ATE432766T1 - Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid - Google Patents

Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid

Info

Publication number
ATE432766T1
ATE432766T1 AT06841526T AT06841526T ATE432766T1 AT E432766 T1 ATE432766 T1 AT E432766T1 AT 06841526 T AT06841526 T AT 06841526T AT 06841526 T AT06841526 T AT 06841526T AT E432766 T1 ATE432766 T1 AT E432766T1
Authority
AT
Austria
Prior art keywords
conditions
purification
concentration
reacting
ethylene oxide
Prior art date
Application number
AT06841526T
Other languages
English (en)
Inventor
Dominicus Maria Rekers
Mathias Jozef Paul Slapak
Original Assignee
Shell Int Research
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Int Research filed Critical Shell Int Research
Application granted granted Critical
Publication of ATE432766T1 publication Critical patent/ATE432766T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B81—MICROSTRUCTURAL TECHNOLOGY
    • B81B—MICROSTRUCTURAL DEVICES OR SYSTEMS, e.g. MICROMECHANICAL DEVICES
    • B81B7/00—Microstructural systems ; Auxiliary parts of microstructural devices or systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00822—Metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00831—Glass
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00833—Plastic
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00867—Microreactors placed in series, on the same or on different supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00869—Microreactors placed in parallel, on the same or on different supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00871—Modular assembly
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00905—Separation
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23C—METHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN  A CARRIER GAS OR AIR 
    • F23C2900/00—Special features of, or arrangements for combustion apparatus using fluid fuels or solid fuels suspended in air; Combustion processes therefor
    • F23C2900/03001—Miniaturized combustion devices using fluid fuels

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Epoxy Compounds (AREA)
  • Incineration Of Waste (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Treatments Of Macromolecular Shaped Articles (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
AT06841526T 2005-12-22 2006-12-20 Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid ATE432766T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP05257995 2005-12-22
PCT/EP2006/070030 WO2007071739A1 (en) 2005-12-22 2006-12-20 Microchannel apparatus for unit operations following ethylene oxide production

Publications (1)

Publication Number Publication Date
ATE432766T1 true ATE432766T1 (de) 2009-06-15

Family

ID=37898787

Family Applications (1)

Application Number Title Priority Date Filing Date
AT06841526T ATE432766T1 (de) 2005-12-22 2006-12-20 Verfahren und vorrichtung zur konzentration und reinigung von ethylenoxid

Country Status (10)

Country Link
EP (4) EP1981632A1 (de)
JP (4) JP2009520943A (de)
KR (4) KR20080080183A (de)
CN (4) CN101384349A (de)
AT (1) ATE432766T1 (de)
CA (4) CA2634366A1 (de)
DE (1) DE602006007180D1 (de)
EA (2) EA200870100A1 (de)
TW (4) TW200740519A (de)
WO (4) WO2007071737A1 (de)

