ATE539805T1 - Verfahren und vorrichtung zur reinigung von hochschmelzenden organischen rohprodukten oder verbindungsgemischen mittels fraktionierter schichtkristallisation - Google Patents
Verfahren und vorrichtung zur reinigung von hochschmelzenden organischen rohprodukten oder verbindungsgemischen mittels fraktionierter schichtkristallisationInfo
- Publication number
- ATE539805T1 ATE539805T1 AT06761242T AT06761242T ATE539805T1 AT E539805 T1 ATE539805 T1 AT E539805T1 AT 06761242 T AT06761242 T AT 06761242T AT 06761242 T AT06761242 T AT 06761242T AT E539805 T1 ATE539805 T1 AT E539805T1
- Authority
- AT
- Austria
- Prior art keywords
- compound mixtures
- organic raw
- raw products
- melting organic
- heat exchanger
- Prior art date
Links
- 238000002844 melting Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 239000000203 mixture Substances 0.000 title abstract 3
- 150000001875 compounds Chemical class 0.000 title abstract 2
- 238000004140 cleaning Methods 0.000 title 1
- 238000002425 crystallisation Methods 0.000 abstract 2
- 230000008025 crystallization Effects 0.000 abstract 2
- 230000008018 melting Effects 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 229930182558 Sterol Natural products 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 238000010583 slow cooling Methods 0.000 abstract 1
- 239000011877 solvent mixture Substances 0.000 abstract 1
- 150000003432 sterols Chemical class 0.000 abstract 1
- 235000003702 sterols Nutrition 0.000 abstract 1
- 230000035900 sweating Effects 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
- B01D9/0031—Evaporation of components of the mixture to be separated by heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Steroid Compounds (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH12542005 | 2005-07-26 | ||
| PCT/CH2006/000391 WO2007012214A1 (en) | 2005-07-26 | 2006-07-26 | Method and device for purifying high melting organic raw products or compound mixtures by means of fractional layer crystallisation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE539805T1 true ATE539805T1 (de) | 2012-01-15 |
Family
ID=35883525
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT06761242T ATE539805T1 (de) | 2005-07-26 | 2006-07-26 | Verfahren und vorrichtung zur reinigung von hochschmelzenden organischen rohprodukten oder verbindungsgemischen mittels fraktionierter schichtkristallisation |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8056362B2 (de) |
| EP (1) | EP1907088B1 (de) |
| CN (1) | CN101247869B (de) |
| AT (1) | ATE539805T1 (de) |
| BR (1) | BRPI0613978B1 (de) |
| CA (1) | CA2616423C (de) |
| NO (1) | NO341184B1 (de) |
| WO (1) | WO2007012214A1 (de) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114230611B (zh) * | 2022-01-26 | 2023-06-20 | 陆宽 | 2-氯-2-氧-1,3,2-二氧磷杂环戊烷的提纯方法 |
| CN115337662B (zh) * | 2022-08-29 | 2024-07-19 | 宁夏宁东泰和化学科技有限公司 | 一种层式熔融结晶提纯间苯二甲酰氯的设备及其提纯方法 |
| CN117205595A (zh) * | 2023-11-07 | 2023-12-12 | 天津纯态化学工程技术有限公司 | 一种层式熔融结晶工艺 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3649708A (en) | 1969-10-16 | 1972-03-14 | Republic Steel Corp | Purification of naphthalene |
| FI65440C (fi) * | 1981-07-21 | 1984-05-10 | Kaukas Ab Oy | Foerfarande foer separering av beta-sitosterol med en laog alfa-sitosterolhalt |
| US4672218A (en) * | 1984-12-04 | 1987-06-09 | The Dow Chemical Company | Method for determining the onset of crystallization |
| US4961935A (en) * | 1987-12-23 | 1990-10-09 | Warner-Lambert Company | Sugarless, substantially anhydrous chewing gum compositions and methods for preparing same |
| JP3188305B2 (ja) * | 1992-05-07 | 2001-07-16 | 月島機械株式会社 | 吸収凝縮器を設けた断熱冷却式溶融晶析方法とその装置 |
| US5767311A (en) * | 1995-06-07 | 1998-06-16 | Glitsch International, Inc. | Method and apparatus for preparing purified terephtalic acid |
| DE19904820A1 (de) * | 1999-02-05 | 2000-08-10 | Stockhausen Chem Fab Gmbh | Verfahren und Vorrichtung zur Reinigung von Stoffen mittels Kristallisation |
| AU7489300A (en) | 1999-09-22 | 2001-04-24 | Cognis Corporation | Purification and recovery of dicarboxylic acids using melt crystallization |
-
2006
- 2006-07-26 CN CN2006800272601A patent/CN101247869B/zh active Active
- 2006-07-26 BR BRPI0613978A patent/BRPI0613978B1/pt not_active IP Right Cessation
- 2006-07-26 AT AT06761242T patent/ATE539805T1/de active
- 2006-07-26 US US11/988,627 patent/US8056362B2/en not_active Expired - Fee Related
- 2006-07-26 WO PCT/CH2006/000391 patent/WO2007012214A1/en not_active Ceased
- 2006-07-26 CA CA2616423A patent/CA2616423C/en active Active
- 2006-07-26 EP EP06761242A patent/EP1907088B1/de active Active
-
2008
- 2008-02-25 NO NO20080984A patent/NO341184B1/no not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| BRPI0613978B1 (pt) | 2017-03-28 |
| EP1907088B1 (de) | 2012-01-04 |
| WO2007012214A1 (en) | 2007-02-01 |
| NO20080984L (no) | 2008-02-25 |
| CN101247869B (zh) | 2011-06-08 |
| BRPI0613978A2 (pt) | 2011-02-22 |
| US8056362B2 (en) | 2011-11-15 |
| CA2616423C (en) | 2013-01-08 |
| NO341184B1 (no) | 2017-09-04 |
| CN101247869A (zh) | 2008-08-20 |
| US20090209773A1 (en) | 2009-08-20 |
| EP1907088A1 (de) | 2008-04-09 |
| CA2616423A1 (en) | 2007-02-01 |
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