ATE307668T1 - Herstellung eines doppelmetallcyanidkatalysators - Google Patents
Herstellung eines doppelmetallcyanidkatalysatorsInfo
- Publication number
- ATE307668T1 ATE307668T1 AT03759958T AT03759958T ATE307668T1 AT E307668 T1 ATE307668 T1 AT E307668T1 AT 03759958 T AT03759958 T AT 03759958T AT 03759958 T AT03759958 T AT 03759958T AT E307668 T1 ATE307668 T1 AT E307668T1
- Authority
- AT
- Austria
- Prior art keywords
- metal
- salt
- metal cyanide
- dmc catalyst
- catalyst
- Prior art date
Links
- 239000002184 metal Substances 0.000 title abstract 11
- 239000003054 catalyst Substances 0.000 title abstract 7
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 abstract 6
- 150000003839 salts Chemical class 0.000 abstract 4
- 150000002825 nitriles Chemical class 0.000 abstract 3
- 125000002947 alkylene group Chemical group 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 239000003999 initiator Substances 0.000 abstract 1
- 150000002736 metal compounds Chemical class 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
- B01J27/26—Cyanides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/02—Ethers
- C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
- C07C43/04—Saturated ethers
- C07C43/10—Saturated ethers of polyhydroxy compounds
- C07C43/11—Polyethers containing —O—(C—C—O—)n units with ≤ 2 n≤ 10
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/02—Ethers
- C07C43/18—Ethers having an ether-oxygen atom bound to a carbon atom of a ring other than a six-membered aromatic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Catalysts (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP02254161 | 2002-06-14 | ||
| PCT/EP2003/006279 WO2003106025A1 (en) | 2002-06-14 | 2003-06-13 | Preparation of a double metal cyanide catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE307668T1 true ATE307668T1 (de) | 2005-11-15 |
Family
ID=29724546
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT03759958T ATE307668T1 (de) | 2002-06-14 | 2003-06-13 | Herstellung eines doppelmetallcyanidkatalysators |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6716788B2 (de) |
| EP (1) | EP1515801B2 (de) |
| JP (1) | JP2005529994A (de) |
| KR (1) | KR100945698B1 (de) |
| CN (1) | CN1662303B (de) |
| AT (1) | ATE307668T1 (de) |
| AU (1) | AU2003242705A1 (de) |
| DE (1) | DE60302073T3 (de) |
| WO (1) | WO2003106025A1 (de) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060058182A1 (en) * | 2004-09-13 | 2006-03-16 | Combs George G | Processes for the preparation of double metal cyanide (DMC) catalysts |
| CN100415647C (zh) * | 2006-09-05 | 2008-09-03 | 黎明化工研究院 | 水溶性金属氰化物盐制备工艺 |
| KR101902018B1 (ko) | 2010-05-18 | 2018-09-27 | 바이엘 인텔렉쳐 프로퍼티 게엠베하 | 폴리에테르 카르보네이트 폴리올의 제조 방법 |
| KR101404702B1 (ko) | 2011-03-08 | 2014-06-17 | 에스케이이노베이션 주식회사 | 에테르 결합 단위체를 함유한 이산화탄소/에폭사이드 공중합체의 제조 방법 |
| CN102875796B (zh) * | 2012-10-16 | 2015-03-04 | 山东蓝星东大化工有限责任公司 | 一种提高聚醚多元醇生产用dmc催化剂活性的方法 |
| EP3106221A1 (de) * | 2015-06-15 | 2016-12-21 | Universität Hamburg | Verfahren zur herstellung von doppelmetallcyanidkatalysatoren und deren verwendung in polymerisierungsreaktionen |
| GB201515350D0 (en) | 2015-08-28 | 2015-10-14 | Econic Technologies Ltd | Method for preparing polyols |
| CN107200837B (zh) | 2016-03-18 | 2019-10-18 | 淮安巴德聚氨酯科技有限公司 | 一种利用dmc催化剂循环制备聚醚多元醇的方法 |
| US10258953B2 (en) | 2016-08-05 | 2019-04-16 | Covestro Llc | Systems and processes for producing polyether polyols |
| GB201703324D0 (en) | 2017-03-01 | 2017-04-12 | Econic Tech Ltd | Method for preparing polyether carbonates |
| PL3622003T3 (pl) * | 2017-05-10 | 2025-02-24 | Dow Global Technologies Llc | Proces polimeryzacji polieterowej |
| GB201717441D0 (en) | 2017-10-24 | 2017-12-06 | Econic Tech Ltd | A polymerisation process |
| GB201814526D0 (en) | 2018-09-06 | 2018-10-24 | Econic Tech Ltd | Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates |
| GB201906214D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Ltd | A polyol block copolymer, compositions and processes therefor |
| GB201906210D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Limited | A polyol block copolymer, compositions and processes therefor |
| EP4106917A2 (de) | 2020-02-22 | 2022-12-28 | Covestro Deutschland AG | Verfahren zur herstellung von doppelmetallcyanid-katalysatoren |
| GB202003002D0 (en) | 2020-03-02 | 2020-04-15 | Crane Ltd | Method of preparation of a polyol block copolymer |
