ATE282044T1 - Chromatographische reinigung von chlorinierter sukrose - Google Patents

Chromatographische reinigung von chlorinierter sukrose

Info

Publication number
ATE282044T1
ATE282044T1 AT98906453T AT98906453T ATE282044T1 AT E282044 T1 ATE282044 T1 AT E282044T1 AT 98906453 T AT98906453 T AT 98906453T AT 98906453 T AT98906453 T AT 98906453T AT E282044 T1 ATE282044 T1 AT E282044T1
Authority
AT
Austria
Prior art keywords
chlorinated sucrose
adsorbent
chromatographic purification
chlorinated
sucrose
Prior art date
Application number
AT98906453T
Other languages
English (en)
Inventor
Stephen J Catani
Duane Leinhos
Thomas O'connor
Original Assignee
Tate & Lyle Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc
Application granted granted Critical
Publication of ATE282044T1 publication Critical patent/ATE282044T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
AT98906453T 1997-02-13 1998-02-11 Chromatographische reinigung von chlorinierter sukrose ATE282044T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US4698097P 1997-02-13 1997-02-13
PCT/US1998/002927 WO1998035974A1 (en) 1997-02-13 1998-02-11 Chromatographic purification of chlorinated sucrose

Publications (1)

Publication Number Publication Date
ATE282044T1 true ATE282044T1 (de) 2004-11-15

Family

ID=21946404

Family Applications (1)

Application Number Title Priority Date Filing Date
AT98906453T ATE282044T1 (de) 1997-02-13 1998-02-11 Chromatographische reinigung von chlorinierter sukrose

Country Status (17)

