ATE454215T1 - Verfahren zur herstellung metallischen geträgerten katalysatoren beinhaltend einen behandlungschritt mit wässriger lösung aus brom und bromionen - Google Patents

Verfahren zur herstellung metallischen geträgerten katalysatoren beinhaltend einen behandlungschritt mit wässriger lösung aus brom und bromionen

Info

Publication number
ATE454215T1
ATE454215T1 AT00940448T AT00940448T ATE454215T1 AT E454215 T1 ATE454215 T1 AT E454215T1 AT 00940448 T AT00940448 T AT 00940448T AT 00940448 T AT00940448 T AT 00940448T AT E454215 T1 ATE454215 T1 AT E454215T1
Authority
AT
Austria
Prior art keywords
bromine
catalyst
metal
aqueous solution
treatment step
Prior art date
Application number
AT00940448T
Other languages
English (en)
Inventor
Michel Devic
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from FR9909260A external-priority patent/FR2796311B1/fr
Application filed by Arkema France filed Critical Arkema France
Application granted granted Critical
Publication of ATE454215T1 publication Critical patent/ATE454215T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06—Halogens; Compounds thereof
    • B01J27/128—Halogens; Compounds thereof with iron group metals or platinum group metals
    • B01J27/13—Platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/22—Halogenating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/006—Separating solid material from the gas/liquid stream by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/222—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid in the presence of a rotating device only
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
    • B01J8/228—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement externally, i.e. the particles leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/029—Preparation from hydrogen and oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00176—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles outside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
AT00940448T 1999-07-16 2000-06-07 Verfahren zur herstellung metallischen geträgerten katalysatoren beinhaltend einen behandlungschritt mit wässriger lösung aus brom und bromionen ATE454215T1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR9909260A FR2796311B1 (fr) 1999-07-16 1999-07-16 Reacteur multietage, ses applications et procede de fabrication du peroxyde d'hydrogene
FR9910310A FR2796312B1 (fr) 1999-07-16 1999-08-09 Catalyseur metallique supporte, sa preparation et ses applications dans la fabrication directe du peroxyde d'hydrogene
PCT/FR2000/001552 WO2001005501A1 (fr) 1999-07-16 2000-06-07 Catalyseur metallique supporte, sa preparation et ses applications dans la fabrication directe du peroxyde d'hydrogene

Publications (1)

Publication Number Publication Date
ATE454215T1 true ATE454215T1 (de) 2010-01-15

Family

ID=26235041

Family Applications (1)

Application Number Title Priority Date Filing Date
AT00940448T ATE454215T1 (de) 1999-07-16 2000-06-07 Verfahren zur herstellung metallischen geträgerten katalysatoren beinhaltend einen behandlungschritt mit wässriger lösung aus brom und bromionen

Country Status (17)

Country Link
US (1) US6958138B1 (de)
EP (1) EP1204477B1 (de)
JP (1) JP4251809B2 (de)
KR (1) KR100554927B1 (de)
CN (1) CN1210105C (de)
AT (1) ATE454215T1 (de)
AU (1) AU764178B2 (de)
BR (1) BR0012222B1 (de)
CA (1) CA2378919C (de)
DE (1) DE60043657D1 (de)
EA (1) EA004475B1 (de)
FR (1) FR2796312B1 (de)
NO (1) NO323596B1 (de)
NZ (1) NZ516005A (de)
PL (1) PL353747A1 (de)
TR (1) TR200200073T2 (de)
WO (1) WO2001005501A1 (de)

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EP1346767A1 (de) * 2002-03-15 2003-09-24 Council of Scientific and Industrial Research Multifunktioneller Katalysator, verwendbar in der Synthese chiraler, vicinaler Diole, und Verfahren zu seiner Herstellung
ATE453603T1 (de) 2003-02-03 2010-01-15 Repsol Quimica Sa Integriertes verfahren zur selektiven oxydation von organischen verbindungen
US7067103B2 (en) 2003-03-28 2006-06-27 Headwaters Nanokinetix, Inc. Direct hydrogen peroxide production using staged hydrogen addition
US7011807B2 (en) 2003-07-14 2006-03-14 Headwaters Nanokinetix, Inc. Supported catalysts having a controlled coordination structure and methods for preparing such catalysts
US7045479B2 (en) 2003-07-14 2006-05-16 Headwaters Nanokinetix, Inc. Intermediate precursor compositions used to make supported catalysts having a controlled coordination structure and methods for preparing such compositions
US7569508B2 (en) 2004-11-17 2009-08-04 Headwaters Technology Innovation, Llc Reforming nanocatalysts and method of making and using such catalysts
US7144565B2 (en) 2003-07-29 2006-12-05 Headwaters Nanokinetix, Inc. Process for direct catalytic hydrogen peroxide production
US7632775B2 (en) 2004-11-17 2009-12-15 Headwaters Technology Innovation, Llc Multicomponent nanoparticles formed using a dispersing agent
JP4655755B2 (ja) * 2005-05-18 2011-03-23 住友化学株式会社 過酸化水素の製造方法
GB0514075D0 (en) 2005-07-11 2005-08-17 Cardiff University Improvements in catalysts
US7396795B2 (en) 2005-08-31 2008-07-08 Headwaters Technology Innovation, Llc Low temperature preparation of supported nanoparticle catalysts having increased dispersion
US7541309B2 (en) 2006-05-16 2009-06-02 Headwaters Technology Innovation, Llc Reforming nanocatalysts and methods of making and using such catalysts
US7563742B2 (en) 2006-09-22 2009-07-21 Headwaters Technology Innovation, Llc Supported nickel catalysts having high nickel loading and high metal dispersion and methods of making same
EP2188049B1 (de) * 2007-08-30 2020-11-25 Solvay Sa Herstellungsverfahren eines katalysators und desser verwendung zur wasserstoffperoxidherstellung durch hydrierung von alkylanthrachinonen
CN101402039B (zh) * 2008-11-13 2010-12-08 北京化工大学 一种负载型金属钯催化剂的制备方法
KR101474571B1 (ko) 2009-05-13 2014-12-19 에스케이이노베이션 주식회사 고분자 전해질 다층박막 촉매 및 그 제조 방법
WO2012171892A1 (en) 2011-06-17 2012-12-20 Solvay Sa Process for the manufacture of hydrogen peroxide
CN103717304A (zh) * 2011-07-15 2014-04-09 索尔维公司 获得过氧化氢的方法和用于该方法的催化剂载体
US8986637B2 (en) * 2012-11-30 2015-03-24 Johnson Matthey Public Limited Company Bimetallic catalyst
KR102055389B1 (ko) 2013-11-26 2019-12-12 에스케이이노베이션 주식회사 황산 처리된 Pt-Pd 담지 고분자 전해질 다층박막 촉매의 제조방법
WO2018016359A1 (ja) * 2016-07-19 2018-01-25 三菱瓦斯化学株式会社 過酸化水素製造用貴金属触媒および過酸化水素の製造方法
KR102002482B1 (ko) * 2017-10-12 2019-07-23 한국과학기술연구원 과산화수소 합성용 Immiscible 복합체 촉매 및 이를 이용한 과산화수소 합성 방법
SI25590A (sl) 2018-01-15 2019-07-31 Univerza V Ljubljani Postopek priprave izotopsko označenega vodikovega peroksida
US11192091B2 (en) * 2019-03-22 2021-12-07 The Hong Kong University Of Science And Technology Palladium-ruthenium alloys for electrolyzers
CN110395696A (zh) * 2019-07-26 2019-11-01 四川轻化工大学 一种基于钯基双金属催化甲酸合成双氧水的方法

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Also Published As

Publication number Publication date
CN1210105C (zh) 2005-07-13
CN1378484A (zh) 2002-11-06
TR200200073T2 (tr) 2003-03-21
EP1204477B1 (de) 2010-01-06
KR100554927B1 (ko) 2006-03-03
PL353747A1 (en) 2003-12-01
NZ516005A (en) 2004-06-25
CA2378919C (fr) 2007-10-02
BR0012222B1 (pt) 2011-03-22
DE60043657D1 (de) 2010-02-25
EP1204477A1 (de) 2002-05-15
NO20016240D0 (no) 2001-12-19
FR2796312B1 (fr) 2001-09-07
JP4251809B2 (ja) 2009-04-08
EA004475B1 (ru) 2004-04-29
CA2378919A1 (fr) 2001-01-25
JP2003520662A (ja) 2003-07-08
FR2796312A1 (fr) 2001-01-19
NO323596B1 (no) 2007-06-11
KR20020040740A (ko) 2002-05-30
BR0012222A (pt) 2002-03-26
EA200200172A1 (ru) 2002-08-29
US6958138B1 (en) 2005-10-25
WO2001005501A1 (fr) 2001-01-25
AU764178B2 (en) 2003-08-14
NO20016240L (no) 2001-12-19
AU5538500A (en) 2001-02-05

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