ATE316812T1 - Methode und apparat zur automatischen extraktion von analyt - Google Patents
Methode und apparat zur automatischen extraktion von analytInfo
- Publication number
- ATE316812T1 ATE316812T1 AT96908637T AT96908637T ATE316812T1 AT E316812 T1 ATE316812 T1 AT E316812T1 AT 96908637 T AT96908637 T AT 96908637T AT 96908637 T AT96908637 T AT 96908637T AT E316812 T1 ATE316812 T1 AT E316812T1
- Authority
- AT
- Austria
- Prior art keywords
- cell
- extraction
- fluid
- analyte
- assembly
- Prior art date
Links
- 238000000605 extraction Methods 0.000 title abstract 6
- 239000012491 analyte Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- 239000012530 fluid Substances 0.000 abstract 7
- 238000000638 solvent extraction Methods 0.000 abstract 2
- 238000011109 contamination Methods 0.000 abstract 1
- 238000011010 flushing procedure Methods 0.000 abstract 1
- 238000010926 purge Methods 0.000 abstract 1
- 238000000194 supercritical-fluid extraction Methods 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0203—Solvent extraction of solids with a supercritical fluid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0207—Control systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0269—Solid material in other moving receptacles
- B01D11/0273—Solid material in other moving receptacles in rotating drums
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
- B01D11/0284—Multistage extraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/043—Carbonates or bicarbonates, e.g. limestone, dolomite, aragonite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
- B01J20/3204—Inorganic carriers, supports or substrates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
- B01J20/3234—Inorganic material layers
- B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N1/4055—Concentrating samples by solubility techniques
- G01N2001/4061—Solvent extraction
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N2030/009—Extraction
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/25—Chemistry: analytical and immunological testing including sample preparation
- Y10T436/25375—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.]
- Y10T436/255—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.] including use of a solid sorbent, semipermeable membrane, or liquid extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Molecular Biology (AREA)
- Biomedical Technology (AREA)
- Automation & Control Theory (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/398,140 US5660727A (en) | 1994-06-14 | 1995-03-03 | Automated analyte supercritical fluid extraction apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE316812T1 true ATE316812T1 (de) | 2006-02-15 |
Family
ID=23574149
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT96908637T ATE316812T1 (de) | 1995-03-03 | 1996-02-29 | Methode und apparat zur automatischen extraktion von analyt |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US5660727A (de) |
| EP (1) | EP0820334B1 (de) |
| JP (1) | JP4060354B2 (de) |
| AT (1) | ATE316812T1 (de) |
| AU (1) | AU695104B2 (de) |
| CA (1) | CA2214526C (de) |
| DE (1) | DE69635777T2 (de) |
| WO (1) | WO1996027417A1 (de) |
Families Citing this family (53)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5660727A (en) * | 1994-06-14 | 1997-08-26 | Dionex Corporation | Automated analyte supercritical fluid extraction apparatus |
