ATE328659T1 - Verfahren zur herstellung von titanhaltigen siliciumdioxidkatalysatoren - Google Patents

Verfahren zur herstellung von titanhaltigen siliciumdioxidkatalysatoren

Info

Publication number
ATE328659T1
ATE328659T1 AT02710350T AT02710350T ATE328659T1 AT E328659 T1 ATE328659 T1 AT E328659T1 AT 02710350 T AT02710350 T AT 02710350T AT 02710350 T AT02710350 T AT 02710350T AT E328659 T1 ATE328659 T1 AT E328659T1
Authority
AT
Austria
Prior art keywords
template
angstrom
carbon atoms
solid
solvent extraction
Prior art date
Application number
AT02710350T
Other languages
English (en)
Inventor
Jun Yamamoto
Junpei Tsuji
Original Assignee
Sumitomo Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co filed Critical Sumitomo Chemical Co
Application granted granted Critical
Publication of ATE328659T1 publication Critical patent/ATE328659T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/0308—Mesoporous materials not having base exchange properties, e.g. Si-MCM-41
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/617—500-1000 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/647—2-50 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
AT02710350T 2001-01-31 2002-01-25 Verfahren zur herstellung von titanhaltigen siliciumdioxidkatalysatoren ATE328659T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2001023248A JP4889865B2 (ja) 2001-01-31 2001-01-31 チタン含有珪素酸化物触媒の製造方法

Publications (1)

Publication Number Publication Date
ATE328659T1 true ATE328659T1 (de) 2006-06-15

Family

ID=18888559

Family Applications (1)

Application Number Title Priority Date Filing Date
AT02710350T ATE328659T1 (de) 2001-01-31 2002-01-25 Verfahren zur herstellung von titanhaltigen siliciumdioxidkatalysatoren

Country Status (11)

Country Link
US (1) US6887823B2 (de)
EP (1) EP1364705B1 (de)
JP (1) JP4889865B2 (de)
KR (1) KR100827943B1 (de)
CN (1) CN1219596C (de)
AT (1) ATE328659T1 (de)
BR (1) BR0206810A (de)
CA (1) CA2436581A1 (de)
DE (1) DE60212082D1 (de)
ES (1) ES2266460T3 (de)
WO (1) WO2002060580A1 (de)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002239381A (ja) * 2001-02-22 2002-08-27 Sumitomo Chem Co Ltd チタン含有珪素酸化物触媒の製造方法及び触媒
US6884743B2 (en) 2002-09-16 2005-04-26 Basf Aktiengesellschaft Catalyst for epoxidation reactions
JP4265212B2 (ja) * 2002-12-19 2009-05-20 住友化学株式会社 チタン含有珪素酸化物触媒の製造方法
CN100430318C (zh) * 2004-09-24 2008-11-05 中国石油化工股份有限公司 含钛多孔材料的合成方法
EP1839750A4 (de) * 2004-12-06 2011-03-02 Sumitomo Chemical Co Verfahren zur herstellung eines titanhaltigen siliciumoxidkatalysators, katalysator und verfahren zur herstellung einer olefinoxidverbindung mit dem katalysator
CN101307039B (zh) * 2007-05-16 2010-12-01 中国石油化工股份有限公司 生产环氧化物的方法
CN101429176B (zh) * 2007-11-07 2011-05-18 中国石油化工股份有限公司 烯烃环氧化的方法
CN102295533B (zh) * 2010-06-24 2013-12-18 中国石油化工股份有限公司 α，α-二甲基苄醇的制备方法
DE102010046245A1 (de) * 2010-09-22 2012-03-22 Süd-Chemie AG Herstellung von Alumo-Phosphaten unter Rückgewinnung von Templaten
TWI426050B (zh) * 2011-04-19 2014-02-11 China Petrochemical Dev Corp Taipei Taiwan A method for preparing titanium-silicon molecular sieve and method for producing cyclohexanone oxime using the molecular sieve
CN102872847B (zh) * 2011-07-12 2014-11-26 中国石油化工股份有限公司 钛氧化硅材料的改性方法
US10011575B2 (en) 2016-07-25 2018-07-03 Oriental Union Chemical Corp. Method for fabricating titanium-containing silicon oxide material and application of the same
US10493430B2 (en) 2016-11-28 2019-12-03 Oriental Union Chemical Corp. Method for fabricating a titanium-containing silicon oxide material with high thermal stability and applications of the same
CN109721064B (zh) * 2017-10-31 2020-10-27 中国石油化工股份有限公司 钛硅分子筛的生产方法以及由该方法生产的钛硅分子筛和氨肟化反应方法
KR102672200B1 (ko) * 2018-03-15 2024-06-05 스미또모 가가꾸 가부시키가이샤 티탄 함유 규소 산화물 성형체의 제조 방법, 및 티탄 함유 규소 산화물 성형체

