ATE540962T1 - Extraktive verfahren zur aufreinigung von sucralose - Google Patents
Extraktive verfahren zur aufreinigung von sucraloseInfo
- Publication number
- ATE540962T1 ATE540962T1 AT03744177T AT03744177T ATE540962T1 AT E540962 T1 ATE540962 T1 AT E540962T1 AT 03744177 T AT03744177 T AT 03744177T AT 03744177 T AT03744177 T AT 03744177T AT E540962 T1 ATE540962 T1 AT E540962T1
- Authority
- AT
- Austria
- Prior art keywords
- sucralose
- purification
- extractive process
- extractive
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
- C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Extraction Or Liquid Replacement (AREA)
- Saccharide Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Seasonings (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/092,715 US7049435B2 (en) | 2002-03-08 | 2002-03-08 | Extractive methods for purifying sucralose |
| PCT/US2003/006627 WO2003076453A1 (en) | 2002-03-08 | 2003-03-06 | Extractive methods for purifying sucralose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE540962T1 true ATE540962T1 (de) | 2012-01-15 |
Family
ID=27804178
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT03744177T ATE540962T1 (de) | 2002-03-08 | 2003-03-06 | Extraktive verfahren zur aufreinigung von sucralose |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US7049435B2 (de) |
| EP (2) | EP2039699A3 (de) |
| JP (1) | JP5196702B2 (de) |
| KR (1) | KR101024882B1 (de) |
| CN (1) | CN1318437C (de) |
| AR (1) | AR038901A1 (de) |
| AT (1) | ATE540962T1 (de) |
| AU (1) | AU2003216515B2 (de) |
| BR (1) | BR0308261A (de) |
| CA (1) | CA2481405A1 (de) |
| IL (1) | IL163662A0 (de) |
| MX (1) | MXPA04009842A (de) |
| RU (1) | RU2326887C2 (de) |
| TW (1) | TW200408647A (de) |
| WO (1) | WO2003076453A1 (de) |
Families Citing this family (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6890581B2 (en) * | 2002-04-05 | 2005-05-10 | Tate & Lyle Public Limited Company | Methods for buffer stabilized aqueous deacylation |
| WO2005087020A1 (en) * | 2004-03-05 | 2005-09-22 | Richmond Chemical Corporation | High-intensity sweetener-polyol compositions |
| CN101098971B (zh) * | 2004-12-10 | 2010-04-21 | V.B.医疗保险私人有限公司 | 有助于从含水反应混合物中选择性萃取4,1',6'三氯半乳蔗糖的盐 |
| US20060188629A1 (en) * | 2005-01-21 | 2006-08-24 | Greg Liesen | Method for the purification of sucralose |
| CN102124017A (zh) * | 2005-06-01 | 2011-07-13 | V.B.医疗保险私人有限公司 | 利用溶剂萃取法纯化氯化蔗糖衍生物的方法 |
| GB2443147A (en) * | 2005-08-30 | 2008-04-23 | Pharmed Medicare Pvt Ltd | Removal of pyridine and pyridine analogs from reaction mass containing sucrose esters |
| US9101160B2 (en) | 2005-11-23 | 2015-08-11 | The Coca-Cola Company | Condiments with high-potency sweetener |
| US7741477B2 (en) * | 2006-01-10 | 2010-06-22 | Alembic Limited | Process for purification of sucralose |
| US9012626B2 (en) * | 2006-06-19 | 2015-04-21 | The Coca-Cola Company | Rebaudioside a composition and method for purifying rebaudioside a |
| US8791253B2 (en) * | 2006-06-19 | 2014-07-29 | The Coca-Cola Company | Rebaudioside A composition and method for purifying rebaudioside A |
| EP2046805A1 (de) * | 2006-07-06 | 2009-04-15 | Alembic Limited | Verbessertes verfahren zur herstellung von hochreiner sucralose |
| US8017168B2 (en) | 2006-11-02 | 2011-09-13 | The Coca-Cola Company | High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith |
| US8030481B2 (en) | 2007-05-21 | 2011-10-04 | The Coca-Cola Company | Stevioside polymorphic and amorphous forms, methods for their formulation, and uses |
| US8436156B2 (en) * | 2008-01-04 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
| EP2254677A1 (de) * | 2008-03-20 | 2010-12-01 | Tate & Lyle Technology Limited | Entfernung von säuren aus tertiäramid-lösungsmitteln |
| US8436157B2 (en) * | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
| WO2009124113A1 (en) * | 2008-04-03 | 2009-10-08 | Tate & Lyle Technology Ltd. | Extraction of less polar impurities from sucralose containing aqueous feed streams |
| AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
| KR20100127875A (ko) * | 2008-04-03 | 2010-12-06 | 테이트 앤드 라일 테크놀러지 리미티드 | 수크랄로오스 추출 효율에 대한 탄수화물 농도의 효과 |
| US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
| US20090299055A1 (en) * | 2008-04-03 | 2009-12-03 | Tate & Lyle Technology Limited | Purification of Sucralose Containing Feed Streams for Sucralose Crystallization |
| GB2468936B (en) | 2009-03-27 | 2011-09-07 | Mohamad Rami Radwan Jaber | Chlorination of sucrose-6-esters |
| GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
| GB2469158B (en) | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
| US8609805B2 (en) | 2009-04-15 | 2013-12-17 | Invista North America S.A R.L. | Copolyether glycol manufacturing process |
| GB2474310B (en) | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
| GB2474311B (en) * | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
| GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
| CN102391319B (zh) * | 2011-10-14 | 2015-01-07 | 山东三和维信生物科技有限公司 | 三氯蔗糖的结晶方法 |
| WO2013056128A1 (en) * | 2011-10-14 | 2013-04-18 | Lexington Pharmaceuticals Laboratories, Llc | Chlorination of carbohydrates and carbohydrate derivatives |
| CN102391320B (zh) * | 2011-12-23 | 2014-03-19 | 盐城捷康三氯蔗糖制造有限公司 | 溶剂热回流纯化三氯蔗糖的方法 |
| US10227367B2 (en) | 2013-12-16 | 2019-03-12 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
| WO2016020635A1 (en) | 2014-08-08 | 2016-02-11 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
| CN104387427A (zh) * | 2014-10-30 | 2015-03-04 | 安徽金禾实业股份有限公司 | 一种三氯蔗糖的生产方法 |
| GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
| CN104861003A (zh) * | 2015-04-24 | 2015-08-26 | 吉安市新琪安科技有限公司 | 一种三氯蔗糖母液的处理方法 |
| GB2551591B (en) * | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
| JP7010944B2 (ja) * | 2016-12-07 | 2022-02-10 | モンサント テクノロジー エルエルシー | クロロフェノール塩を精製、回収および転換するためならびにそれから調製される生成物を調製および回収するための方法 |
| CN106674292B (zh) * | 2016-12-09 | 2019-02-22 | 福建科宏生物工程股份有限公司 | 一种三氯蔗糖水结晶母液的提纯处理方法 |
| CN108264527A (zh) * | 2018-01-15 | 2018-07-10 | 山东三和维信生物科技有限公司 | 一种提高三氯蔗糖纯度的方法 |
| CN109315745A (zh) * | 2018-10-28 | 2019-02-12 | 四川泰之味食品有限公司 | 一种泡椒花生及其制备方法 |
| CN111499672B (zh) * | 2019-01-30 | 2021-07-20 | 山东新和成精化科技有限公司 | 一种用于纯化三氯蔗糖的萃取方法 |
| WO2022067621A1 (zh) | 2020-09-30 | 2022-04-07 | 安徽金禾实业股份有限公司 | 三氯蔗糖的纯化方法 |
| EP4215538B1 (de) * | 2020-11-13 | 2026-03-11 | Anhui Jinhe Industrial Co., Ltd. | Verfahren zur reinigung von sucralose |
