ATE392412T1 - Verfahren zur herstellung von 4,4'-diphenylmethan diisocyanat - Google Patents

Verfahren zur herstellung von 4,4'-diphenylmethan diisocyanat

Info

Publication number: ATE392412T1
Authority: AT; Austria
Prior art keywords: diphenylmethane diisocyanate; polyisocyanates; mixture; diisocyanates; give
Prior art date: 2005-06-10

Application number

AT06011048T

Other languages

English (en)

Inventor

Berthold Keggenhoff

Ralf Echterhoff

Ricardo Serra

Original Assignee

Bayer Materialscience Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2005-06-10

Filing date

2006-05-30

Publication date

2008-05-15

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=36972692&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ATE392412(T1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

2006-05-30 Application filed by Bayer Materialscience Ag filed Critical Bayer Materialscience Ag

2008-05-15 Application granted granted Critical

2008-05-15 Publication of ATE392412T1 publication Critical patent/ATE392412T1/de

Links

UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 title abstract 5
238000004519 manufacturing process Methods 0.000 title abstract 3
229920001228 polyisocyanate Polymers 0.000 abstract 6
239000005056 polyisocyanate Substances 0.000 abstract 6
125000005442 diisocyanate group Chemical group 0.000 abstract 5
239000000203 mixture Substances 0.000 abstract 5
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 2
150000004985 diamines Chemical class 0.000 abstract 2
CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical class C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 abstract 2
238000004821 distillation Methods 0.000 abstract 2
229920000768 polyamine Polymers 0.000 abstract 2
LFSYUSUFCBOHGU-UHFFFAOYSA-N 1-isocyanato-2-[(4-isocyanatophenyl)methyl]benzene Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=CC=C1N=C=O LFSYUSUFCBOHGU-UHFFFAOYSA-N 0.000 abstract 1
YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 1
239000003377 acid catalyst Substances 0.000 abstract 1
238000002425 crystallisation Methods 0.000 abstract 1
230000008025 crystallization Effects 0.000 abstract 1
239000012948 isocyanate Substances 0.000 abstract 1
150000002513 isocyanates Chemical class 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/12—Derivatives of isocyanic acid having isocyanate groups bound to carbon atoms of six-membered aromatic rings
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/14—Derivatives of isocyanic acid containing at least two isocyanate groups bound to the same carbon skeleton

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Polyurethanes Or Polyureas (AREA)

AT06011048T 2005-06-10 2006-05-30 Verfahren zur herstellung von 4,4'-diphenylmethan diisocyanat ATE392412T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE102005026864A DE102005026864A1 (de)	2005-06-10	2005-06-10	Verfahren zur Herstellung von 4,4'-Diphenylmethandiisocyanat

Publications (1)

Publication Number	Publication Date
ATE392412T1 true ATE392412T1 (de)	2008-05-15

Family

ID=36972692

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT06011048T ATE392412T1 (de)	2005-06-10	2006-05-30	Verfahren zur herstellung von 4,4'-diphenylmethan diisocyanat

Country Status (12)

