ATE354560T1 - Verfahren zur aufreinigung von durch oxidieren eines gasförmigen substrats erhaltener (meth)acrylsäure - Google Patents

Verfahren zur aufreinigung von durch oxidieren eines gasförmigen substrats erhaltener (meth)acrylsäure

Info

Publication number: ATE354560T1
Authority: AT; Austria
Prior art keywords: acrylic acid; meth; column; solvent; absorption
Prior art date: 2003-11-04

Application number

AT04791448T

Other languages

English (en)

Inventor

Michel Fauconet

Denis Laurent

Original Assignee

Arkema France

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2003-11-04

Filing date

2004-10-01

Publication date

2007-03-15

2004-10-01 Application filed by Arkema France filed Critical Arkema France

2007-03-15 Application granted granted Critical

2007-03-15 Publication of ATE354560T1 publication Critical patent/ATE354560T1/de

Links

CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 title abstract 6
238000000034 method Methods 0.000 title abstract 2
230000001590 oxidative effect Effects 0.000 title 1
239000000758 substrate Substances 0.000 title 1
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 6
238000010521 absorption reaction Methods 0.000 abstract 5
239000002904 solvent Substances 0.000 abstract 5
239000000203 mixture Substances 0.000 abstract 3
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 abstract 2
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract 2
HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 abstract 2
VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 abstract 2
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 abstract 2
NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 abstract 2
238000010992 reflux Methods 0.000 abstract 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 abstract 1
150000001243 acetic acids Chemical class 0.000 abstract 1
150000001253 acrylic acids Chemical class 0.000 abstract 1
239000008246 gaseous mixture Substances 0.000 abstract 1
230000002209 hydrophobic effect Effects 0.000 abstract 1
239000012535 impurity Substances 0.000 abstract 1
239000003112 inhibitor Substances 0.000 abstract 1
239000001282 iso-butane Substances 0.000 abstract 1
230000003647 oxidation Effects 0.000 abstract 1
238000007254 oxidation reaction Methods 0.000 abstract 1
239000001294 propane Substances 0.000 abstract 1
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 1
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 abstract 1
238000000746 purification Methods 0.000 abstract 1
238000010517 secondary reaction Methods 0.000 abstract 1
238000000926 separation method Methods 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/64—Separation; Purification; Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Crystallography & Structural Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

AT04791448T 2003-11-04 2004-10-01 Verfahren zur aufreinigung von durch oxidieren eines gasförmigen substrats erhaltener (meth)acrylsäure ATE354560T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FR0312906A FR2861724B1 (fr)	2003-11-04	2003-11-04	Procede de purification de l'acide (meth)acrylique obtenu par oxydation d'un substrat gazeux

Publications (1)

Publication Number	Publication Date
ATE354560T1 true ATE354560T1 (de)	2007-03-15

Family

ID=34429866

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT04791448T ATE354560T1 (de)	2003-11-04	2004-10-01	Verfahren zur aufreinigung von durch oxidieren eines gasförmigen substrats erhaltener (meth)acrylsäure

Country Status (9)

Country	Link
US (1)	US7622607B2 (de)
EP (1)	EP1680389B1 (de)
JP (1)	JP2007510636A (de)
KR (1)	KR101052710B1 (de)
CN (1)	CN1902154B (de)
AT (1)	ATE354560T1 (de)
DE (1)	DE602004004924T2 (de)
FR (1)	FR2861724B1 (de)
WO (1)	WO2005054171A2 (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2957594B1 (fr) *	2010-03-18	2013-04-26	Arkema France	Procede de fabrication d'acide acrylique bio-ressource de grade polymere a partir de glycerol
DE102012207811A1 (de)	2012-05-10	2012-07-12	Basf Se	Verfahren der heterogen katalysierten Gasphasenpartialoxidation von (Meth)acrolein zu (Meth)acrylsäure
CN102775295B (zh) *	2012-08-10	2015-07-01	上海华谊丙烯酸有限公司	一种提纯丙烯酸的方法
US9505671B2 (en) *	2012-10-31	2016-11-29	Washington State University	Renewable para-xylene from acetic acid
WO2015012876A1 (en) *	2013-07-22	2015-01-29	Washington State University	Improved use of byproduct acetic acid from oxidative methods of making acrylic acid and/or methacrylic acid
JP2016520096A (ja)	2013-05-20	2016-07-11	サウディベーシックインダストリーズコーポレイション	酢酸及びアクリル酸の精製方法
FR3012143B1 (fr) *	2013-10-18	2016-08-26	Arkema France	Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone
CN104016821A (zh) *	2014-06-10	2014-09-03	中国科学院过程工程研究所	一种（甲基）丙烯醛、（甲基）丙烯酸及其酯的阻聚剂及阻聚方法
DE102014215437A1 (de) *	2014-08-05	2015-11-05	Basf Se	Kolonne zur thermischen Behandlung eines Fluids
US10093551B2 (en) *	2014-09-23	2018-10-09	Basf Se	Process and plant for treatment of secondary components obtained in acrolein and/or (meth)acrylic acid production
FR3049601B1 (fr) *	2016-03-29	2018-03-09	Arkema France	Procede ameliore de production d'acide (meth)acrylique
KR102079774B1 (ko)	2016-11-25	2020-02-20	주식회사 엘지화학	(메트)아크릴산의 연속 회수 방법 및 장치
KR102079775B1 (ko) *	2016-11-25	2020-02-20	주식회사 엘지화학	(메트)아크릴산의 연속 회수 방법 및 장치