| WO2024082177A1 (zh) * | 2022-10-19 | 2024-04-25 | 安徽金禾实业股份有限公司 | 一种利用水解体系制备三氯蔗糖粗品的方法 |
| CN116134043A (zh) * | 2022-10-19 | 2023-05-16 | 安徽金禾实业股份有限公司 | 一种利用改进的水解体系制备三氯蔗糖粗品的方法 |
| WO2024082157A1 (zh) * | 2022-10-19 | 2024-04-25 | 安徽金禾实业股份有限公司 | 一种利用改进的醇水碱解体系制备三氯蔗糖粗品的方法 |
Family Cites Families (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3065399D1 (en) | 1979-12-18 | 1983-11-24 | Tate & Lyle Plc | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| GB2065646B (en) * | 1979-12-18 | 1983-10-05 | Tate & Lyle Ltd | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose |
| ZA807578B (en) * | 1979-12-18 | 1981-11-25 | Tate & Lyle Patent Holdings | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| DE3062467D1 (en) | 1979-12-20 | 1983-04-28 | Tate & Lyle Plc | Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| ATE9355T1 (de) | 1980-07-08 | 1984-09-15 | Tate & Lyle Public Limited Company | Verfahren zur herstellung von 4,1',6'-trichlor4,1',6'-trideoxygalactosucrose (tgs). |
| CA1183133A (en) | 1980-10-28 | 1985-02-26 | Tate & Lyle Public Limited Company | Sweet chlorine-substituted disaccharides |
| GB8525871D0 (en) | 1985-10-21 | 1985-11-27 | Tate & Lyle Plc | Chemical compound |
| ES2052923T3 (es) * | 1988-09-16 | 1994-07-16 | Tate & Lyle Plc | Un procedimiento para la cloracion de azucares. |
| GB8822673D0 (en) | 1988-09-27 | 1988-11-02 | Tate & Lyle Plc | Selective acylation of sugars |
| GB8822674D0 (en) | 1988-09-27 | 1988-11-02 | Tate & Lyle Plc | Preparation of acylated sucrose derivatives |
| NZ234143A (en) | 1989-06-28 | 1991-10-25 | Mcneil Ppc Inc | Aqueous pharmaceutical suspension formulation for administering substantially insoluble pharmaceutical agents |
| US4980463A (en) | 1989-07-18 | 1990-12-25 | Noramco, Inc. | Sucrose-6-ester chlorination |
| US5034551A (en) | 1990-04-23 | 1991-07-23 | Noramco, Inc. | Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds |
| NZ240818A (en) * | 1990-12-14 | 1993-08-26 | Mcneil Ppc Inc | Liquid sucralose concentrate compositions containing preservative, buffer and liquid |
| US5272137A (en) | 1992-02-14 | 1993-12-21 | Mcneil-Pfc, Inc. | Aqueous pharmaceutical suspension for pharmaceutical actives |
| US5397588A (en) | 1992-06-18 | 1995-03-14 | Mcneil-Ppc, Inc. | Reduced calorie fruit spreads |
| US5270071A (en) | 1992-06-18 | 1993-12-14 | Mcneil-Ppc, Inc. | Reduced calorie fruit spreads |
| US5354902A (en) | 1992-10-26 | 1994-10-11 | Mcneil-Ppc, Inc. | Stabilized sorbic acid or salt thereof |
| CA2110313C (en) | 1992-12-01 | 2004-10-26 | Edward John Roche | Pharmaceutical compositions containing a guanidinothiazole compound and antacids |
| US5298611A (en) | 1993-03-12 | 1994-03-29 | Mcneil-Ppc, Inc. | Sucralose pentaester production |
| US5530106A (en) | 1993-03-12 | 1996-06-25 | Mcneil-Ppc, Inc. | Recovery of sucralose intermediates |
| EP0620001A1 (de) | 1993-04-16 | 1994-10-19 | McNEIL-PPC, INC. | Wässrige pharmazeutische Suspension und Verfahren zu ihrer Herstellung |
| CA2128820A1 (en) | 1993-07-27 | 1995-01-28 | Walter G. Gowan, Jr. | Rapidly disintegrating pharmaceutical dosage form and process for preparation thereof |
| US5674522A (en) | 1993-10-07 | 1997-10-07 | Mcneil-Ppc, Inc. | Beverage concentrate for drug delivery |
