ATE301631T1 - Verfahren zur herstellung von 2-ethylhexylacrylat - Google Patents

Verfahren zur herstellung von 2-ethylhexylacrylat

Info

Publication number: ATE301631T1
Authority: AT; Austria
Prior art keywords: ethylhexyl acrylate; ethylhexanol; acid; acrylic acid; esterification
Prior art date: 2001-04-02

Application number

AT02290719T

Other languages

English (en)

Inventor

Jacqueline Bessalem

Michel Fauconet

Stephane Lepizzera

Original Assignee

Arkema

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2001-04-02

Filing date

2002-03-21

Publication date

2005-08-15

2002-03-21 Application filed by Arkema filed Critical Arkema

2005-08-15 Application granted granted Critical

2005-08-15 Publication of ATE301631T1 publication Critical patent/ATE301631T1/de

Links

GOXQRTZXKQZDDN-UHFFFAOYSA-N 2-Ethylhexyl acrylate Chemical compound CCCCC(CC)COC(=O)C=C GOXQRTZXKQZDDN-UHFFFAOYSA-N 0.000 title abstract 7
238000004519 manufacturing process Methods 0.000 title abstract 3
YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 abstract 12
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 abstract 5
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract 5
238000005886 esterification reaction Methods 0.000 abstract 5
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
239000002253 acid Substances 0.000 abstract 4
230000032050 esterification Effects 0.000 abstract 4
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 3
239000008346 aqueous phase Substances 0.000 abstract 3
239000012074 organic phase Substances 0.000 abstract 3
-1 2-ethylhexyl Chemical group 0.000 abstract 2
238000004821 distillation Methods 0.000 abstract 2
239000012535 impurity Substances 0.000 abstract 2
239000011541 reaction mixture Substances 0.000 abstract 2
238000000926 separation method Methods 0.000 abstract 2
238000006243 chemical reaction Methods 0.000 abstract 1
230000008030 elimination Effects 0.000 abstract 1
238000003379 elimination reaction Methods 0.000 abstract 1
230000007062 hydrolysis Effects 0.000 abstract 1
238000006460 hydrolysis reaction Methods 0.000 abstract 1
239000000203 mixture Substances 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
- C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
- C07C69/54—Acrylic acid esters; Methacrylic acid esters
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Detergent Compositions (AREA)

AT02290719T 2001-04-02 2002-03-21 Verfahren zur herstellung von 2-ethylhexylacrylat ATE301631T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FR0104442A FR2822825B1 (fr)	2001-04-02	2001-04-02	Procede de fabrication d'acrylate de 2-ethylhexyle comportant le lavage a l'eau du brut

Publications (1)

Publication Number	Publication Date
ATE301631T1 true ATE301631T1 (de)	2005-08-15

Family

ID=8861832

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT02290719T ATE301631T1 (de)	2001-04-02	2002-03-21	Verfahren zur herstellung von 2-ethylhexylacrylat

Country Status (9)

Country	Link
US (1)	US6603036B2 (de)
EP (1)	EP1247795B1 (de)
JP (1)	JP3782032B2 (de)
KR (1)	KR100473661B1 (de)
CN (1)	CN1181039C (de)
AT (1)	ATE301631T1 (de)
DE (1)	DE60205422T2 (de)
FR (1)	FR2822825B1 (de)
TW (1)	TW575558B (de)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
KR101114400B1 (ko) *	2006-09-01	2012-02-14	주식회사 엘지화학	회분공정에 의한 2-에틸헥실 아크릴레이트의 제조방법
WO2010107284A2 (ko) *	2009-03-19	2010-09-23	주식회사 엘지화학	고순도 아크릴산 생산을 위한 분리벽형 증류탑 및 이를 이용한 분별증류방법
KR101496488B1 (ko)	2010-12-29	2015-02-26	주식회사 엘지화학	고순도 2-에틸헥실-아크릴레이트 생산을 위한 분리벽형 증류탑 및 이를 이용한 제조방법
FR3024143B1 (fr) *	2014-07-28	2016-07-15	Arkema France	Procede perfectionne de fabrication de (meth)acrylates d'alkyle
CN104262146B (zh) *	2014-09-24	2017-10-27	江苏国胶化学科技有限公司	丙烯酸异辛酯的分水罐系统装置
CN106365996B (zh) *	2016-08-08	2020-03-24	江苏国胶新材料有限公司	丙烯酸异辛酯酯化液水洗工艺
WO2018114429A1 (de) *	2016-12-21	2018-06-28	Basf Se	Verfahren zur destillativen gewinnung von rein-2-ethylhexylacrylat oder rein-2-propylheptylacrylat aus dem entsprechenden roh-alkylacrylat
FR3091871B1 (fr) *	2019-01-22	2020-12-18	Arkema France	Procede de purification d’esters (meth)acryliques a l’aide d’une colonne a partition
CN119430365A (zh) *	2024-11-27	2025-02-14	平湖石化有限责任公司	一种丙烯酸的萃取处理工艺及应用

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4019781A1 (de) *	1990-06-21	1992-01-02	Basf Ag	Verfahren zur herstellung von monoethylenisch ungesaettigten carbonsaeureestern
FR2700767B1 (fr)	1993-01-27	1995-04-07	Atochem Elf Sa	Procédé perfectionné de fabrication de (méthacrylates d'alkyle par estérification directe.
FR2721313B1 (fr)	1994-06-17	1996-07-19	Atochem Elf Sa	Procédé de fabrication d'acrylates d'alkyle par estérification directe.
FR2723089B1 (fr) *	1994-07-28	1996-09-06	Atochem Elf Sa	Procede de fabrication de l'acrylate de butyle par esterification directe

2001
- 2001-04-02 FR FR0104442A patent/FR2822825B1/fr not_active Expired - Lifetime
2002
- 2002-03-21 EP EP02290719A patent/EP1247795B1/de not_active Expired - Lifetime
- 2002-03-21 DE DE60205422T patent/DE60205422T2/de not_active Expired - Fee Related
- 2002-03-21 AT AT02290719T patent/ATE301631T1/de not_active IP Right Cessation
- 2002-04-01 JP JP2002098571A patent/JP3782032B2/ja not_active Expired - Fee Related
- 2002-04-02 TW TW91106624A patent/TW575558B/zh not_active IP Right Cessation
- 2002-04-02 US US10/113,924 patent/US6603036B2/en not_active Expired - Fee Related
- 2002-04-02 CN CNB021192162A patent/CN1181039C/zh not_active Expired - Fee Related
- 2002-04-02 KR KR10-2002-0017898A patent/KR100473661B1/ko not_active Expired - Fee Related

Also Published As

Publication number	Publication date
US20020193623A1 (en)	2002-12-19
DE60205422T2 (de)	2006-05-24
US6603036B2 (en)	2003-08-05
KR100473661B1 (ko)	2005-03-08
FR2822825B1 (fr)	2003-05-16
TW575558B (en)	2004-02-11
CN1379015A (zh)	2002-11-13
DE60205422D1 (de)	2005-09-15
EP1247795B1 (de)	2005-08-10
EP1247795A1 (de)	2002-10-09
FR2822825A1 (fr)	2002-10-04
KR20020077821A (ko)	2002-10-14
JP2002322133A (ja)	2002-11-08
JP3782032B2 (ja)	2006-06-07
CN1181039C (zh)	2004-12-22

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Legal Events

Date	Code	Title	Description
2006-02-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties