ATE316812T1 - Methode und apparat zur automatischen extraktion von analyt - Google Patents

Methode und apparat zur automatischen extraktion von analyt

Info

Publication number
ATE316812T1
ATE316812T1 AT96908637T AT96908637T ATE316812T1 AT E316812 T1 ATE316812 T1 AT E316812T1 AT 96908637 T AT96908637 T AT 96908637T AT 96908637 T AT96908637 T AT 96908637T AT E316812 T1 ATE316812 T1 AT E316812T1
Authority
AT
Austria
Prior art keywords
cell
extraction
fluid
analyte
assembly
Prior art date
Application number
AT96908637T
Other languages
English (en)
Inventor
Gary L Gleave
Norman J Rothe
David W Kemp
Bruce E Richter
John L Ezzell
Original Assignee
Dionex Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dionex Corp filed Critical Dionex Corp
Application granted granted Critical
Publication of ATE316812T1 publication Critical patent/ATE316812T1/de

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/34—Purifying; Cleaning
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0203—Solvent extraction of solids with a supercritical fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0207—Control systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0269—Solid material in other moving receptacles
    • B01D11/0273—Solid material in other moving receptacles in rotating drums
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/028—Flow sheets
    • B01D11/0284—Multistage extraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/043—Carbonates or bicarbonates, e.g. limestone, dolomite, aragonite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40—Concentrating samples
    • G01N1/4055—Concentrating samples by solubility techniques
    • G01N2001/4061—Solvent extraction
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N2030/009—Extraction
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/25—Chemistry: analytical and immunological testing including sample preparation
    • Y10T436/25375—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.]
    • Y10T436/255—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.] including use of a solid sorbent, semipermeable membrane, or liquid extraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Automation & Control Theory (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analysing Biological Materials (AREA)
  • Extraction Or Liquid Replacement (AREA)
AT96908637T 1995-03-03 1996-02-29 Methode und apparat zur automatischen extraktion von analyt ATE316812T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/398,140 US5660727A (en) 1994-06-14 1995-03-03 Automated analyte supercritical fluid extraction apparatus

Publications (1)

Publication Number Publication Date
ATE316812T1 true ATE316812T1 (de) 2006-02-15

Family

ID=23574149

Family Applications (1)

Application Number Title Priority Date Filing Date
AT96908637T ATE316812T1 (de) 1995-03-03 1996-02-29 Methode und apparat zur automatischen extraktion von analyt

Country Status (8)

Country Link
US (2) US5660727A (de)
EP (1) EP0820334B1 (de)
JP (1) JP4060354B2 (de)
AT (1) ATE316812T1 (de)
AU (1) AU695104B2 (de)
CA (1) CA2214526C (de)
DE (1) DE69635777T2 (de)
WO (1) WO1996027417A1 (de)

Families Citing this family (53)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5660727A (en) * 1994-06-14 1997-08-26 Dionex Corporation Automated analyte supercritical fluid extraction apparatus
EP0791815A3 (de) * 1996-02-20 1998-09-09 Leco Corporation Einrichtung zur Extraktion von Analyten einer Probe unter Druck
US6890491B1 (en) * 1997-06-10 2005-05-10 Pharmacopeia Drug Discovery, Inc. Method and apparatus for universal fluid exchange
WO1999018421A1 (en) * 1997-10-03 1999-04-15 Monterey Bay Aquarium Research Institute Aquatic autosampler device
AU759239B2 (en) * 1997-11-28 2003-04-10 Provalis Diagnostics Limited Device and apparatus for conducting an assay
DK199801455A (da) * 1998-11-10 2000-05-11 Fls Miljoe A S Fremgangsmåde til imprægnering eller ekstrahering af et harpiksholdigt træsubstrat
DK199801456A (da) * 1998-11-10 2000-05-11 Fls Miljoe A S Fremgangsmåde til imprægnering eller ekstrahering af et harpiksholdigt træsubstrat
US6180069B1 (en) 1999-02-18 2001-01-30 Leco Corporation Cleaning system and method for cleaning a flow restrictor in a supercritical fluid extraction system
US6319476B1 (en) 1999-03-02 2001-11-20 Perseptive Biosystems, Inc. Microfluidic connector
US6184039B1 (en) * 1999-05-04 2001-02-06 Andrew R. Komarek Method for determining the fat content of feed, food, and other materials utilizing filter media encapsulation
CN1104921C (zh) * 1999-08-17 2003-04-09 吴士杰 一种无高压泵的可实现工业化超临界流体萃取装置
EP1136808A1 (de) * 2000-03-20 2001-09-26 Carlo Squicciarini Automatisches System für die Extraktion und Analyse von restlichen Lösungsmittel in Materialproben
PT1267900E (pt) * 2000-03-28 2004-08-31 Birken Gmbh Emulsao contendo um extracto de planta contendo um triterpeno processo para a preparacao desta emulsao e para a obtencao do extracto de planta
GB0021887D0 (en) * 2000-09-06 2000-10-18 Provalis Diagnostics Ltd Assay device
US20030096422A1 (en) * 2001-11-16 2003-05-22 Ong Eng Shi Pressurized liquid extraction method and apparatus
US20040101444A1 (en) * 2002-07-15 2004-05-27 Xeotron Corporation Apparatus and method for fluid delivery to a hybridization station
EP1556150A4 (de) * 2002-10-09 2008-03-19 Fluid Man Systems Inc Integrierte flüssigkeitsextraktion unterdruck und reinigungssystem
WO2005052551A1 (ja) * 2003-11-26 2005-06-09 Mitsubishi Denki Kabushiki Kaisha 微量含有物の分析方法
EP3002062A3 (de) * 2005-12-09 2016-05-25 Alfa Wassermann, Inc. Probe-teilvolumen-messvorrichtung für ein automatisiertes probeentnahmesystem
US20090221079A1 (en) 2008-02-28 2009-09-03 Dionex Corporation Sample pretreatment and extraction
US7908934B2 (en) * 2008-02-29 2011-03-22 Dionex Corporation Valve assembly
WO2010087109A1 (ja) * 2009-01-29 2010-08-05 株式会社 日立ハイテクノロジーズ 生体サンプルの前処理装置、及びそれを備えた質量分析装置
WO2010150842A1 (ja) * 2009-06-25 2010-12-29 株式会社日立ハイテクノロジーズ 前処理装置及びそれを備えた質量分析装置
CN102472692B (zh) * 2009-08-10 2015-01-07 株式会社日立高新技术 试样处理系统
JP5440871B2 (ja) 2010-08-20 2014-03-12 株式会社ダイフク 容器保管設備
CN102527078B (zh) * 2010-12-28 2014-06-18 上海光谱仪器有限公司 一种萃取池防反喷装置及萃取池
DE102011105555A1 (de) * 2011-06-25 2012-12-27 Hydac Filtertechnik Gmbh Filtervorrichtung
US9459184B2 (en) 2012-03-08 2016-10-04 Dionex Corporation Sorption of water from a sample using a polymeric drying agent
US11123655B2 (en) 2013-02-13 2021-09-21 Dionex Corporation Apparatus for parallel accelerated solvent extraction
US9440166B2 (en) 2012-08-30 2016-09-13 Dionex Corporation Method and device to extract an analyte from a sample with gas assistance
JP6070450B2 (ja) * 2013-01-22 2017-02-01 株式会社島津製作所 超臨界流体成分抽出装置
US9375697B2 (en) 2014-03-12 2016-06-28 Dionex Corporation Extraction cell assembly with quick-release seal removal
JP6670315B2 (ja) * 2015-01-12 2020-03-18 アドヴィオン インコーポレーテッドＡｄｖｉｏｎ Ｉｎｃ． 表面抽出インタフェース
US9739692B2 (en) 2015-03-27 2017-08-22 Dionex Corporation Pump-less method and apparatus for solvent extraction from a sample
EP3405847A4 (de) 2016-01-20 2019-10-30 Waters Technologies Corporation Systeme, verfahren und vorrichtungen für probenextraktions- und injektionsprobleme in der chromatografie
US10456709B2 (en) * 2016-05-10 2019-10-29 Green Mill Supercritical, Inc. Dispersion flow device for extraction vessel and methods of use
US10295447B2 (en) 2017-07-10 2019-05-21 Cem Corporation Rapid energized dispersive solid phase extraction (SPE) for analytical analysis
US10241014B2 (en) 2017-07-10 2019-03-26 Cem Corporation Instrument for analytical sample preparation
US10330573B2 (en) 2017-07-10 2019-06-25 Cem Corporation Rapid sample preparation for analytical analysis using dispersive energized extraction
EP3466512B1 (de) * 2017-10-09 2020-04-29 SEPIAtec GmbH Sammlermodul für ein sfc-system
BR112020009867A2 (pt) 2018-01-04 2020-11-03 Amryt Research Limited composição formadora de cremosidade
US11050777B2 (en) 2018-11-20 2021-06-29 Saudi Arabian Oil Company Method and system for remediating cybersecurity vulnerabilities based on utilization
US10858596B2 (en) 2019-03-06 2020-12-08 Saudi Arabian Oil Company Separation of fractions in hydrocarbon samples using an accelerated solvent extractor
EP4121753A1 (de) * 2020-03-17 2023-01-25 Waters Technologies Corporation Probenmanager, system und verfahren
US11913916B2 (en) 2020-03-17 2024-02-27 Waters Technologies Corporation Needle drive, system and method
CN114264539B (zh) * 2020-09-16 2024-06-28 中国烟草总公司郑州烟草研究院 溶剂辅助的热解析设备
US11684877B2 (en) 2020-09-30 2023-06-27 Dionex Corporation Extraction cell cap assembly with toolless disassembly
US12436071B2 (en) * 2020-12-18 2025-10-07 Conopco, Inc. Method
DE102020134836B3 (de) 2020-12-23 2022-03-24 LCTech GmbH Extraktionssystem zur Extraktion von Analyten aus einer Probe
CN114894593B (zh) * 2022-06-16 2026-03-31 赛默飞世尔（上海）仪器有限公司 样品制备系统及通过其从样品中萃取待分析物的方法
CN122180868A (zh) 2023-12-26 2026-06-09 戴安公司 用于伴随式且并行的微量样品萃取和微萃取浓缩的装置
FR3159751A1 (fr) 2024-03-01 2025-09-05 Universite D'aix Marseille Appareil de traitement d’un échantillon liquide ou solide avec du dioxyde de carbone supercritique
WO2025240164A1 (en) 2024-05-17 2025-11-20 Dionex Corporation Methods and devices for streamline extraction, clean-up, and enrichment of target analytes from solid and semi-solid samples