| US5498709A (en) * | 1994-10-17 | 1996-03-12 | Mcneil-Ppc, Inc. | Production of sucralose without intermediate isolation of crystalline sucralose-6-ester |
| US5593696A (en) | 1994-11-21 | 1997-01-14 | Mcneil-Ppc, Inc. | Stabilized composition of famotidine and sucralfate for treatment of gastrointestinal disorders |
| ES2231964T3 (es) * | 1997-02-13 | 2005-05-16 | TATE & LYLE PUBLIC LIMITED COMPANY | Purificacion cromatografica de sucrosa clorada. |
| AU753587B2 (en) | 1997-11-14 | 2002-10-24 | Johnson & Johnson Consumer Companies, Inc. | Highly flavored dental floss |
| BR9912529A (pt) | 1998-07-07 | 2001-05-02 | Johnson & Johnson | Método de aperfeiçoamento da liberação de doçura da sucralose |
| US6090401A (en) | 1999-03-31 | 2000-07-18 | Mcneil-Ppc, Inc. | Stable foam composition |
| US6211246B1 (en) | 1999-06-10 | 2001-04-03 | Mcneil-Ppc, Inc. | Rapidly absorbed liquid compositions |
| US6258381B1 (en) | 2000-02-11 | 2001-07-10 | Mcneil-Ppc, Inc. | Tablet and process for making the same |
| US6277409B1 (en) | 2000-02-11 | 2001-08-21 | Mcneil-Ppc, Inc. | Protective coating for tablet |
-
2002
- 2002-03-08 US US10/092,715 patent/US7049435B2/en not_active Expired - Lifetime
-
2003
- 2003-03-06 MX MXPA04009842A patent/MXPA04009842A/es active IP Right Grant
- 2003-03-06 CN CNB038055279A patent/CN1318437C/zh not_active Expired - Lifetime
- 2003-03-06 JP JP2003574668A patent/JP5196702B2/ja not_active Expired - Fee Related
- 2003-03-06 EP EP08011594A patent/EP2039699A3/de not_active Withdrawn
- 2003-03-06 WO PCT/US2003/006627 patent/WO2003076453A1/en not_active Ceased
- 2003-03-06 EP EP03744177A patent/EP1483278B1/de not_active Expired - Lifetime
- 2003-03-06 AT AT03744177T patent/ATE540962T1/de active
- 2003-03-06 AU AU2003216515A patent/AU2003216515B2/en not_active Ceased
- 2003-03-06 CA CA002481405A patent/CA2481405A1/en not_active Abandoned
- 2003-03-06 RU RU2004129749/04A patent/RU2326887C2/ru not_active IP Right Cessation
- 2003-03-06 KR KR1020047014006A patent/KR101024882B1/ko not_active Expired - Fee Related
- 2003-03-06 BR BR0308261-0A patent/BR0308261A/pt not_active IP Right Cessation
- 2003-03-06 IL IL16366203A patent/IL163662A0/xx unknown
- 2003-03-07 TW TW092104871A patent/TW200408647A/zh unknown
- 2003-03-07 AR ARP030100792A patent/AR038901A1/es not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| CN1318437C (zh) | 2007-05-30 |
| CA2481405A1 (en) | 2003-09-18 |
| MXPA04009842A (es) | 2005-06-17 |
| AU2003216515A1 (en) | 2003-09-22 |
| EP2039699A3 (de) | 2010-11-17 |
| US7049435B2 (en) | 2006-05-23 |
| KR101024882B1 (ko) | 2011-03-31 |
| AR038901A1 (es) | 2005-02-02 |
| RU2004129749A (ru) | 2005-04-20 |
| KR20040099305A (ko) | 2004-11-26 |
| BR0308261A (pt) | 2005-01-04 |
| AU2003216515B2 (en) | 2008-07-10 |
| EP1483278A1 (de) | 2004-12-08 |
| IL163662A0 (en) | 2005-12-18 |
| EP1483278B1 (de) | 2012-01-11 |
| JP5196702B2 (ja) | 2013-05-15 |
| JP2005526075A (ja) | 2005-09-02 |
| RU2326887C2 (ru) | 2008-06-20 |
| EP2039699A2 (de) | 2009-03-25 |
| CN1646551A (zh) | 2005-07-27 |
| WO2003076453A1 (en) | 2003-09-18 |
| TW200408647A (en) | 2004-06-01 |
| US20030171574A1 (en) | 2003-09-11 |
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