Country	Link
US (1)	US20080275269A1 (de)
EP (1)	EP1734035B1 (de)
JP (1)	JP2006348030A (de)
KR (1)	KR20060128732A (de)
CN (1)	CN1876625A (de)
AT (1)	ATE392412T1 (de)
BR (1)	BRPI0602173A (de)
DE (2)	DE102005026864A1 (de)
ES (1)	ES2304037T3 (de)
PT (1)	PT1734035E (de)
SG (1)	SG128579A1 (de)
TW (1)	TW200710071A (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US20060136816A1 (en) *	2004-12-20	2006-06-22	Microsoft Corporation	File formats, methods, and computer program products for representing documents
DE102006004041A1 (de) *	2006-01-28	2007-08-02	Bayer Materialscience Ag	Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe
DE102008012037A1 (de) *	2008-03-01	2009-09-03	Bayer Materialscience Ag	Verfahren zur Herstellung von Methylen-diphenyl-diisocyanaten
WO2010040675A2 (en) *	2008-10-06	2010-04-15	Huntsman International Llc	Process for the simultaneous production of different mixtures of diisocyanate isomers of the diphenylmethane series
EP2184144A1 (de) *	2008-11-06	2010-05-12	Huntsman International Llc	Polyisocyanatzusammensetzung zum Binden von lignozellulosehaltigen Materialien
WO2013081873A1 (en) *	2011-11-30	2013-06-06	Dow Global Technologies Llc	Process for the production of methylene diphenyl diisocyanate isomer mixtures with high 2,4'- methylene diphenyl diisocyanate purity
EP3362588A1 (de)	2015-10-15	2018-08-22	Covestro Deutschland AG	Verfahren zur herstellung aminofunktioneller aromaten
CN106977408A (zh) *	2017-04-19	2017-07-25	杨桂廷	副品红隐色基的制备方法
EP3498689A1 (de)	2017-12-14	2019-06-19	Sulzer Chemtech AG	Anlage und verfahren zur reinigung eines isomeren monomers wie z. b. 4,4 '-methylendiphenyldiisocyanat aus einem rohgemisch
KR102134009B1 (ko) *	2019-08-26	2020-07-15	주식회사 에이피텍	피착이 우수한 폴리우레아 수지 조성물
CN110511163B (zh) *	2019-09-02	2021-09-07	万华化学集团股份有限公司	光化反应制备多异氰酸酯的方法以及制备水性聚氨酯树脂的方法
CN113321599A (zh) *	2021-06-30	2021-08-31	甘肃银光聚银化工有限公司	一种制备高纯度间苯二亚甲基二异氰酸酯的方法
CN115806508B (zh) *	2022-12-20	2024-10-18	万华化学（宁波）有限公司	低2,2’-mdi含量的二苯基甲烷二异氰酸酯及其制备方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE755243Q (fr) *	1965-07-08	1971-02-01	Upjohn Co	Procedes de fabrication d'isocyanates et de polyisocyanates
GB1229181A (de)	1968-08-01	1971-04-21
US3897314A (en) *	1970-07-18	1975-07-29	Bayer Ag	Process for removing distillation residue from crude isocyanates
US4118410A (en) *	1971-02-04	1978-10-03	Gottfried Reuter Gmbh I.L.	Polyphenyl-polymethylene-polyisocyanate mixtures
CA1004234A (en) *	1972-08-04	1977-01-25	Bayer Aktiengesellschaft	Process for the production of polyamines
US3892634A (en) *	1973-02-20	1975-07-01	Upjohn Co	Separation of 2,4{40 {0 and 4,4{40 {0 methylene bis(phenyl isocyanate) from polymethylene polyphenyl polyisocyanates
US4189354A (en) *	1976-07-10	1980-02-19	Bayer Aktiengesellschaft	Process for the production of diisocyanatodiphenyl methane isomers with an adjusted content of chlorine compounds
DE2631168B2 (de)	1976-07-10	1979-03-08	Bayer Ag, 5090 Leverkusen	Verfahren zur Herstellung von Diisocyanatodiphenylmethan-Isomeren mit einem eingestellten Gehalt an Chlorverbindungen
DE3145010A1 (de)	1981-11-12	1983-05-19	Bayer Ag, 5090 Leverkusen	Verfahren zur herstellung von 4,4'-diisocyanatodiphenylmethan
DE3329124A1 (de) *	1983-08-11	1985-02-28	Bayer Ag, 5090 Leverkusen	Verfahren zur reinigung von polyisocyanaten und die so gereinigten polyisocyanate
JP2875877B2 (ja) *	1990-10-23	1999-03-31	三井化学株式会社	メチレン架橋ポリフェニレンポリイソシアネートの製造方法
US5258417A (en) *	1992-12-28	1993-11-02	Basf Corporation	Low viscosity polymeric MDI
DE19817691A1 (de) *	1998-04-21	1999-10-28	Basf Ag	Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl
DE10111337A1 (de) *	2001-03-08	2002-09-12	Basf Ag	Verfahren zur Herstellung von MDI, insbesondere von 2.4'-MDI
DE10260092A1 (de) *	2002-12-19	2004-07-01	Basf Ag	Verfahren zur Reinigung von Isocyanaten
EP1475367B1 (de)	2003-05-08	2010-07-07	Bayer MaterialScience AG	Verfahren zur Destillation eines Gemisches isomerer Diisocyanatodiphenylmethane
DE10333929A1 (de) *	2003-07-25	2005-02-24	Bayer Materialscience Ag	Herstellung von Mischungen von Di- und Polyisocyanaten der Diphenylmethanreihe mit hohen Gehalten an 4,4'-Methylendiphenyldiisocyanat und 2,4'-Methylendiphenyldiisocyanat