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE786398A (fr)	1971-07-21	1973-01-18	Basf Ag	Procede de preparation de l'acide acrylique anhydre
DE2241714A1 (de) *	1972-08-24	1974-03-28	Basf Ag	Verfahren zur abtrennung von acrylsaeure aus den reaktionsgasen der propylenoder acroleinoxydation
DE4308087C2 (de)	1993-03-13	1997-02-06	Basf Ag	Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein
DE4436243A1 (de)	1994-10-11	1996-04-18	Basf Ag	Verfahren zur Abtrennung von (Meth)acrylsäure aus dem Reaktionsgasgemisch der katalytischen Gasphasenoxidation C¶3¶-/C¶4¶-Verbindungen
DE19600955A1 (de) *	1996-01-12	1997-07-17	Basf Ag	Verfahren zur Herstellung von Acrylsäure und deren Ester
FR2756280B1 (fr) *	1996-11-25	1998-12-24	Atochem Elf Sa	Purification de l'acide acrylique obtenu par oxydation catalytique du propylene
JPH1112222A (ja) *	1997-06-25	1999-01-19	Nippon Shokubai Co Ltd	アクリル酸の回収方法
EP1035103B1 (de) *	1999-03-05	2003-10-15	Rohm And Haas Company	Verfahren zur Herstellung von Acrylsäure
FR2798382B1 (fr) *	1999-09-14	2001-10-26	Atofina	Procede de purification de l'acide acrylique obtenu par oxydation du propylene et/ou de l'acroleine
US6888025B2 (en)	2000-02-14	2005-05-03	Nippon Shokubai, Co. Ltd.	Method for absorbing acrylic acid and method for purifying acrylic acid
JP2001226320A (ja) *	2000-02-14	2001-08-21	Nippon Shokubai Co Ltd	アクリル酸の捕集方法およびアクリル酸の精製方法
JP2001247510A (ja) *	2000-03-08	2001-09-11	Nippon Shokubai Co Ltd	アクリル酸の製造方法
DE10115277A1 (de) *	2001-03-28	2002-06-13	Basf Ag	Verfahren zur kontinuierlichen Gewinnung von(Meth)acrylsäure
JP4016650B2 (ja) *	2001-12-14	2007-12-05	三菱化学株式会社	（メタ）アクリル酸の製造方法

2003
- 2003-11-04 FR FR0312906A patent/FR2861724B1/fr not_active Expired - Fee Related
2004
- 2004-10-01 CN CN200480039855XA patent/CN1902154B/zh not_active Expired - Fee Related
- 2004-10-01 JP JP2006537336A patent/JP2007510636A/ja active Pending
- 2004-10-01 AT AT04791448T patent/ATE354560T1/de not_active IP Right Cessation
- 2004-10-01 DE DE602004004924T patent/DE602004004924T2/de not_active Expired - Lifetime
- 2004-10-01 US US10/577,168 patent/US7622607B2/en not_active Expired - Fee Related
- 2004-10-01 KR KR1020067010962A patent/KR101052710B1/ko not_active Expired - Fee Related
- 2004-10-01 EP EP04791448A patent/EP1680389B1/de not_active Expired - Lifetime
- 2004-10-01 WO PCT/FR2004/002481 patent/WO2005054171A2/fr not_active Ceased

