, Inc. Winding core pressure relief for fluted filter
EP2085376B1 (de) 2008-01-30 2012-09-05 Evonik Röhm GmbH Verfahren zur Herstellung hochreiner Methacrylsäure
DE102008000787A1 (de) * 2008-03-20 2009-09-24 Evonik Röhm Gmbh Verfahren zur Aufreinigung von Methacrylsäure
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JP5432852B2 (ja) * 2009-09-30 2014-03-05 ローム アンド ハース カンパニー メタクリル酸メチルの精製によって生じる流れから価値のある化合物を回収する方法
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KR20120093202A (ko) * 2009-10-09 2012-08-22 다우 글로벌 테크놀로지스 엘엘씨 단열식 플러그 흐름 반응기 및 염화 및/또는 불화 프로펜 및 고급 알켄의 제조 방법
EP2485997B1 (de) 2009-10-09 2015-09-09 Dow Global Technologies LLC Verfahren zur herstellung von chlorierten und/oder fluorierten probenen und höheren alkenen
JP5782038B2 (ja) * 2009-10-09 2015-09-24 ダウ グローバル テクノロジーズ エルエルシー 等温多管式反応器及び該反応器を組み込んだプロセス
KR101174203B1 (ko) 2010-04-09 2012-08-14 박병진 폐인조 대리석으로부터 메타크릴산메틸을 회수하는 장치 및 그 방법
EP2625160B1 (de) * 2010-10-07 2014-08-13 Rohm and Haas Company Verfahren zur herstellung eines methacrylsäureesters
CA2837292C (en) 2011-05-31 2020-01-28 Blue Cube Ip Llc Process for the production of chlorinated propenes
CA2836493A1 (en) 2011-05-31 2012-12-06 Max Markus Tirtowidjojo Process for the production of chlorinated propenes
ES2721451T3 (es) 2011-06-08 2019-07-31 Dow Agrosciences Llc Procedimiento para la producción de propenos clorados y/o fluorados
CN103717559A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
EP2739595B1 (de) 2011-08-07 2018-12-12 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propenen
CA2856271A1 (en) 2011-11-21 2013-05-30 Dow Global Technologies Llc Process for the production of chlorinated alkanes
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JP6059246B2 (ja) 2011-12-02 2017-01-11 ブルー キューブ アイピー エルエルシー 塩素化アルカンの製造方法
JP6170068B2 (ja) 2011-12-13 2017-07-26 ブルー キューブ アイピー エルエルシー 塩素化プロパン及びプロペンの製造方法
EP2794528B1 (de) 2011-12-22 2020-02-26 Blue Cube IP LLC Verfahren zur herstellung von tetrachlormethan
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US9321707B2 (en) 2012-09-20 2016-04-26 Blue Cube Ip Llc Process for the production of chlorinated propenes
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CN103254091B (zh) * 2013-05-21 2015-04-08 重庆紫光化工股份有限公司 一种甲基丙烯酰胺、甲基丙烯酸甲酯和甲基丙烯酸的联合生产方法
FR3008627B1 (fr) * 2013-07-19 2017-02-24 Arkema France Cuve de conversion thermique utilisee dans un procede d'amidification de cyanohydrine d'acetone
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BR112017007905B1 (pt) 2014-10-27 2021-11-30 Rohm And Haas Company Processo para a produção de metil metacrilato
CN106795091B (zh) * 2014-10-27 2020-11-03 罗门哈斯公司 用于生产甲基丙烯酸甲酯的减少积垢的方法
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CN110394143B (zh) * 2019-08-21 2024-06-07 兖矿能源集团股份有限公司 一种煤消解管式反应装置
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CN113121343A (zh) * 2021-03-15 2021-07-16 江苏新东风化工科技有限公司 一种丙烯酸正丁酯的中和生产工艺
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Also Published As

Publication number Publication date
US20020188153A1 (en) 2002-12-12
US6545176B1 (en) 2003-04-08
KR100691647B1 (ko) 2007-03-09
JP2000159728A (ja) 2000-06-13
EP0999200B1 (de) 2002-07-17
CN1254706A (zh) 2000-05-31
ES2179599T3 (es) 2003-01-16
BR9904993B1 (pt) 2011-02-08
DE69902137D1 (de) 2002-08-22
EP0999200A1 (de) 2000-05-10
BR9904993A (pt) 2000-08-08
KR20000035177A (ko) 2000-06-26
JP5213901B2 (ja) 2013-06-19
US6610177B2 (en) 2003-08-26
CN1173921C (zh) 2004-11-03
JP2010209087A (ja) 2010-09-24
TW505629B (en) 2002-10-11
JP4553425B2 (ja) 2010-09-29
DE69902137T2 (de) 2003-01-30

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