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4367342A (en) * 1969-04-02 1983-01-04 Shell Oil Company Olefin epoxidation
DE4138155A1 (de) * 1991-11-21 1993-05-27 Basf Ag Verfahren zur herstellung von im wesentlichen alkalifreien titansilikat-kristallen mit zeolithstruktur
US6106802A (en) * 1997-01-31 2000-08-22 Intevep, S.A. Stable synthetic material and method for preparing same
US6042807A (en) * 1997-04-02 2000-03-28 Arco Chemical Technology, L.P. Tellurium-containing molecular sieves
SG73663A1 (en) 1998-08-04 2000-06-20 Sumitomo Chemical Co A process for producing propylene oxide
SG82626A1 (en) * 1998-08-04 2001-08-21 Sumitomo Chemical Co Titanium-containing silicon oxide catalyst
ES2156506B1 (es) * 1998-10-14 2002-03-01 Sumitomo Chemical Co Metodo para la produccion de oxido de propileno.
JP2001031662A (ja) 1999-07-14 2001-02-06 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法
JP4399913B2 (ja) * 1999-08-25 2010-01-20 住友化学株式会社 オキシラン化合物の製造方法
DE19954322A1 (de) * 1999-11-10 2001-05-17 Basf Ag Oxid und Verfahren zu dessen Herstellung
BR0107953A (pt) * 2000-02-02 2002-10-22 Sumitomo Chemical Co Catalisador moldado, processo para produção de catalisador moldado e processo para produção de composto de oxirano

Also Published As

Publication number Publication date
DE60212082D1 (de) 2006-07-20
EP1364705A4 (de) 2004-11-10
JP2002224563A (ja) 2002-08-13
EP1364705B1 (de) 2006-06-07
ES2266460T3 (es) 2007-03-01
KR20030077603A (ko) 2003-10-01
US20040067846A1 (en) 2004-04-08
CN1500004A (zh) 2004-05-26
CN1219596C (zh) 2005-09-21
CA2436581A1 (en) 2002-08-08
US6887823B2 (en) 2005-05-03
BR0206810A (pt) 2004-02-03
JP4889865B2 (ja) 2012-03-07
WO2002060580A1 (en) 2002-08-08
EP1364705A1 (de) 2003-11-26
KR100827943B1 (ko) 2008-05-13

Similar Documents

Publication Publication Date Title
DE60212082D1 (de) Verfahren zur herstellung von titanhaltigen siliciumdioxidkatalysatoren
CA2423666C (en) Crystalline mww-type titanosilicate, its preparation and use thereof for producing epoxides
JP4897321B2 (ja) チタンシリカライトモレキュラーシーブおよびその製造方法
Álvaro et al. Synthesis of chiral periodic mesoporous silicas (ChiMO) of MCM-41 type with binaphthyl and cyclohexadiyl groups incorporated in the framework and direct measurement of their optical activity
Macquarrie et al. Organically modified hexagonal mesoporous silicas (HMS)—Remarkable effect of preparation solvent on physical and chemical properties
Narasimharao et al. Novel solid basic catalysts by nitridation of zeolite beta at low temperature
EP0066074B1 (de) Polymere tertiäre und sekundäre Organosiloxanamine, ihre Herstellung und Verwendung
DE60017286T2 (de) Mikroporöse materialien grosser oberfläche, welche in den oxidationsreaktionen tiq-6 und metiq-6 aktiv sind
JP2003525188A (ja) 中間孔または中間孔と微小孔を持つ無機酸化物およびその調製方法
CN113710649A (zh) 双(氟磺酰基)亚胺的纯化
ATE334744T1 (de) Geformter katalysator, verfahren zu dessen herstellung sowie verfahren zur herstellung einer oxirankomponente
RU2005127414A (ru) Способ получения этилового спирта
ATE273966T1 (de) Verfahren zur herstellung von olefinoxiden
DE60034303T2 (de) Verfahren zur Oxidation mit einem Katalysator von einer Antimontrifluorid und Siliziumdioxid enthaltenden Zusammensatzung
ATE518864T1 (de) Verfahren zur herstellung von carbapenemverbindungen
EP1261551B1 (de) Verfahren zur herstellung eines titanhaltigen zeolithen
CN119793517A (zh) 一种负载铼的纳米片状纯硅s-1沸石催化剂及其制备方法与应用
CN116332198B (zh) 钛硅分子筛及其制备方法和催化氧化环烷烃的方法
CN117645305A (zh) 一种级孔钛硅分子筛及其制备方法和环己酮氨肟化的方法
Macquarrie et al. New organically modified hexagonal mesoporous silicas: Preparation and applications in catalysis
US20040034258A1 (en) Crystalline MWW-type titanosilicate catalyst for producing oxidized compound, production process for the catalyst, and process for producing oxidized compound by using the catalyst
JP2006083103A (ja) 芳香族ポリアミンの製造方法
WO2005005441A3 (en) Process for preparing cyclic organohydrogensiloxanes
CN109772325A (zh) 一种Cu2+掺杂的空心结构微球芬顿催化剂及其制备方法和应用
JP2668496B2 (ja) ケイ素系粉末物質の新規な製造方法

Legal Events

Date Code Title Description
RER Ceased as to paragraph 5 lit. 3 law introducing patent treaties