| GB202003003D0 (en) | 2020-03-02 | 2020-04-15 | Econic Tech Ltd | A polyol block copolymer |
| GB202017531D0 (en) | 2020-11-05 | 2020-12-23 | Econic Tech Limited | (poly)ol block copolymer |
| MX2024001871A (es) | 2021-08-11 | 2024-03-04 | Econic Tech Ltd | Metodo para preparar tensoactivos mediante copolimerizacion de epoxidos y co2 utilizando una mezcla de un catalizador bimetalico macrociclico y un catalizador de cianuro bimetalico. |
| GB202115335D0 (en) | 2021-10-25 | 2021-12-08 | Econic Tech Ltd | Surface-active agent |
| GB2626546A (en) | 2023-01-25 | 2024-07-31 | Econic Tech Ltd | Surface-active agent |
| GB2626989A (en) | 2023-02-10 | 2024-08-14 | Econic Tech Ltd | Surface-active agent |
| EP4702078A1 (de) | 2023-04-25 | 2026-03-04 | Unilever IP Holdings B.V. | Zusammensetzungen |
| GB2629367A (en) | 2023-04-25 | 2024-10-30 | Econic Tech Ltd | Surface-active agent |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5158922A (en) | 1992-02-04 | 1992-10-27 | Arco Chemical Technology, L.P. | Process for preparing metal cyanide complex catalyst |
| CA2138063C (en) * | 1993-12-23 | 2007-02-20 | Bi Le-Khac | Polyurethane foam-supported double metal cyanide catalysts for polyol synthesis |
| US5767323A (en) * | 1995-12-22 | 1998-06-16 | Arco Chemical Technology, L.P. | Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation |
| US5777177A (en) † | 1996-02-07 | 1998-07-07 | Arco Chemical Technology, L.P. | Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter |
| US5689012A (en) † | 1996-07-18 | 1997-11-18 | Arco Chemical Technology, L.P. | Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter |
| US5900384A (en) * | 1996-07-18 | 1999-05-04 | Arco Chemical Technology L.P. | Double metal cyanide catalysts |
| US5783513A (en) * | 1997-03-13 | 1998-07-21 | Arco Chemical Technology, L.P. | Process for making double metal cyanide catalysts |
| DE19730467A1 (de) | 1997-07-16 | 1999-01-21 | Bayer Ag | Neue Zink/Metall-Hexacyanocobaltat-Katalysatoren für die Herstellung von Polyetherpolyolen |
| US5952261A (en) † | 1998-03-20 | 1999-09-14 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts modified with Group IIA compounds |
| US6423662B1 (en) * | 1999-07-09 | 2002-07-23 | Dow Global Technologies Inc. | Incipient wetness method for making metal-containing cyanide catalysts |
| AR024682A1 (es) † | 1999-07-09 | 2002-10-23 | Dow Chemical Co | Metodo para la preparacion de catalizadores de cianuro de metal mediante el uso de acidos policarboxilicos, y un proceso para polimerizar oxidos dealquileno. |
| KR20020030779A (ko) | 1999-07-09 | 2002-04-25 | 그래햄 이. 테일러 | 금속 시안화물 촉매와 불포화 개시제 화합물을 사용하는알킬렌 옥사이드의 중합 |
| CA2404652A1 (en) | 2000-03-30 | 2001-10-04 | Shell Internationale Research Maatschappij B.V. | Dmc complex catalyst and process for its preparation |
| IT1318530B1 (it) | 2000-05-19 | 2003-08-27 | Enichem Spa | Sistema catalitico a base di cianuri bimetallici e loro impiego nellasintesi di polieteri-polioli. |
-
2003
- 2003-06-10 US US10/457,988 patent/US6716788B2/en not_active Expired - Lifetime
- 2003-06-13 CN CN038138441A patent/CN1662303B/zh not_active Expired - Lifetime
- 2003-06-13 JP JP2004512913A patent/JP2005529994A/ja active Pending
- 2003-06-13 KR KR1020047020359A patent/KR100945698B1/ko not_active Expired - Lifetime
- 2003-06-13 EP EP03759958A patent/EP1515801B2/de not_active Expired - Lifetime
- 2003-06-13 AT AT03759958T patent/ATE307668T1/de not_active IP Right Cessation
- 2003-06-13 AU AU2003242705A patent/AU2003242705A1/en not_active Abandoned
- 2003-06-13 DE DE60302073T patent/DE60302073T3/de not_active Expired - Lifetime
- 2003-06-13 WO PCT/EP2003/006279 patent/WO2003106025A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| JP2005529994A (ja) | 2005-10-06 |
| EP1515801A1 (de) | 2005-03-23 |
| CN1662303B (zh) | 2010-05-12 |
| DE60302073T3 (de) | 2009-10-08 |
| EP1515801B1 (de) | 2005-10-26 |
| KR100945698B1 (ko) | 2010-03-05 |
| US6716788B2 (en) | 2004-04-06 |
| DE60302073D1 (de) | 2005-12-01 |
| DE60302073T2 (de) | 2006-07-13 |
| EP1515801B2 (de) | 2008-11-05 |
| AU2003242705A1 (en) | 2003-12-31 |
| CN1662303A (zh) | 2005-08-31 |
| US20030236162A1 (en) | 2003-12-25 |
| KR20050004922A (ko) | 2005-01-12 |
| WO2003106025A1 (en) | 2003-12-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |