ATE321896T1 - Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure - Google Patents

Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure

Info

Publication number: ATE321896T1
Authority: AT; Austria
Prior art keywords: phosphoric acid; hydrogen peroxide; uranium; acid; weak
Prior art date: 2003-03-31

Application number

AT03733002T

Other languages

English (en)

Inventor

Harvinderpal Reds Materi Singh

Shyamkant Laxmidutt Red Mishra

Anitha Reds Materi Mallavarapu

Vijayalakshmi Reds Ravishankar

Ashok Baswanthappa Giriyalkar

Manojkumar Kedarnath R Kotekar

Tapan Kumar Indian R Mukherjee

Marg Prabhadevi Savarkar

Original Assignee

Secretary Dept Atomic Energy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2003-03-31

Filing date

2003-03-31

Publication date

2006-04-15

2003-03-31 Application filed by Secretary Dept Atomic Energy filed Critical Secretary Dept Atomic Energy

2006-04-15 Application granted granted Critical

2006-04-15 Publication of ATE321896T1 publication Critical patent/ATE321896T1/de

Links

NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title abstract 10
229910000147 aluminium phosphate Inorganic materials 0.000 title abstract 5
229910052770 Uranium Inorganic materials 0.000 title abstract 3
239000003337 fertilizer Substances 0.000 title abstract 2
238000000034 method Methods 0.000 title abstract 2
JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 title abstract 2
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 6
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 4
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
SEGLCEQVOFDUPX-UHFFFAOYSA-N di-(2-ethylhexyl)phosphoric acid Chemical compound CCCCC(CC)COP(O)(=O)OCC(CC)CCCC SEGLCEQVOFDUPX-UHFFFAOYSA-N 0.000 abstract 2
238000000605 extraction Methods 0.000 abstract 2
229910052742 iron Inorganic materials 0.000 abstract 2
STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 abstract 2
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
239000002253 acid Substances 0.000 abstract 1
239000003513 alkali Substances 0.000 abstract 1
ZAASRHQPRFFWCS-UHFFFAOYSA-P diazanium;oxygen(2-);uranium Chemical compound [NH4+].[NH4+].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[U].[U] ZAASRHQPRFFWCS-UHFFFAOYSA-P 0.000 abstract 1
239000003350 kerosene Substances 0.000 abstract 1
239000002244 precipitate Substances 0.000 abstract 1
230000001376 precipitating effect Effects 0.000 abstract 1
238000011084 recovery Methods 0.000 abstract 1
229910052708 sodium Inorganic materials 0.000 abstract 1
239000011734 sodium Substances 0.000 abstract 1
230000002195 synergetic effect Effects 0.000 abstract 1
-1 uranium peroxide Chemical class 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
- C22B3/384—Pentavalent phosphorus oxyacids, esters thereof
- C22B3/3846—Phosphoric acid, e.g. (O)P(OH)3
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/026—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries liquid-liquid extraction with or without dissolution in organic solvents
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0221—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching
- C22B60/0226—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching using acidic solutions or liquors
- C22B60/0243—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching using acidic solutions or liquors phosphorated ion as active agent
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/0278—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries by chemical methods
- C22B60/0282—Solutions containing P ions, e.g. treatment of solutions resulting from the leaching of phosphate ores or recovery of uranium from wet-process phosphoric acid
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling

Landscapes

Engineering & Computer Science (AREA)
Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
General Life Sciences & Earth Sciences (AREA)
Materials Engineering (AREA)
Geology (AREA)
Manufacturing & Machinery (AREA)
Environmental & Geological Engineering (AREA)
Mechanical Engineering (AREA)
Metallurgy (AREA)
Organic Chemistry (AREA)
Geochemistry & Mineralogy (AREA)
Extraction Or Liquid Replacement (AREA)
Manufacture And Refinement Of Metals (AREA)
Fertilizers (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Inorganic Compounds Of Heavy Metals (AREA)

AT03733002T 2003-03-31 2003-03-31 Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure ATE321896T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
PCT/IN2003/000132 WO2004087971A1 (en)	2003-03-31	2003-03-31	A process for recovery of high purity uranium from fertilizer grade weak phosphoric acid

Publications (1)

Publication Number	Publication Date
ATE321896T1 true ATE321896T1 (de)	2006-04-15

Family

ID=33104981

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT03733002T ATE321896T1 (de)	2003-03-31	2003-03-31	Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure

Country Status (7)

Country	Link
US (1)	US7192563B2 (de)
EP (1)	EP1511869B9 (de)
AT (1)	ATE321896T1 (de)
AU (1)	AU2003238666A1 (de)
DE (1)	DE60304330T2 (de)
ES (1)	ES2261944T3 (de)
WO (1)	WO2004087971A1 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN100400687C (zh) *	2006-10-30	2008-07-09	北京斯帕顿矿产资源投资咨询有限公司	从磷酸盐中提取放射性铀的方法
CN100387734C (zh) *	2006-10-30	2008-05-14	北京斯帕顿矿产资源投资咨询有限公司	从粉煤灰中提取放射性铀的方法
UA98370C2 (ru)	2007-12-26	2012-05-10	Ториум Пауэр Инк.	Ядерный реактор (варианты), топливная сборка из зажигающе-воспроизводящих модулей для ядерного реактора (варианты) и топливный элемент топливной сборки
US8116423B2 (en)	2007-12-26	2012-02-14	Thorium Power, Inc.	Nuclear reactor (alternatives), fuel assembly of seed-blanket subassemblies for nuclear reactor (alternatives), and fuel element for fuel assembly
JP5755568B2 (ja)	2008-12-25	2015-07-29	トリウム・パワー、インクＴｈｏｒｉｕｍＰｏｗｅｒ，Ｉｎｃ．	軽水炉核燃料集合体および軽水炉
EP2512614A1 (de) *	2009-12-15	2012-10-24	Cytec Technology Corp.	Verfahren und zusammensetzungen zur entfernung von unreinheiten aus einer mit unreinheiten belasteten ionischen flüssigkeit
FI122274B (fi) *	2010-02-02	2011-11-15	Outotec Oyj	Uuttoprosessi
WO2011143172A1 (en)	2010-05-11	2011-11-17	Thorium Power, Inc.	Fuel assembly with metal fuel alloy kernel and method of manufacturing thereof
US10192644B2 (en)	2010-05-11	2019-01-29	Lightbridge Corporation	Fuel assembly
US10170207B2 (en)	2013-05-10	2019-01-01	Thorium Power, Inc.	Fuel assembly
CN106636690B (zh) *	2016-12-07	2018-05-18	中核四0四有限公司	一种酸性含硝酸铵含铀废水中铀的回收方法
CN115948665B (zh) *	2021-10-08	2024-10-18	中核矿业科技集团有限公司	一种高稳定性的铀纯化萃取方法
CN114686688A (zh) *	2021-10-25	2022-07-01	核工业北京化工冶金研究院	一种萃取法深度除铀方法
CN115849451A (zh) *	2022-11-11	2023-03-28	中核四0四有限公司	一种含铀废液的回收处理方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2352062A1 (fr)	1976-05-19	1977-12-16	Minemet Rech Sa	Procede pour l'extraction de l'uranium contenu dans les minerais phosphates.
US4258013A (en) *	1977-09-14	1981-03-24	Earth Sciences Inc.	Uranium recovery from wet process phosphoric acid
US4302427A (en) *	1979-03-19	1981-11-24	International Minerals & Chemical Corporation	Recovery of uranium from wet-process phosphoric acid
US4649029A (en) *	1984-04-13	1987-03-10	Inderjit Nirdosh	Processes for extraction of uranium and radium from uranium-containing ores using ferric nitrate

2002
- 2002-03-31 US US10/486,507 patent/US7192563B2/en not_active Expired - Fee Related
2003
- 2003-03-31 EP EP03733002A patent/EP1511869B9/de not_active Expired - Lifetime
- 2003-03-31 WO PCT/IN2003/000132 patent/WO2004087971A1/en not_active Ceased
- 2003-03-31 ES ES03733002T patent/ES2261944T3/es not_active Expired - Lifetime
- 2003-03-31 AT AT03733002T patent/ATE321896T1/de not_active IP Right Cessation
- 2003-03-31 DE DE60304330T patent/DE60304330T2/de not_active Expired - Lifetime
- 2003-03-31 AU AU2003238666A patent/AU2003238666A1/en not_active Abandoned

Also Published As

Publication number	Publication date
US20040247504A1 (en)	2004-12-09
WO2004087971A1 (en)	2004-10-14
EP1511869A1 (de)	2005-03-09
DE60304330T2 (de)	2006-11-30
EP1511869B1 (de)	2006-03-29
ES2261944T3 (es)	2006-11-16
DE60304330D1 (de)	2006-05-18
AU2003238666A1 (en)	2004-10-25
US7192563B2 (en)	2007-03-20
EP1511869B9 (de)	2006-10-11

Legal Events

Date	Code	Title	Description
2006-09-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties

Publication	Publication Date	Title
ATE321896T1 (de)	2006-04-15	Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure
Wang et al.	2012	Extraction and separation of cobalt (II), copper (II) and manganese (II) by Cyanex272, PC-88A and their mixtures
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ES8206387A1 (es)	1982-08-16	Procedimiento para la recuperacion del uranio (vi) presente en una solucion de acido fosforico.
CA1179148A (en)	1984-12-11	Process for recovering uranium using an alkyl pyrophosphoric acid and alkaline stripping solution
USRE31686E (en)	1984-09-25	Reductive stripping process for the recovery of uranium from wet-process phosphoric acid
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JPS54150311A (en)	1979-11-26	Extracting method for uranium from acidic aqueous solution