ATE458540T1 - Verfahren zur trennung von propylenglykol von wässrigen zusammensetzungen - Google Patents

Verfahren zur trennung von propylenglykol von wässrigen zusammensetzungen

Info

Publication number
ATE458540T1
ATE458540T1 AT06830581T AT06830581T ATE458540T1 AT E458540 T1 ATE458540 T1 AT E458540T1 AT 06830581 T AT06830581 T AT 06830581T AT 06830581 T AT06830581 T AT 06830581T AT E458540 T1 ATE458540 T1 AT E458540T1
Authority
AT
Austria
Prior art keywords
mixture
propylene glycol
aqueous compositions
separating
separating propylene
Prior art date
Application number
AT06830581T
Other languages
English (en)
Inventor
Armin Diefenbacher
Hans-Georg Goebbel
Stefan Bitterlich
Hartwig Voss
Henning Schultz
Anna Forlin
Renate Patrascu
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from ITMI20052524 external-priority patent/ITMI20052524A1/it
Application filed by Basf Se filed Critical Basf Se
Application granted granted Critical
Publication of ATE458540T1 publication Critical patent/ATE458540T1/de

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/26Multiple-effect evaporating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/02Evaporators with heating coils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/32Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322Reboiler specifications
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S159/00Concentrating evaporators
    • Y10S159/08Multieffect or multistage
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00Distillation: processes, separatory
    • Y10S203/17Saline water conversion

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
AT06830581T 2005-12-29 2006-12-13 Verfahren zur trennung von propylenglykol von wässrigen zusammensetzungen ATE458540T1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ITMI20052524 ITMI20052524A1 (it) 2005-12-29 2005-12-29 Un procedimento per separare propilenglicole da composizioni acquose
US77578906P 2006-02-23 2006-02-23
PCT/EP2006/069647 WO2007074066A1 (en) 2005-12-29 2006-12-13 A process for separating propylene glycol from aqueous compositions

Publications (1)

Publication Number Publication Date
ATE458540T1 true ATE458540T1 (de) 2010-03-15

Family

ID=37835604

Family Applications (1)

Application Number Title Priority Date Filing Date
AT06830581T ATE458540T1 (de) 2005-12-29 2006-12-13 Verfahren zur trennung von propylenglykol von wässrigen zusammensetzungen

Country Status (9)

Country Link
US (1) US8197645B2 (de)
EP (1) EP1973620B1 (de)
KR (1) KR101363846B1 (de)
CN (1) CN101351252B (de)
AT (1) ATE458540T1 (de)
DE (1) DE602006012549D1 (de)
ES (1) ES2340325T3 (de)
RU (1) RU2412929C9 (de)
WO (1) WO2007074066A1 (de)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2459720B1 (de) 2009-07-30 2016-04-27 Metabolic Explorer Mutante glycerol-dehydrogenase zur herstellung einer biochemikalie durch fermentation
CN102575235B (zh) 2009-07-30 2015-05-20 代谢探索者公司 用于通过发酵生产生物化学品的突变甲基乙二醛合酶(mgs)
US8969053B2 (en) 2009-07-30 2015-03-03 Metabolic Explorer Mutant YqhD enzyme for the production of a biochemical by fermentation
KR101818277B1 (ko) 2010-07-14 2018-01-12 다우 글로벌 테크놀로지스 엘엘씨 알킬렌 옥사이드 및 글리콜 에터를 제조하기 위한 방법 및 조립체
EP2686081A4 (de) 2011-04-25 2014-12-10 Trevi Systems Inc Rückgewinnung retrograder löslicher stoffe zur wasserbehandlung durch vorwärtsosmose
US9233900B2 (en) * 2012-05-11 2016-01-12 Sumitomo Chemical Company, Limited Method for producing glycols from oxirane compound
KR101695215B1 (ko) * 2013-10-07 2017-01-11 (주)에어레인 Ipa 함유 폐수로부터 ipa의 농축 및 폐수처리를 위한 병합 막분리 공정
RU2760003C1 (ru) * 2017-11-30 2021-11-22 Чайна Петролиум энд Кемикал Корпорейшн Способ и система для получения алкиленоксида
CN110963891B (zh) * 2018-09-29 2024-02-23 长春美禾科技发展有限公司 一种生物基丙二醇的精制方法
DE102018219557A1 (de) 2018-11-15 2020-05-20 Thyssenkrupp Ag Verfahren zur Herstellung und Reinigung von Propylenglykol
EP3892349A1 (de) * 2020-04-06 2021-10-13 Evonik Operations GmbH Verfahren und anlage zur rückgewinnung von methoxypropanolen aus einem wässrigen strom
CN111517919B (zh) * 2020-04-29 2021-05-11 苏州苏震生物工程有限公司 一种提取发酵法的多元醇的方法
US11148986B1 (en) 2020-04-29 2021-10-19 Suzhou Suzhen Bioengineering Co., Ltd Method for extracting polyol from a fermentation process
CN111559819B (zh) * 2020-04-30 2022-07-12 常州瑞华化工工程技术股份有限公司 一种从丙烯环氧化碱洗废水中回收丙二醇和其它有机物的方法
NL2025637B1 (en) * 2020-05-20 2021-12-07 Ioniqa Tech B V A separation method and reactor system for a glycol-water mixture
CN113135817B (zh) * 2021-04-22 2023-04-18 中建安装集团有限公司 过氧化氢氧化丙烯制备环氧丙烷工艺废水回收醚醇的方法
CN115869771A (zh) * 2022-12-30 2023-03-31 山东产研久膜科技开发有限公司 一种高纯度丙二醇甲醚的制备装置及方法
CN117164435A (zh) * 2023-09-06 2023-12-05 江苏嘉宏新材料有限公司 一种环氧丙烷生产过程中丙二醇产品除去轻组分的工艺