| EP0791815A3 (de) * | 1996-02-20 | 1998-09-09 | Leco Corporation | Einrichtung zur Extraktion von Analyten einer Probe unter Druck |
| US6890491B1 (en) * | 1997-06-10 | 2005-05-10 | Pharmacopeia Drug Discovery, Inc. | Method and apparatus for universal fluid exchange |
| WO1999018421A1 (en) * | 1997-10-03 | 1999-04-15 | Monterey Bay Aquarium Research Institute | Aquatic autosampler device |
| AU759239B2 (en) * | 1997-11-28 | 2003-04-10 | Provalis Diagnostics Limited | Device and apparatus for conducting an assay |
| DK199801456A (da) * | 1998-11-10 | 2000-05-11 | Fls Miljoe A S | Fremgangsmåde til imprægnering eller ekstrahering af et harpiksholdigt træsubstrat |
| DK199801455A (da) | 1998-11-10 | 2000-05-11 | Fls Miljoe A S | Fremgangsmåde til imprægnering eller ekstrahering af et harpiksholdigt træsubstrat |
| US6180069B1 (en) | 1999-02-18 | 2001-01-30 | Leco Corporation | Cleaning system and method for cleaning a flow restrictor in a supercritical fluid extraction system |
| US6319476B1 (en) | 1999-03-02 | 2001-11-20 | Perseptive Biosystems, Inc. | Microfluidic connector |
| US6184039B1 (en) * | 1999-05-04 | 2001-02-06 | Andrew R. Komarek | Method for determining the fat content of feed, food, and other materials utilizing filter media encapsulation |
| CN1104921C (zh) * | 1999-08-17 | 2003-04-09 | 吴士杰 | 一种无高压泵的可实现工业化超临界流体萃取装置 |
| EP1136808A1 (de) * | 2000-03-20 | 2001-09-26 | Carlo Squicciarini | Automatisches System für die Extraktion und Analyse von restlichen Lösungsmittel in Materialproben |
| EA013736B1 (ru) * | 2000-03-28 | 2010-06-30 | Биркен Гмбх | Эмульсия, содержащая растительный экстракт, в частности экстракт берёзовой коры, и ее применение |
| GB0021887D0 (en) * | 2000-09-06 | 2000-10-18 | Provalis Diagnostics Ltd | Assay device |
| US20030096422A1 (en) * | 2001-11-16 | 2003-05-22 | Ong Eng Shi | Pressurized liquid extraction method and apparatus |
| US20040101444A1 (en) * | 2002-07-15 | 2004-05-27 | Xeotron Corporation | Apparatus and method for fluid delivery to a hybridization station |
| AU2003282482A1 (en) * | 2002-10-09 | 2004-05-04 | Fluid Management Systems, Inc. | Integrated pressurized liquid extraction and purification system |
| WO2005052551A1 (ja) * | 2003-11-26 | 2005-06-09 | Mitsubishi Denki Kabushiki Kaisha | 微量含有物の分析方法 |
| CA2620666C (en) | 2005-12-09 | 2014-04-01 | Alfa Wassermann, Inc. | Automated fraction collection system |
| US20090221079A1 (en) | 2008-02-28 | 2009-09-03 | Dionex Corporation | Sample pretreatment and extraction |
| US7908934B2 (en) * | 2008-02-29 | 2011-03-22 | Dionex Corporation | Valve assembly |
| WO2010087109A1 (ja) * | 2009-01-29 | 2010-08-05 | 株式会社 日立ハイテクノロジーズ | 生体サンプルの前処理装置、及びそれを備えた質量分析装置 |
| JP5242787B2 (ja) * | 2009-06-25 | 2013-07-24 | 株式会社日立ハイテクノロジーズ | 前処理装置及びそれを備えた質量分析装置 |
| JP5611951B2 (ja) * | 2009-08-10 | 2014-10-22 | 株式会社日立ハイテクノロジーズ | 試料処理システム |
| JP5440871B2 (ja) | 2010-08-20 | 2014-03-12 | 株式会社ダイフク | 容器保管設備 |
| CN102527078B (zh) * | 2010-12-28 | 2014-06-18 | 上海光谱仪器有限公司 | 一种萃取池防反喷装置及萃取池 |
| DE102011105555A1 (de) * | 2011-06-25 | 2012-12-27 | Hydac Filtertechnik Gmbh | Filtervorrichtung |
| US9459184B2 (en) | 2012-03-08 | 2016-10-04 | Dionex Corporation | Sorption of water from a sample using a polymeric drying agent |
