ATE468312T1 - Verfahren und anlage zur heterogenen synthese von chemischen verbindungen - Google Patents

Verfahren und anlage zur heterogenen synthese von chemischen verbindungen

Info

Publication number
ATE468312T1
ATE468312T1 AT02802977T AT02802977T ATE468312T1 AT E468312 T1 ATE468312 T1 AT E468312T1 AT 02802977 T AT02802977 T AT 02802977T AT 02802977 T AT02802977 T AT 02802977T AT E468312 T1 ATE468312 T1 AT E468312T1
Authority
AT
Austria
Prior art keywords
hetergeneous
synthesis
plant
chemical compounds
compounds
Prior art date
Application number
AT02802977T
Other languages
English (en)
Inventor
Ermanno Filippi
Enrico Rizzi
Mirco Tarozzo
Original Assignee
Methanol Casale Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Methanol Casale Sa filed Critical Methanol Casale Sa
Application granted granted Critical
Publication of ATE468312T1 publication Critical patent/ATE468312T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis
    • C01C1/0405—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst
    • C01C1/0417—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • C01C1/0423—Cold wall reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0207—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal
    • B01J8/0214—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal in a cylindrical annular shaped bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0407—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds
    • B01J8/0415—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis
    • C01C1/0405—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • C07C29/152—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D9/00—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D9/0006—Heat-exchange apparatus having stationary plate-like or laminated conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the plate-like or laminated conduits being enclosed within a pressure vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00309—Controlling the temperature by indirect heat exchange with two or more reactions in heat exchange with each other, such as an endothermic reaction in heat exchange with an exothermic reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Fluid Mechanics (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
AT02802977T 2001-11-11 2002-10-02 Verfahren und anlage zur heterogenen synthese von chemischen verbindungen ATE468312T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP01126840A EP1310475A1 (de) 2001-11-11 2001-11-11 Verfahren und Anlage zur heterogenen Synthese von chemischen Verbindungen
PCT/EP2002/011027 WO2003042143A1 (en) 2001-11-11 2002-10-02 Process and plant for the heterogeneous synthesis of chemical compounds

Publications (1)

Publication Number Publication Date
ATE468312T1 true ATE468312T1 (de) 2010-06-15

Family

ID=8179218

Family Applications (1)

Application Number Title Priority Date Filing Date
AT02802977T ATE468312T1 (de) 2001-11-11 2002-10-02 Verfahren und anlage zur heterogenen synthese von chemischen verbindungen

Country Status (15)

Country Link
US (1) US6946494B2 (de)
EP (2) EP1310475A1 (de)
CN (1) CN1305822C (de)
AR (1) AR037344A1 (de)
AT (1) ATE468312T1 (de)
AU (1) AU2002363759B2 (de)
BR (2) BR0209799A (de)
CA (1) CA2433846C (de)
DE (1) DE60236448D1 (de)
EG (1) EG23247A (de)
MX (1) MXPA03006821A (de)
MY (1) MY131898A (de)
RU (1) RU2310641C2 (de)
UA (1) UA81221C2 (de)
WO (1) WO2003042143A1 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1153653A1 (de) * 2000-05-11 2001-11-14 Methanol Casale S.A. Reaktor für exotherme oder endotherme Reaktionen
EP1221339A1 (de) * 2001-01-05 2002-07-10 Methanol Casale S.A. Katalytischer Reaktor mit Wärmetauscher für endothermischer und exothermischer chemischer Reaktionen
EP1236505A1 (de) * 2001-02-27 2002-09-04 Methanol Casale S.A. Verfahren zur Durchführung von chemischen Reaktionen unter pseudo-isothermischen Bedingungen
MX2007001173A (es) * 2004-01-15 2007-09-25 Methanol Casale Sa Reactor catalitico de lecho fijo.
CN102247792A (zh) * 2011-04-30 2011-11-23 甘肃银光聚银化工有限公司 一种新型多相搅拌反应器
JP2017536229A (ja) * 2014-10-30 2017-12-07 サビック グローバル テクノロジーズ ベスローテン フエンノートシャップ 径方向に設置された冷却板を備えた反応器、及びそれを使用した方法
EP3050849A1 (de) 2015-01-27 2016-08-03 Casale SA Verfahren zur Synthese von Ammoniak
EP3471871A1 (de) * 2016-06-21 2019-04-24 Haldor Topsøe A/S Axial-/radialströmungswandler
EP3401006A1 (de) * 2017-05-11 2018-11-14 Casale Sa Mehrbettkatalysatorumwandler mit zwischenbettkühlung
AR113649A1 (es) * 2017-12-20 2020-05-27 Haldor Topsoe As Convertidor de flujo axial enfriado
AR113648A1 (es) 2017-12-20 2020-05-27 Haldor Topsoe As Convertidor de flujo axial adiabático
CN113226536A (zh) * 2019-02-01 2021-08-06 托普索公司 板式换热器与放热反应器的结合使用
CN109999749A (zh) * 2019-03-15 2019-07-12 中国煤层气集团有限公司 两相或多相反应容器
US12157718B2 (en) 2019-09-27 2024-12-03 Sumitomo Chemical Company, Limited Chemistry reaction method and chemistry reaction device

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3796547A (en) * 1969-11-26 1974-03-12 Texaco Inc Heat exchange apparatus for catalytic system
DE2153437B2 (de) 1971-10-27 1974-11-21 Metallgesellschaft Ag, 6000 Frankfurt Reaktor zur Herstellung von Methanol
DE3201776A1 (de) * 1982-01-21 1983-09-08 Krupp-Koppers Gmbh, 4300 Essen Verfahren zur gleichzeitigen erzeugung von methanol- und ammoniak-synthesegas.
FR2536676B1 (fr) * 1982-11-26 1993-01-22 Inst Francais Du Petrole Reacteurs a plaques pour syntheses chimiques effectuees sous haute pression en phase gazeuse et en catalyse heterogene
SU1370115A1 (ru) * 1986-06-27 1988-01-30 Новомосковский филиал Московского химико-технологического института им.Д.И.Менделеева Способ автоматического управлени температурным режимом реактора синтеза метанола
CN87105309A (zh) 1986-07-24 1988-06-15 苏联科学院托普切也夫石油化工合成所 甲醇的制备方法
DE19605572A1 (de) 1996-02-15 1997-08-21 Metallgesellschaft Ag Verfahren zum Erzeugen von Methanol
RU2136359C1 (ru) * 1997-07-14 1999-09-10 Институт катализа им.Г.К.Борескова СО РАН Реактор для проведения гетерогенного экзотермического синтеза

Also Published As

Publication number Publication date
AR037344A1 (es) 2004-11-03
EP1444186B1 (de) 2010-05-19
MY131898A (en) 2007-09-28
EG23247A (en) 2004-09-29
EP1444186A1 (de) 2004-08-11
CA2433846A1 (en) 2003-05-22
RU2310641C2 (ru) 2007-11-20
CN1305822C (zh) 2007-03-21
US6946494B2 (en) 2005-09-20
BRPI0209799B1 (pt) 2019-07-02
MXPA03006821A (es) 2003-12-04
DE60236448D1 (de) 2010-07-01
AU2002363759B2 (en) 2008-06-05
RU2003128885A (ru) 2005-04-10
CN1498199A (zh) 2004-05-19
BR0209799A (pt) 2004-06-01
CA2433846C (en) 2010-08-17
US20040204507A1 (en) 2004-10-14
EP1310475A1 (de) 2003-05-14
UA81221C2 (en) 2007-12-25
WO2003042143A1 (en) 2003-05-22

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