Country Link
US (1) US5977349A (de)
EP (1) EP0970096B1 (de)
JP (2) JP4623763B2 (de)
KR (2) KR100619874B1 (de)
AT (1) ATE282044T1 (de)
AU (1) AU6167598A (de)
BR (1) BR9807377B1 (de)
CA (1) CA2280784A1 (de)
DE (1) DE69827482T2 (de)
DK (1) DK0970096T3 (de)
ES (1) ES2231964T3 (de)
IL (1) IL131394A0 (de)
NO (1) NO313553B1 (de)
NZ (1) NZ337573A (de)
PT (1) PT970096E (de)
TR (1) TR199902413T2 (de)
WO (1) WO1998035974A1 (de)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998035974A1 (en) * 1997-02-13 1998-08-20 Mcneil-Ppc Inc. Chromatographic purification of chlorinated sucrose
US6998480B2 (en) * 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US7049435B2 (en) * 2002-03-08 2006-05-23 Tate & Lyle Public Limited Company Extractive methods for purifying sucralose
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
CN101098972A (zh) * 2004-12-10 2008-01-02 法马德医疗保险私人有限公司 硅烷化硅胶色谱纯化6-乙酰基-4,1',6'三氯半乳蔗糖和4,1',6'三氯半乳蔗糖的改良方法
US8148112B2 (en) * 2005-02-16 2012-04-03 National University Corporation Hokkaido University Sugar chain containing 4-position halogenated galactose and application thereof
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
WO2007023505A2 (en) * 2005-06-06 2007-03-01 Pharmed Medicare Private Limited Method for purification of chlorinated sucrose derivatives from reaction mixture by chromatography
WO2007052303A2 (en) * 2005-08-30 2007-05-10 Pharmed Medicare Pvt. Ltd. Process for production of chlorinated sucrose based on hydrophobic affinity chromatography.
EP2029522A2 (de) * 2006-05-23 2009-03-04 V.B. Medicare Pvt. Ltd. Rückgewinnung von dimethylformamid und anderen lösungsmitteln aus verfahrensströmen aus der herstellung von trichlorgalactosaccharose
CN101029062B (zh) * 2007-04-09 2011-06-15 淄博联技甜味剂有限公司 三氯蔗糖的合成工艺
US8436156B2 (en) * 2008-01-04 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
WO2009117317A1 (en) * 2008-03-20 2009-09-24 Tate & Lyle Technology Ltd Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US8212022B2 (en) * 2008-04-03 2012-07-03 Tate & Lyle Technology Limited Effect of carbohydrate concentration on sucralose extraction efficiency
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
WO2009124113A1 (en) * 2008-04-03 2009-10-08 Tate & Lyle Technology Ltd. Extraction of less polar impurities from sucralose containing aqueous feed streams
GB2468936B (en) 2009-03-27 2011-09-07 Mohamad Rami Radwan Jaber Chlorination of sucrose-6-esters
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
US20120034366A1 (en) * 2010-08-05 2012-02-09 Tate & Lyle Ingredients Americas, Inc. Carbohydrate compositions
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN102830197B (zh) * 2012-07-25 2015-07-15 湖北省宏源药业科技股份有限公司 一种中控监测单酯法合成三氯蔗糖过程的方法
GB2539112B (en) 2013-12-16 2020-11-04 Tate & Lyle Tech Ltd Chlorination of sucrose-6-esters
WO2016020635A1 (en) 2014-08-08 2016-02-11 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ZA807578B (en) * 1979-12-18 1981-11-25 Tate & Lyle Patent Holdings Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3165986D1 (en) * 1980-07-08 1984-10-18 Tate & Lyle Plc Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
ZA817425B (en) * 1980-10-28 1982-10-27 Tate & Lyle Patent Holdings Sweet chlorine-substituted disaccharides
EP0067535B1 (de) * 1981-05-22 1985-01-30 TATE & LYLE PUBLIC LIMITED COMPANY Brom substituierte Derivate von Sucrose
GB8316201D0 (en) * 1982-09-13 1983-07-20 Tate & Lyle Plc Sucrose derivatives
GB8822673D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Selective acylation of sugars
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
JPH06253879A (ja) * 1993-03-01 1994-09-13 Snow Brand Milk Prod Co Ltd グルクロン酸結合オリゴ糖の分離方法
US5298611A (en) * 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
US5530106A (en) * 1993-03-12 1996-06-25 Mcneil-Ppc, Inc. Recovery of sucralose intermediates
EP0687491A1 (de) * 1994-06-16 1995-12-20 Daicel Chemical Industries, Ltd. Chromatographisches simuliertes Wanderbetttrennungsverfahren
US5498709A (en) * 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
WO1998035974A1 (en) * 1997-02-13 1998-08-20 Mcneil-Ppc Inc. Chromatographic purification of chlorinated sucrose

Also Published As

Publication number Publication date
JP5132665B2 (ja) 2013-01-30
JP2010090160A (ja) 2010-04-22
BR9807377A (pt) 2001-06-19
KR100619874B1 (ko) 2006-09-06
US5977349A (en) 1999-11-02
BR9807377B1 (pt) 2009-12-01
NO993920L (no) 1999-10-11
NZ337573A (en) 2000-06-23
KR20050093860A (ko) 2005-09-23
EP0970096A1 (de) 2000-01-12
TR199902413T2 (xx) 2000-01-21
DE69827482D1 (de) 2004-12-16
CA2280784A1 (en) 1998-08-20
PT970096E (pt) 2005-03-31
JP2001511812A (ja) 2001-08-14
DE69827482T2 (de) 2005-12-15
ES2231964T3 (es) 2005-05-16
JP4623763B2 (ja) 2011-02-02
WO1998035974A1 (en) 1998-08-20
AU6167598A (en) 1998-09-08
NO993920D0 (no) 1999-08-13
KR100531261B1 (ko) 2005-11-28
NO313553B1 (no) 2002-10-21
KR20000071081A (ko) 2000-11-25
IL131394A0 (en) 2001-01-28
DK0970096T3 (da) 2005-03-21
EP0970096B1 (de) 2004-11-10

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