ATE549619T1 - Vorrichtung und verfahren zur charakterisierung von polymeren - Google Patents
Vorrichtung und verfahren zur charakterisierung von polymerenInfo
- Publication number
- ATE549619T1 ATE549619T1 AT06718819T AT06718819T ATE549619T1 AT E549619 T1 ATE549619 T1 AT E549619T1 AT 06718819 T AT06718819 T AT 06718819T AT 06718819 T AT06718819 T AT 06718819T AT E549619 T1 ATE549619 T1 AT E549619T1
- Authority
- AT
- Austria
- Prior art keywords
- tref
- gpc
- characterization
- polymer sample
- fractionation
- Prior art date
Links
- 229920000642 polymer Polymers 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- 238000012512 characterization method Methods 0.000 abstract 3
- 238000005194 fractionation Methods 0.000 abstract 3
- 238000004458 analytical method Methods 0.000 abstract 1
- 238000010828 elution Methods 0.000 abstract 1
- 230000001360 synchronised effect Effects 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/468—Flow patterns using more than one column involving switching between different column configurations
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N2030/0075—Separation due to differential desorption
- G01N2030/008—Thermal desorption
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/3007—Control of physical parameters of the fluid carrier of temperature same temperature for whole column
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/14—Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation
- G01N25/147—Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation by cristallisation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
- G01N30/463—Flow patterns using more than one column with serial coupling of separation columns for multidimensional chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/50—Conditioning of the sorbent material or stationary liquid
- G01N30/52—Physical parameters
- G01N30/54—Temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
- G01N33/442—Resins; Plastics
Landscapes
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Examining Or Testing Airtightness (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US64633105P | 2005-01-24 | 2005-01-24 | |
| PCT/US2006/001803 WO2006081116A1 (en) | 2005-01-24 | 2006-01-19 | Apparatus for method for polymer characterization |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE549619T1 true ATE549619T1 (de) | 2012-03-15 |
Family
ID=36499304
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT06718819T ATE549619T1 (de) | 2005-01-24 | 2006-01-19 | Vorrichtung und verfahren zur charakterisierung von polymeren |
Country Status (5)
| Country | Link |
|---|---|
| US (3) | US7985593B2 (de) |
| EP (2) | EP2410325B1 (de) |
| AT (1) | ATE549619T1 (de) |
| ES (1) | ES2632565T3 (de) |
| WO (1) | WO2006081116A1 (de) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2632565T3 (es) | 2005-01-24 | 2017-09-14 | Dow Global Technologies Llc | Aparato y métodos para la caracterización de polímeros |
| MX2007014763A (es) * | 2005-05-24 | 2008-02-12 | Chevron Phillips Chemical Co | Un metodo bidimensional en linea integrado y dispositivo para fraccionamiento de elucion de elevacion de temperatura analitica sincronizada y cromatografia de permeacion de gel. |
| EP1950241A1 (de) | 2007-01-25 | 2008-07-30 | Borealis Technology Oy | Multimodale Polyethylenzusammensetzung |
| US8722817B2 (en) | 2009-06-05 | 2014-05-13 | Dow Global Technologies Llc | Process to make long chain branched (LCB), block, or interconnected copolymers of ethylene |
| US20110003940A1 (en) | 2009-07-01 | 2011-01-06 | Dow Global Technologies Inc. | Ethylene-based polymer compositions for use as a blend component in shrinkage film applications |
| US8629214B2 (en) | 2009-07-01 | 2014-01-14 | Dow Global Technologies Llc. | Ethylene-based polymer compositions for use as a blend component in shrinkage film applications |
| US8318896B2 (en) * | 2009-12-21 | 2012-11-27 | Dow Global Technologies Llc | Chromatography of polyolefin polymers |
| JP5975987B2 (ja) | 2010-06-14 | 2016-08-23 | ダウ グローバル テクノロジーズ エルエルシー | シュリンクフィルム用途においてブレンド成分として使用するためのエチレン系ポリマー組成物 |
| CN102958692A (zh) | 2010-06-24 | 2013-03-06 | 陶氏环球技术有限公司 | 包含乙烯和任选硅烷的长链支化(lcb)嵌段或互连共聚物的电子器件模块 |