2005
- 2005-06-10 DE DE102005026864A patent/DE102005026864A1/de not_active Withdrawn
2006
- 2006-05-30 DE DE602006000927T patent/DE602006000927T2/de active Active
- 2006-05-30 AT AT06011048T patent/ATE392412T1/de not_active IP Right Cessation
- 2006-05-30 PT PT06011048T patent/PT1734035E/pt unknown
- 2006-05-30 EP EP06011048A patent/EP1734035B1/de not_active Revoked
- 2006-05-30 ES ES06011048T patent/ES2304037T3/es active Active
- 2006-06-06 SG SG200603840A patent/SG128579A1/en unknown
- 2006-06-07 US US11/448,444 patent/US20080275269A1/en not_active Abandoned
- 2006-06-08 BR BRPI0602173-5A patent/BRPI0602173A/pt not_active Application Discontinuation
- 2006-06-08 CN CNA2006100915805A patent/CN1876625A/zh active Pending
- 2006-06-09 KR KR1020060051883A patent/KR20060128732A/ko not_active Ceased
- 2006-06-09 TW TW095120481A patent/TW200710071A/zh unknown
- 2006-06-09 JP JP2006161455A patent/JP2006348030A/ja not_active Withdrawn

Also Published As

Publication number	Publication date
EP1734035A1 (de)	2006-12-20
KR20060128732A (ko)	2006-12-14
EP1734035B1 (de)	2008-04-16
DE602006000927T2 (de)	2009-07-09
CN1876625A (zh)	2006-12-13
TW200710071A (en)	2007-03-16
SG128579A1 (en)	2007-01-30
JP2006348030A (ja)	2006-12-28
DE602006000927D1 (de)	2008-05-29
BRPI0602173A (pt)	2007-05-02
PT1734035E (pt)	2008-06-27
US20080275269A1 (en)	2008-11-06
ES2304037T3 (es)	2008-09-01
DE102005026864A1 (de)	2006-12-14

Legal Events

Date	Code	Title
2008-10-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties
2012-02-15	RZN	Patent revoked
2012-04-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties

Publication	Publication Date	Title
DE602006000927D1 (de)	2008-05-29	Verfahren zur Herstellung von 4,4'-Diphenylmethan Diisocyanat
ATE506341T1 (de)	2011-05-15	Verfahren zur herstellung von di- und polyaminen der diphenylmethanreihe
WO2010149544A3 (en)	2011-03-17	Process for the production of isocyanates, preferably diisocyanates and polyisocyanates with solvent recirculation
ATE478907T1 (de)	2010-09-15	Verfahren zur herstellung von polyurethanen
RU2007117488A (ru)	2008-11-20	Способ получения изоцианатов
DE50313194D1 (de)	2010-11-25	Verfahren zur kontinuierlichen herstellung von isocyanaten
TW200617050A (en)	2006-06-01	Improved process for the production of carbodiimide modified organic isocyanates
ATE482190T1 (de)	2010-10-15	Verfahren zur herstellung von toluylendiisocyanat
SG132626A1 (en)	2007-06-28	A process for the production of 4,4æ-diphenylmethane diisocyanate
TW200617049A (en)	2006-06-01	A process for preparing polyisocyanates by the adiabatic phosgenation of primary amines
ATE446947T1 (de)	2009-11-15	Verfahren zur herstellung von isocyanaten
CA2475662A1 (en)	2005-01-25	Production of mixtures of diisocyanates and polyisocyanates from the diphenylmethane series with high contents of 4,4'-methylenediphenyl diisocyanate and 2,4'-methylenediphenyl diisocyanate
ATE345323T1 (de)	2006-12-15	Verfahren zur herstellung von polyisocyanaten der diphenylmethanreihe durch phosgenierung von nicht-neutralisiertem polyamin der diphenylmethanreihe
WO2011006807A3 (en)	2011-12-22	Process for preparing light-coloured isocyanates of the diphenylmethane series
WO2006130405A3 (en)	2007-02-15	Process for the preparation of polyisocyanates of the diphenylmethane series
RU2007117490A (ru)	2008-11-20	Способ совместного получения изоцианатов и хлора
ATE522494T1 (de)	2011-09-15	Verfahren zur herstellung von mischungen von diphenylmethandiisocyanaten und polyphenylpolymethylenpolyisocyanaten
DE50208205D1 (de)	2006-11-02	Verfahren zur herstellung von mdi, insbesondere von 2,4'-mdi
PT2062876E (pt)	2011-09-22	Método para a produção de diisocianatos aromáticos em fase gasosa
JP2012532918A (ja)	2012-12-20	ジフェニルメタンジイソシアネート類の明色イソシアネートの製造方法
ATE393761T1 (de)	2008-05-15	Verfahren zur herstellung von isocyanaten
DE502006006826D1 (de)	2010-06-10	Verfahren zur Herstellung von Di-und Polyaminen der Diphenylmethanreihe
CA2174194A1 (en)	1996-12-07	Urethane-free, diphenylmethane diisocyanate prepolymers and process for their production and use
ATE452874T1 (de)	2010-01-15	Verfahren zur herstellung von isocyanaten
PT2502904E (pt)	2013-12-04	Processo para a produção de poliisocianatos