Also Published As

Publication number	Publication date
WO2005054171A3 (fr)	2005-08-11
CN1902154A (zh)	2007-01-24
KR101052710B1 (ko)	2011-08-01
JP2007510636A (ja)	2007-04-26
KR20060121134A (ko)	2006-11-28
US20080281124A1 (en)	2008-11-13
WO2005054171A2 (fr)	2005-06-16
EP1680389B1 (de)	2007-02-21
DE602004004924D1 (de)	2007-04-05
CN1902154B (zh)	2010-05-05
US7622607B2 (en)	2009-11-24
EP1680389A2 (de)	2006-07-19
FR2861724A1 (fr)	2005-05-06
FR2861724B1 (fr)	2005-12-30
DE602004004924T2 (de)	2007-11-15

Legal Events

Date	Code	Title	Description
2007-08-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties

Publication	Publication Date	Title
ATE354560T1 (de)	2007-03-15	Verfahren zur aufreinigung von durch oxidieren eines gasförmigen substrats erhaltener (meth)acrylsäure
ATE356794T1 (de)	2007-04-15	Verfahren zur herstellung von (meth)acrylsaeureestern
ATE522492T1 (de)	2011-09-15	Verfahren zur herstellung von (meth)acrylaten von c10-alkoholgemischen
DE50214752D1 (de)	2010-12-16	Verfahren zur herstellung wasserabsorbierender harze
ATE469116T1 (de)	2010-06-15	Verfahren zur kontinuierlichen herstellung von ungesättigten carbonsäureanhydriden
DE50304605D1 (de)	2006-09-21	Verfahren zur herstellung von acrylsäure
ATE346835T1 (de)	2006-12-15	Verfahren zur herstellung von acrolein und/oder acrylsäure
JP7105799B2 (ja)	2022-07-25	分離壁を備えた蒸留カラムを含む（メタ）アクリル酸の精製方法
DE60333529D1 (de)	2010-09-09	Verfahren zur Entsäurung von Erdgas
KR101535496B1 (ko)	2015-07-09	(메트)아크릴산의 연속 회수 방법 및 회수 장치
ATE459609T1 (de)	2010-03-15	Verfahren zur aufreinigung von propylenoxid
KR960022433A (ko)	1996-07-18	주성분으로서 (메타) 아크릴산 및 (메타) 아크릴산 보다 높은 비점을 가지는 비활성 소수성 유기 액체를 포함하며, 부성분으로서 저급 알데히드를 포함하는 혼합물로부터 (메타) 아크릴산을 정류하는 방법
ATE319697T1 (de)	2006-03-15	Verfahren zur kontinuierlichen reindestillation des bei der propylenoxidsynthese verwendeten lösungsmittels methanol
CA2282492A1 (en)	1998-09-17	Method for extracting (meth)acrylic acid
KR102291247B1 (ko)	2021-08-20	메타크롤레인을 분리하는 방법
ATE223885T1 (de)	2002-09-15	Verfahren zur reinigung von einem acrolein enthaltenden gasstromes
ATE405540T1 (de)	2008-09-15	Verfahren zur destillativen trennung von wässrigen aminlösungen
US7015357B2 (en)	2006-03-21	Processes for producing (meth)acrylic acid
KR900017987A (ko)	1990-12-20	아크릴산 에스테르의 제조방법
ATE468315T1 (de)	2010-06-15	Verfahren zur herstellung von (meth)acrylsäure
DE60012546D1 (de)	2004-09-02	Verfahren zur reinigung von durch oxidation von propylen und/oder acrolein hergestellten acrylsäure
CN110099889B (zh)	2023-04-04	经由分隔壁塔的丙烯酸提纯
ATE365153T1 (de)	2007-07-15	Verfahren zur abtrennung von triethanolamin aus einem durch die umsetzung von ammoniak mit ethylenoxid erhaltenen stoffgemisch
ATE158268T1 (de)	1997-10-15	Verfahren zur spaltung von tertiärbutylalkohol in einer reaktionsdestillationskolonne
DE502005004980D1 (de)	2008-09-18	Verfahren zur herstellung von spezifikationsgerechtem phthalsäureanhydrid