| US9440166B2 (en) * | 2012-08-30 | 2016-09-13 | Dionex Corporation | Method and device to extract an analyte from a sample with gas assistance |
| US11123655B2 (en) | 2013-02-13 | 2021-09-21 | Dionex Corporation | Apparatus for parallel accelerated solvent extraction |
| JP6070450B2 (ja) * | 2013-01-22 | 2017-02-01 | 株式会社島津製作所 | 超臨界流体成分抽出装置 |
| US9375697B2 (en) | 2014-03-12 | 2016-06-28 | Dionex Corporation | Extraction cell assembly with quick-release seal removal |
| WO2016115111A1 (en) * | 2015-01-12 | 2016-07-21 | Advion Inc. | Surface extraction interface |
| US9739692B2 (en) | 2015-03-27 | 2017-08-22 | Dionex Corporation | Pump-less method and apparatus for solvent extraction from a sample |
| EP3405847A4 (de) | 2016-01-20 | 2019-10-30 | Waters Technologies Corporation | Systeme, verfahren und vorrichtungen für probenextraktions- und injektionsprobleme in der chromatografie |
| US10456709B2 (en) * | 2016-05-10 | 2019-10-29 | Green Mill Supercritical, Inc. | Dispersion flow device for extraction vessel and methods of use |
| US10330573B2 (en) | 2017-07-10 | 2019-06-25 | Cem Corporation | Rapid sample preparation for analytical analysis using dispersive energized extraction |
| US10295447B2 (en) | 2017-07-10 | 2019-05-21 | Cem Corporation | Rapid energized dispersive solid phase extraction (SPE) for analytical analysis |
| US10241014B2 (en) | 2017-07-10 | 2019-03-26 | Cem Corporation | Instrument for analytical sample preparation |
| EP3466512B1 (de) * | 2017-10-09 | 2020-04-29 | SEPIAtec GmbH | Sammlermodul für ein sfc-system |
| CN111356479A (zh) | 2018-01-04 | 2020-06-30 | 安瑞特研究有限公司 | 含有白桦脂醇的桦树皮提取物及其制剂 |
| US11050777B2 (en) | 2018-11-20 | 2021-06-29 | Saudi Arabian Oil Company | Method and system for remediating cybersecurity vulnerabilities based on utilization |
| US10858596B2 (en) * | 2019-03-06 | 2020-12-08 | Saudi Arabian Oil Company | Separation of fractions in hydrocarbon samples using an accelerated solvent extractor |
| CN115516308B (zh) * | 2020-03-17 | 2025-08-19 | 沃特世科技公司 | 针驱动器、系统和方法 |
| CN115667908B (zh) * | 2020-03-17 | 2026-02-10 | 沃特世科技公司 | 样品管理器、系统和方法 |
| CN114264539B (zh) * | 2020-09-16 | 2024-06-28 | 中国烟草总公司郑州烟草研究院 | 溶剂辅助的热解析设备 |
| US11684877B2 (en) | 2020-09-30 | 2023-06-27 | Dionex Corporation | Extraction cell cap assembly with toolless disassembly |
| WO2022129287A1 (en) * | 2020-12-18 | 2022-06-23 | Unilever Ip Holdings B.V. | A method |
| DE102020134836B3 (de) | 2020-12-23 | 2022-03-24 | LCTech GmbH | Extraktionssystem zur Extraktion von Analyten aus einer Probe |
| CN114894593B (zh) | 2022-06-16 | 2026-03-31 | 赛默飞世尔(上海)仪器有限公司 | 样品制备系统及通过其从样品中萃取待分析物的方法 |
| WO2025144546A1 (en) | 2023-12-26 | 2025-07-03 | Dionex Corporation | Apparatus for concomitant and parallel microsample extraction and microextract concentration |
| FR3159751A1 (fr) | 2024-03-01 | 2025-09-05 | Universite D'aix Marseille | Appareil de traitement d’un échantillon liquide ou solide avec du dioxyde de carbone supercritique |
| WO2025240164A1 (en) | 2024-05-17 | 2025-11-20 | Dionex Corporation | Methods and devices for streamline extraction, clean-up, and enrichment of target analytes from solid and semi-solid samples |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3418084A (en) * | 1966-10-27 | 1968-12-24 | Instrumentation Specialties Co | Rectangular fraction collector |
| US4168955A (en) * | 1977-03-28 | 1979-09-25 | Instrumentation Specialties Company | Chemical analyzer |