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US7294734B2 (en) 2003-05-02 2007-11-13 Velocys, Inc. Process for converting a hydrocarbon to an oxygenate or a nitrile
CN101023068B (zh) 2004-08-12 2013-02-13 万罗赛斯公司 使用微通道工艺技术将乙烯转化成环氧乙烷的方法
US7459589B2 (en) 2005-12-22 2008-12-02 Shell Oil Company Process for the preparation of an alkylene glycol
US7750170B2 (en) 2005-12-22 2010-07-06 Shell Oil Company Process for mixing an oxidant having explosive potential with a hydrocarbon
AU2009233786B2 (en) 2008-04-09 2014-04-24 Velocys Inc. Process for converting a carbonaceous material to methane, methanol and/or dimethyl ether using microchannel process technology
US8100996B2 (en) 2008-04-09 2012-01-24 Velocys, Inc. Process for upgrading a carbonaceous material using microchannel process technology
EP2313385A2 (de) * 2008-07-14 2011-04-27 Velocys Inc. Verfahren zur herstellung von ethylenoxid unter anwendung einer mikrokanalverfahrenstechnologie
EP2300447A1 (de) 2008-07-14 2011-03-30 Basf Se Verfahren zur herstellung von ethylenoxid
US8747656B2 (en) 2008-10-10 2014-06-10 Velocys, Inc. Process and apparatus employing microchannel process technology
EP2223741A1 (de) 2009-02-13 2010-09-01 Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO Mikrofluidisches System mit einem Stapel von Verfahrensmodulen und Wärmetauschermodule
US8524927B2 (en) 2009-07-13 2013-09-03 Velocys, Inc. Process for making ethylene oxide using microchannel process technology
EP2493812B1 (de) * 2009-08-10 2018-02-14 Standardgraphene Co., Ltd. Verfahren zur herstellung von graphenbasiertem material in nanogrösse und ausrüstung zu seiner herstellung
TWI493141B (zh) * 2010-03-29 2015-07-21 Guan Bang Chen 微管路之觸媒燃燒器
US9676623B2 (en) 2013-03-14 2017-06-13 Velocys, Inc. Process and apparatus for conducting simultaneous endothermic and exothermic reactions
CN103386334A (zh) * 2013-08-07 2013-11-13 苏州扬清芯片科技有限公司 一种微流控芯片的制冷方法
DE102015111614A1 (de) * 2015-07-17 2017-01-19 Karlsruher Institut für Technologie Mikrostrukturreaktor zur Durchführung exothermer, heterogen katalysierter Reaktionen mit effizienter Verdampfungskühlung
CN106316783A (zh) * 2016-08-23 2017-01-11 张英 一种1，2‑己二醇的气液管道式制备方法
JP6838983B2 (ja) * 2017-02-03 2021-03-03 株式会社ガスター 放熱ユニット 暖房システム
JP6732672B2 (ja) * 2017-02-03 2020-07-29 株式会社ガスター 浴湯熱暖房システム
EP3770145A1 (de) 2019-07-24 2021-01-27 Basf Se Verfahren zur kontinuierlichen herstellung von acrolein oder acrylsäure als zielprodukt aus propen
KR20240165086A (ko) * 2023-05-15 2024-11-22 주식회사 에코마스터 마이크로채널 반응기 및 이를 이용한 수소제조 반응기
CN116943597B (zh) * 2023-08-31 2025-11-25 天津凯莱英医药科技发展有限公司 反应器

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US4760200A (en) * 1985-12-31 1988-07-26 Union Carbide Corporation Process for the production of alkylene glycols
US5811062A (en) * 1994-07-29 1998-09-22 Battelle Memorial Institute Microcomponent chemical process sheet architecture
US6126723A (en) * 1994-07-29 2000-10-03 Battelle Memorial Institute Microcomponent assembly for efficient contacting of fluid
US5914091A (en) * 1996-02-15 1999-06-22 Atmi Ecosys Corp. Point-of-use catalytic oxidation apparatus and method for treatment of voc-containing gas streams
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Also Published As

Publication number Publication date
EA200870101A1 (ru) 2008-12-30
WO2007071739A1 (en) 2007-06-28
DE602006007180D1 (de) 2009-07-16
KR20080080184A (ko) 2008-09-02
KR20080080183A (ko) 2008-09-02
TW200803973A (en) 2008-01-16
KR20080080182A (ko) 2008-09-02
TW200740518A (en) 2007-11-01
CA2634366A1 (en) 2007-06-28
CN101384349A (zh) 2009-03-11
JP2009520764A (ja) 2009-05-28
JP2009520762A (ja) 2009-05-28
CN101384350A (zh) 2009-03-11
EA200870100A1 (ru) 2008-12-30
WO2007071744A1 (en) 2007-06-28
CA2634440A1 (en) 2007-06-28
EP1976625A1 (de) 2008-10-08
EP1973645A1 (de) 2008-10-01
CN101384352A (zh) 2009-03-11
CN101384351A (zh) 2009-03-11
JP2009520767A (ja) 2009-05-28
JP2009520943A (ja) 2009-05-28
TW200735958A (en) 2007-10-01
EP1981632A1 (de) 2008-10-22
EP1979087A1 (de) 2008-10-15
KR20080080372A (ko) 2008-09-03
TW200740519A (en) 2007-11-01
CA2634409A1 (en) 2007-06-28
CA2634417A1 (en) 2007-06-28
WO2007071737A1 (en) 2007-06-28
EP1976625B1 (de) 2009-06-03
WO2007071741A1 (en) 2007-06-28

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