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4005997A (en) 1975-02-24 1977-02-01 The Dow Chemical Company Gas dehydration with liquid desiccants and regeneration thereof
DE3143734A1 (de) * 1981-11-04 1983-05-11 Hoechst Ag, 6230 Frankfurt Verfahren zur kontinuierlichen rektifikation eines alkohole enthaltenden fluessigkeitsgemisches"
US5262013A (en) 1991-07-17 1993-11-16 Amalgamated Technologies, Inc. Coolant recycling method and apparatus
US5552023A (en) * 1993-12-15 1996-09-03 Alliedsignal Inc. Recovery of spent deicing fluid
US5425853A (en) * 1994-06-30 1995-06-20 Lloyd Berg Separation of propylene glycol from ethylene glycol by azeotropic distillation
DE19843697A1 (de) * 1998-09-23 2000-03-30 Basf Ag Verfahren zur Herstellung von hochreinem Monoethylenglykol
DE19843652A1 (de) * 1998-09-23 2000-03-30 Basf Ag Verfahren zur Herstellung von hochreinem Monoethylenglykol
JP3800488B2 (ja) * 2000-05-08 2006-07-26 株式会社日本触媒 エチレングリコールの製造方法
US7141683B2 (en) * 2002-05-02 2006-11-28 Degussa Ag Process for the epoxidation of olefins
DE10233382A1 (de) 2002-07-23 2004-01-29 Basf Ag Verfahren zur kontinuierlich betriebenen Reindestillation des bei der koppel-produktfreien Synthese von Propylenoxid anfallenden 1.2-Propylenglykols
US7323579B2 (en) * 2004-07-07 2008-01-29 Basf Aktiengesellschaft Separation of propylene oxide from a mixture comprising propylene oxide and methanol
US20060161010A1 (en) * 2005-01-18 2006-07-20 Basf Aktiengesellschaft Process for the epoxidation of an olefin with improved energy balance

Also Published As

Publication number Publication date
US20080289948A1 (en) 2008-11-27
KR20080091169A (ko) 2008-10-09
KR101363846B1 (ko) 2014-02-14
RU2412929C2 (ru) 2011-02-27
RU2412929C9 (ru) 2012-04-10
RU2008130915A (ru) 2010-02-10
CN101351252B (zh) 2011-07-20
CN101351252A (zh) 2009-01-21
ES2340325T3 (es) 2010-06-01
EP1973620A1 (de) 2008-10-01
DE602006012549D1 (de) 2010-04-08
EP1973620B1 (de) 2010-02-24
WO2007074066A1 (en) 2007-07-05
US8197645B2 (en) 2012-06-12

Similar Documents

Publication Publication Date Title
ATE458540T1 (de) Verfahren zur trennung von propylenglykol von wässrigen zusammensetzungen
ATE457818T1 (de) Verfahren zur konzentration von wasserlöslichem organischem material
WO2006100320A3 (fr) Procede de conversion d'hydrocarbures aliphatiques poly hydroxyles en chlorhydrines
NO20080122L (no) Blanding av diisononylestere av 1,2syklodikarbonsyrer, fremgangsmate for dere fremstilling og anvendelse derav
DE502006009278D1 (de) Membran-destillationsverfahren und membran-destillationsvorrichtung
WO2009069584A1 (ja) トリレンジアミンの脱水方法および脱水装置
WO2007075580A3 (en) Recovery of residual plant components after distillation of essential oils
BRPI0413017A (pt) processo para separar misturas azeotrópicas ou de ebulição próxima por meio de uma retificação extrativa
AR067766A1 (es) Metodo para modular la expresion de una planta de fosfoenolpiruvato carboxilasa (pepc), proteina de la caja u de clase iii y proteina de pqqc.
NZ585218A (en) Method for the preparation of morphine compounds
ATE358666T1 (de) Verfahren zur reinigung von dimethylacetamid (dmac)
EP1506939A3 (en) Process and apparatus for enriching ammonia
DE502005005419D1 (de) Verfahren zur entfernung von fibronektin aus plasmafraktionen
NO20062749L (no) Fremgangsmate pa separering av trioksan fra en blanding inneholdende trioksan, formaldehyd og vann
ATE279414T1 (de) Verfahren zur herstellung von reinem triethylendiamin (teda)
ATE541942T1 (de) Verfahren zur rückgewinnung von shikimisäure
RU2017141778A (ru) Способ очистки 1,4-диаминобутана
SA521422610B1 (ar) أنظمة وطرق لتحلية تركيبات مائية خلال التحلية الأيزوتروبية غير المتجانسة
ATE386734T1 (de) Verfahren zur herstellung von (4-hydroxy-6-oxo- tetrahydropyran-2-yl) acetonitril und dessen derivaten
MY144850A (en) A process for separating propylene glycol from aqueous compositions
DK1517873T3 (da) Fremgangsmåde til behandling af en remanens af organisk materiale
ATE388948T1 (de) Verfahren zur isolierung von alpha-mangostin
EP1944027A4 (de) Pharmazeutische zusammensetzung zur behandlung oder prävention von nephritis und herstellungsverfahren dafür
CA3069454C (en) Method for producing 3-hydroxy-3-methylbutyrate or salt thereof
WO2006133257A3 (en) Use of cis-epoxyeicosatrienoic acids and inhibitors of soluble epoxide hydrolase to reduce cardiomyopathy

Legal Events

Date Code Title Description
RER Ceased as to paragraph 5 lit. 3 law introducing patent treaties