ATE549619T1 - Vorrichtung und verfahren zur charakterisierung von polymeren - Google Patents
Vorrichtung und verfahren zur charakterisierung von polymerenInfo
- Publication number
- ATE549619T1 ATE549619T1 AT06718819T AT06718819T ATE549619T1 AT E549619 T1 ATE549619 T1 AT E549619T1 AT 06718819 T AT06718819 T AT 06718819T AT 06718819 T AT06718819 T AT 06718819T AT E549619 T1 ATE549619 T1 AT E549619T1
- Authority
- AT
- Austria
- Prior art keywords
- tref
- gpc
- characterization
- polymer sample
- fractionation
- Prior art date
Links
- 229920000642 polymer Polymers 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- 238000012512 characterization method Methods 0.000 abstract 3
- 238000005194 fractionation Methods 0.000 abstract 3
- 238000004458 analytical method Methods 0.000 abstract 1
- 238000010828 elution Methods 0.000 abstract 1
- 230000001360 synchronised effect Effects 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/468—Flow patterns using more than one column involving switching between different column configurations
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N2030/0075—Separation due to differential desorption
- G01N2030/008—Thermal desorption
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/3007—Control of physical parameters of the fluid carrier of temperature same temperature for whole column
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/14—Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation
- G01N25/147—Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation by cristallisation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
- G01N30/463—Flow patterns using more than one column with serial coupling of separation columns for multidimensional chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/50—Conditioning of the sorbent material or stationary liquid
- G01N30/52—Physical parameters
- G01N30/54—Temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
- G01N33/442—Resins; Plastics
Landscapes
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Examining Or Testing Airtightness (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US64633105P | 2005-01-24 | 2005-01-24 | |
| PCT/US2006/001803 WO2006081116A1 (en) | 2005-01-24 | 2006-01-19 | Apparatus for method for polymer characterization |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE549619T1 true ATE549619T1 (de) | 2012-03-15 |
Family
ID=36499304
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT06718819T ATE549619T1 (de) | 2005-01-24 | 2006-01-19 | Vorrichtung und verfahren zur charakterisierung von polymeren |
Country Status (5)
| Country | Link |
|---|---|
| US (3) | US7985593B2 (de) |
| EP (2) | EP2410325B1 (de) |
| AT (1) | ATE549619T1 (de) |
| ES (1) | ES2632565T3 (de) |
| WO (1) | WO2006081116A1 (de) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE549619T1 (de) | 2005-01-24 | 2012-03-15 | Dow Global Technologies Llc | Vorrichtung und verfahren zur charakterisierung von polymeren |
| MX2007014763A (es) * | 2005-05-24 | 2008-02-12 | Chevron Phillips Chemical Co | Un metodo bidimensional en linea integrado y dispositivo para fraccionamiento de elucion de elevacion de temperatura analitica sincronizada y cromatografia de permeacion de gel. |
| EP1950241A1 (de) | 2007-01-25 | 2008-07-30 | Borealis Technology Oy | Multimodale Polyethylenzusammensetzung |
| US8722817B2 (en) | 2009-06-05 | 2014-05-13 | Dow Global Technologies Llc | Process to make long chain branched (LCB), block, or interconnected copolymers of ethylene |
| US20110003940A1 (en) | 2009-07-01 | 2011-01-06 | Dow Global Technologies Inc. | Ethylene-based polymer compositions for use as a blend component in shrinkage film applications |
| US8629214B2 (en) | 2009-07-01 | 2014-01-14 | Dow Global Technologies Llc. | Ethylene-based polymer compositions for use as a blend component in shrinkage film applications |
| US8318896B2 (en) * | 2009-12-21 | 2012-11-27 | Dow Global Technologies Llc | Chromatography of polyolefin polymers |
| JP5975987B2 (ja) | 2010-06-14 | 2016-08-23 | ダウ グローバル テクノロジーズ エルエルシー | シュリンクフィルム用途においてブレンド成分として使用するためのエチレン系ポリマー組成物 |
| CN102958692A (zh) | 2010-06-24 | 2013-03-06 | 陶氏环球技术有限公司 | 包含乙烯和任选硅烷的长链支化(lcb)嵌段或互连共聚物的电子器件模块 |
| KR20130098353A (ko) | 2010-09-29 | 2013-09-04 | 다우 글로벌 테크놀로지스 엘엘씨 | 수축 필름 응용에 사용하기 적합한 에틸렌/알파-올레핀 인터폴리머, 및 그로부터 제조된 물품 |
| BR112013007288B1 (pt) | 2010-09-29 | 2022-05-31 | Dow Global Technologies Llc | Processo para fazer um interpolímero de etileno/alfa-olefina |
| WO2012166861A1 (en) | 2011-06-02 | 2012-12-06 | Dow Global Technologies Llc | Size exclusion chromatography of polymers |
| JP5992036B2 (ja) | 2011-06-03 | 2016-09-14 | ダウ グローバル テクノロジーズ エルエルシー | ポリマーのクロマトグラフィー |
| EP3008462B1 (de) | 2013-06-14 | 2022-07-27 | Waters Technologies Corporation | Vorgehensweise für skalierungsverfahren zwischen chromatografiesystemen mit superkritischen flüssigkeiten |
| WO2015023533A1 (en) * | 2013-08-12 | 2015-02-19 | Waters Technologies Corporation | Mobile phase controller for supercritical fluid chromatography systems |
| WO2017040127A1 (en) | 2015-08-28 | 2017-03-09 | Dow Global Technologies Llc | Chromatography of polymers with reduced co-crystallization |
| KR102641325B1 (ko) | 2015-09-01 | 2024-02-28 | 다우 글로벌 테크놀로지스 엘엘씨 | 상이한 미세구조를 갖는 올레핀계 중합체의 크로마토그래피 분해능을 증가시키는 방법 |
| US10302621B2 (en) | 2016-06-15 | 2019-05-28 | Exxonmobil Chemical Patents Inc. | Methods for characterizing branching distribution in polymers |
| US10732158B2 (en) | 2016-08-31 | 2020-08-04 | Exxonmobil Chemical Patents Inc. | Integrated high-throughput methods to characterize multi-component polymers |
| WO2019090092A1 (en) | 2017-11-02 | 2019-05-09 | Dow Global Technologies Llc | Chromatography of polymers using particles coated with graphene-based compositions |
| CN112534249A (zh) | 2018-06-29 | 2021-03-19 | 陶氏环球技术有限责任公司 | 聚合物的无定形含量的测定 |
| US11802865B2 (en) | 2021-12-27 | 2023-10-31 | Chevron Phillips Chemical Company Lp | Utilizing aTREF data with chemometric analysis for determining the types of polyethylene present in polymer blends and multilayer films |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6260407B1 (en) | 1998-04-03 | 2001-07-17 | Symyx Technologies, Inc. | High-temperature characterization of polymers |
| US6612153B2 (en) * | 2001-06-05 | 2003-09-02 | Agilent Technologies, Inc. | Planar manifold with integrated heated injector inlet and unheated pneumatics |
| US20030037592A1 (en) * | 2001-08-21 | 2003-02-27 | Thermo Finnigan Llc | Gas chromatograph oven assembly |
| JP4564842B2 (ja) | 2002-05-15 | 2010-10-20 | ダウ グローバル テクノロジーズ インコーポレーテッド | 高分子の分子位相的分別 |
| US7507337B2 (en) * | 2004-09-03 | 2009-03-24 | Symyx Technologies, Inc. | System and method for rapid chromatography with fluid temperature and mobile phase composition control |
| ATE549619T1 (de) | 2005-01-24 | 2012-03-15 | Dow Global Technologies Llc | Vorrichtung und verfahren zur charakterisierung von polymeren |
| MX2007014763A (es) * | 2005-05-24 | 2008-02-12 | Chevron Phillips Chemical Co | Un metodo bidimensional en linea integrado y dispositivo para fraccionamiento de elucion de elevacion de temperatura analitica sincronizada y cromatografia de permeacion de gel. |
-
2006
- 2006-01-19 AT AT06718819T patent/ATE549619T1/de active
- 2006-01-19 WO PCT/US2006/001803 patent/WO2006081116A1/en not_active Ceased
- 2006-01-19 EP EP11185804.9A patent/EP2410325B1/de not_active Expired - Lifetime
- 2006-01-19 EP EP06718819A patent/EP1853905B1/de not_active Expired - Lifetime
- 2006-01-19 ES ES11185804.9T patent/ES2632565T3/es not_active Expired - Lifetime
- 2006-01-19 US US11/794,417 patent/US7985593B2/en not_active Expired - Fee Related
-
2011
- 2011-06-15 US US13/160,883 patent/US8323569B2/en not_active Expired - Fee Related
-
2012
- 2012-11-08 US US13/672,363 patent/US20130061662A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| US20080166817A1 (en) | 2008-07-10 |
| WO2006081116B1 (en) | 2006-11-09 |
| US20130061662A1 (en) | 2013-03-14 |
| ES2632565T3 (es) | 2017-09-14 |
| EP2410325B1 (de) | 2017-05-17 |
| WO2006081116A1 (en) | 2006-08-03 |
| EP2410325A1 (de) | 2012-01-25 |
| US8323569B2 (en) | 2012-12-04 |
| EP1853905B1 (de) | 2012-03-14 |
| EP1853905A1 (de) | 2007-11-14 |
| US7985593B2 (en) | 2011-07-26 |
| US20110239746A1 (en) | 2011-10-06 |
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