| WO2012044293A1 (en) | 2010-09-29 | 2012-04-05 | Dow Global Technologies Llc | An ethylene/alpha-olefin interpolymer suitable for use in fiber applications, and fibers made therefrom |
| BR112013006985A2 (pt) | 2010-09-29 | 2020-11-24 | Dow Global Technologies Llc | interpolímero de eitleno/alfa-olefina, processo para preparar um interpolímero de etileno/alfa-olefina, composição e filme. |
| WO2012166861A1 (en) | 2011-06-02 | 2012-12-06 | Dow Global Technologies Llc | Size exclusion chromatography of polymers |
| US10274465B2 (en) | 2011-06-03 | 2019-04-30 | Dow Global Technologies Llc | Chromatography of polymers |
| US11565197B2 (en) | 2013-06-14 | 2023-01-31 | Waters Technologies Corporation | Methodology for scaling methods between supercritical fluid chromatography systems |
| EP3033159B1 (de) | 2013-08-12 | 2023-04-19 | Waters Technologies Corporation | Mobiler phasenregler für superkritische flüssigkeitschromatografiesysteme |
| JP6797897B6 (ja) | 2015-08-28 | 2021-01-20 | ダウ グローバル テクノロジーズ エルエルシー | 低減した共結晶化を有するポリマーのクロマトグラフィー |
| ES2784322T3 (es) | 2015-09-01 | 2020-09-24 | Dow Global Technologies Llc | Método para aumentar la resolución cromatográfica de polímeros a base de olefina con diferentes microestructuras |
| US10302621B2 (en) | 2016-06-15 | 2019-05-28 | Exxonmobil Chemical Patents Inc. | Methods for characterizing branching distribution in polymers |
| US10732158B2 (en) | 2016-08-31 | 2020-08-04 | Exxonmobil Chemical Patents Inc. | Integrated high-throughput methods to characterize multi-component polymers |
| US11857948B2 (en) | 2017-11-02 | 2024-01-02 | Dow Global Technologies Llc | Chromatography of polymers using particles coated with graphene-based compositions |
| US11988650B2 (en) | 2018-06-29 | 2024-05-21 | Dow Global Technologies Llc | Determination of the amorphous content of polymers |
| US11802865B2 (en) | 2021-12-27 | 2023-10-31 | Chevron Phillips Chemical Company Lp | Utilizing aTREF data with chemometric analysis for determining the types of polyethylene present in polymer blends and multilayer films |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6260407B1 (en) | 1998-04-03 | 2001-07-17 | Symyx Technologies, Inc. | High-temperature characterization of polymers |
| US6612153B2 (en) * | 2001-06-05 | 2003-09-02 | Agilent Technologies, Inc. | Planar manifold with integrated heated injector inlet and unheated pneumatics |
| US20030037592A1 (en) * | 2001-08-21 | 2003-02-27 | Thermo Finnigan Llc | Gas chromatograph oven assembly |
| EP1506393A1 (de) | 2002-05-15 | 2005-02-16 | Dow Gloval Technologies Inc. | Molekültopologiefraktionierung von makromolekülen |
| WO2006029017A1 (en) * | 2004-09-03 | 2006-03-16 | Symyx Technologies, Inc. | System and method for rapid chromatography with fluid temperature and mobile phase composition control |
| ES2632565T3 (es) | 2005-01-24 | 2017-09-14 | Dow Global Technologies Llc | Aparato y métodos para la caracterización de polímeros |
| MX2007014763A (es) * | 2005-05-24 | 2008-02-12 | Chevron Phillips Chemical Co | Un metodo bidimensional en linea integrado y dispositivo para fraccionamiento de elucion de elevacion de temperatura analitica sincronizada y cromatografia de permeacion de gel. |
-
2006
- 2006-01-19 ES ES11185804.9T patent/ES2632565T3/es not_active Expired - Lifetime
- 2006-01-19 EP EP11185804.9A patent/EP2410325B1/de not_active Expired - Lifetime
- 2006-01-19 US US11/794,417 patent/US7985593B2/en not_active Expired - Fee Related
- 2006-01-19 AT AT06718819T patent/ATE549619T1/de active
- 2006-01-19 WO PCT/US2006/001803 patent/WO2006081116A1/en not_active Ceased
- 2006-01-19 EP EP06718819A patent/EP1853905B1/de not_active Expired - Lifetime
-
2011
- 2011-06-15 US US13/160,883 patent/US8323569B2/en not_active Expired - Fee Related
-
2012
- 2012-11-08 US US13/672,363 patent/US20130061662A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP1853905A1 (de) | 2007-11-14 |
| US20130061662A1 (en) | 2013-03-14 |
| US7985593B2 (en) | 2011-07-26 |
| US20110239746A1 (en) | 2011-10-06 |
| EP2410325A1 (de) | 2012-01-25 |
| EP2410325B1 (de) | 2017-05-17 |
| WO2006081116A1 (en) | 2006-08-03 |
| US20080166817A1 (en) | 2008-07-10 |
| US8323569B2 (en) | 2012-12-04 |
| WO2006081116B1 (en) | 2006-11-09 |
| ES2632565T3 (es) | 2017-09-14 |
| EP1853905B1 (de) | 2012-03-14 |
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