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3418084A (en) * 1966-10-27 1968-12-24 Instrumentation Specialties Co Rectangular fraction collector
US4168955A (en) * 1977-03-28 1979-09-25 Instrumentation Specialties Company Chemical analyzer
US4335620A (en) * 1980-07-16 1982-06-22 The Upjohn Company Temperature controlled sample carrier
US4429584A (en) * 1981-12-01 1984-02-07 The Upjohn Company Microprocessor controllable automatic sampler
US4711764A (en) * 1982-10-08 1987-12-08 Analytichem International, Inc. Automatic sample injector and disposable sample cassette
US5193703A (en) * 1990-03-02 1993-03-16 Hewlett-Packard Company Methods and apparatus for forming an integral high pressure seal using mechanical actuation
US5133859A (en) * 1990-03-02 1992-07-28 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5601707A (en) * 1990-07-13 1997-02-11 Isco, Inc. Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography
US5198197A (en) * 1990-07-13 1993-03-30 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5160624A (en) * 1990-07-13 1992-11-03 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5173188A (en) * 1990-07-13 1992-12-22 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5614089A (en) * 1990-07-13 1997-03-25 Isco, Inc. Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography
US5268102A (en) * 1990-07-13 1993-12-07 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5132014A (en) * 1990-07-13 1992-07-21 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5250195A (en) * 1990-07-13 1993-10-05 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5205987A (en) * 1991-02-28 1993-04-27 Suprex Corporation Off-line supercritical fluid extraction collection system
EP0619751B1 (de) * 1992-10-16 2003-05-07 Suprex Corporation Automatisierte extrakion mittels eines superkritischen fluidum
US5660727A (en) * 1994-06-14 1997-08-26 Dionex Corporation Automated analyte supercritical fluid extraction apparatus

Also Published As

Publication number Publication date
DE69635777T2 (de) 2006-10-12
WO1996027417A1 (en) 1996-09-12
CA2214526A1 (en) 1996-09-12
EP0820334B1 (de) 2006-02-01
US5785856A (en) 1998-07-28
EP0820334A4 (de) 1998-12-09
EP0820334A1 (de) 1998-01-28
JPH11501567A (ja) 1999-02-09
AU5181596A (en) 1996-09-23
JP4060354B2 (ja) 2008-03-12
CA2214526C (en) 2001-01-16
DE69635777D1 (de) 2006-04-13
AU695104B2 (en) 1998-08-06
US5660727A (en) 1997-08-26

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