| US4335620A (en) * | 1980-07-16 | 1982-06-22 | The Upjohn Company | Temperature controlled sample carrier |
| US4429584A (en) * | 1981-12-01 | 1984-02-07 | The Upjohn Company | Microprocessor controllable automatic sampler |
| US4711764A (en) * | 1982-10-08 | 1987-12-08 | Analytichem International, Inc. | Automatic sample injector and disposable sample cassette |
| US5193703A (en) * | 1990-03-02 | 1993-03-16 | Hewlett-Packard Company | Methods and apparatus for forming an integral high pressure seal using mechanical actuation |
| US5133859A (en) * | 1990-03-02 | 1992-07-28 | Hewlett-Packard Company | Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids |
| US5198197A (en) * | 1990-07-13 | 1993-03-30 | Isco, Inc. | Apparatus and method for supercritical fluid extraction |
| US5601707A (en) * | 1990-07-13 | 1997-02-11 | Isco, Inc. | Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography |
| US5614089A (en) * | 1990-07-13 | 1997-03-25 | Isco, Inc. | Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography |
| US5250195A (en) * | 1990-07-13 | 1993-10-05 | Isco, Inc. | Apparatus and method for supercritical fluid extraction |
| US5160624A (en) * | 1990-07-13 | 1992-11-03 | Isco, Inc. | Apparatus and method for supercritical fluid extraction |
| US5173188A (en) * | 1990-07-13 | 1992-12-22 | Isco, Inc. | Apparatus and method for supercritical fluid extraction |
| US5132014A (en) * | 1990-07-13 | 1992-07-21 | Isco, Inc. | Apparatus and method for supercritical fluid extraction |
| US5268102A (en) * | 1990-07-13 | 1993-12-07 | Isco, Inc. | Apparatus and method for supercritical fluid extraction |
| US5205987A (en) * | 1991-02-28 | 1993-04-27 | Suprex Corporation | Off-line supercritical fluid extraction collection system |
| EP0619751B1 (de) * | 1992-10-16 | 2003-05-07 | Suprex Corporation | Automatisierte extrakion mittels eines superkritischen fluidum |
| US5660727A (en) * | 1994-06-14 | 1997-08-26 | Dionex Corporation | Automated analyte supercritical fluid extraction apparatus |
-
1995
- 1995-03-03 US US08/398,140 patent/US5660727A/en not_active Expired - Lifetime
-
1996
- 1996-02-29 WO PCT/US1996/002945 patent/WO1996027417A1/en not_active Ceased
- 1996-02-29 CA CA002214526A patent/CA2214526C/en not_active Expired - Fee Related
- 1996-02-29 JP JP52699696A patent/JP4060354B2/ja not_active Expired - Fee Related
- 1996-02-29 DE DE69635777T patent/DE69635777T2/de not_active Expired - Lifetime
- 1996-02-29 AT AT96908637T patent/ATE316812T1/de not_active IP Right Cessation
- 1996-02-29 EP EP96908637A patent/EP0820334B1/de not_active Expired - Lifetime
- 1996-02-29 AU AU51815/96A patent/AU695104B2/en not_active Ceased
-
1997
- 1997-03-18 US US08/820,771 patent/US5785856A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0820334B1 (de) | 2006-02-01 |
| US5660727A (en) | 1997-08-26 |
| CA2214526C (en) | 2001-01-16 |
| DE69635777T2 (de) | 2006-10-12 |
| CA2214526A1 (en) | 1996-09-12 |
| JP4060354B2 (ja) | 2008-03-12 |
| AU695104B2 (en) | 1998-08-06 |
| EP0820334A4 (de) | 1998-12-09 |
| JPH11501567A (ja) | 1999-02-09 |
| WO1996027417A1 (en) | 1996-09-12 |
| EP0820334A1 (de) | 1998-01-28 |
| DE69635777D1 (de) | 2006-04-13 |
| US5785856A (en) | 1998-07-28 |
| AU5181596A (en) | 1996-09-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |