AU626176B2 - Improved pitch carbon fiber spinning process - Google Patents

Improved pitch carbon fiber spinning process Download PDF

Info

Publication number: AU626176B2
Authority: AU; Australia
Prior art keywords: opening; capillary; area; spinneret; diameter
Prior art date: 1989-02-16
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Ceased

Application number

AU49844/90A

Other languages

English (en)

Other versions

AU4984490A (en

Inventor

Uel Duane Jennings

Roger Allen Ross

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

University of Tennessee Research Foundation

Original Assignee

EI Du Pont de Nemours and Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-02-16

Filing date

1990-02-16

Publication date

1992-07-23

1990-02-16 Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co

1990-08-23 Publication of AU4984490A publication Critical patent/AU4984490A/en

1992-07-23 Application granted granted Critical

1992-07-23 Publication of AU626176B2 publication Critical patent/AU626176B2/en

2006-07-06 Assigned to UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION reassignment UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION Alteration of Name(s) in Register under S187 Assignors: E.I. DU PONT DE NEMOURS AND COMPANY

2010-02-16 Anticipated expiration legal-status Critical

Status Ceased legal-status Critical Current

Links

229920000049 Carbon (fiber) Polymers 0.000 title claims description 10
239000004917 carbon fiber Substances 0.000 title claims description 10
238000009987 spinning Methods 0.000 title claims description 10
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title description 3
239000000835 fiber Substances 0.000 claims description 52
239000011295 pitch Substances 0.000 claims description 32
238000000034 method Methods 0.000 claims description 21
230000008569 process Effects 0.000 claims description 17
230000006641 stabilisation Effects 0.000 claims description 9
238000011105 stabilization Methods 0.000 claims description 9
238000011144 upstream manufacturing Methods 0.000 claims description 4
239000011302 mesophase pitch Substances 0.000 claims description 2
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
238000005336 cracking Methods 0.000 description 9
238000003763 carbonization Methods 0.000 description 7
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 6
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
238000010438 heat treatment Methods 0.000 description 5
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
230000009286 beneficial effect Effects 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 4
238000009826 distribution Methods 0.000 description 4
229910052799 carbon Inorganic materials 0.000 description 3
238000004519 manufacturing process Methods 0.000 description 3
239000000203 mixture Substances 0.000 description 3
239000008188 pellet Substances 0.000 description 3
SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 2
239000012296 anti-solvent Substances 0.000 description 2
238000013459 approach Methods 0.000 description 2
238000001914 filtration Methods 0.000 description 2
238000005087 graphitization Methods 0.000 description 2
230000004048 modification Effects 0.000 description 2
238000012986 modification Methods 0.000 description 2
238000009656 pre-carbonization Methods 0.000 description 2
238000010791 quenching Methods 0.000 description 2
238000010992 reflux Methods 0.000 description 2
241000234282 Allium Species 0.000 description 1
235000002732 Allium cepa var. cepa Nutrition 0.000 description 1
229920013683 Celanese Polymers 0.000 description 1
CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
241001062472 Stokellia anisodon Species 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000000919 ceramic Substances 0.000 description 1
230000008859 change Effects 0.000 description 1
238000004140 cleaning Methods 0.000 description 1
239000002131 composite material Substances 0.000 description 1
239000012141 concentrate Substances 0.000 description 1
239000002178 crystalline material Substances 0.000 description 1
230000007423 decrease Effects 0.000 description 1
230000001627 detrimental effect Effects 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000003822 epoxy resin Substances 0.000 description 1
238000013023 gasketing Methods 0.000 description 1
229910002804 graphite Inorganic materials 0.000 description 1
239000010439 graphite Substances 0.000 description 1
150000002431 hydrogen Chemical class 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000000155 melt Substances 0.000 description 1
238000002074 melt spinning Methods 0.000 description 1
239000002184 metal Substances 0.000 description 1
239000011317 mixed pitch Substances 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
229920000620 organic polymer Polymers 0.000 description 1
239000004033 plastic Substances 0.000 description 1
238000001907 polarising light microscopy Methods 0.000 description 1
229920000647 polyepoxide Polymers 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
230000009467 reduction Effects 0.000 description 1
230000002787 reinforcement Effects 0.000 description 1
229920002545 silicone oil Polymers 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000002904 solvent Substances 0.000 description 1
238000004381 surface treatment Methods 0.000 description 1
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D4/00—Spinnerette packs; Cleaning thereof
- D01D4/02—Spinnerettes
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/253—Formation of filaments, threads, or the like with a non-circular cross section; Spinnerette packs therefor
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/145—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues

Landscapes

Engineering & Computer Science (AREA)
Textile Engineering (AREA)
Mechanical Engineering (AREA)
Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Inorganic Fibers (AREA)
Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)

AU49844/90A 1989-02-16 1990-02-16 Improved pitch carbon fiber spinning process Ceased AU626176B2 (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US31151189A	1989-02-16	1989-02-16
US311511		1989-02-16

Publications (2)

Publication Number	Publication Date
AU4984490A AU4984490A (en)	1990-08-23
AU626176B2 true AU626176B2 (en)	1992-07-23

Family

ID=23207232

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AU49844/90A Ceased AU626176B2 (en)	1989-02-16	1990-02-16	Improved pitch carbon fiber spinning process

Country Status (7)

Country	Link
EP (1)	EP0383339B1 (fr)
JP (1)	JP2897137B2 (fr)
KR (1)	KR0140867B1 (fr)
AU (1)	AU626176B2 (fr)
CA (1)	CA2009528C (fr)
DE (1)	DE69019193T2 (fr)
ES (1)	ES2072324T3 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP4601875B2 (ja) *	2001-08-02	2010-12-22	新日鉄マテリアルズ株式会社	炭素繊維の製造方法
WO2015016199A1 (fr) *	2013-07-30	2015-02-05	東レ株式会社	Faisceau de fibres de carbone et faisceau de fibres ignifugées
CN104047066B (zh) *	2014-07-01	2016-08-17	陕西天策新材料科技有限公司	一种中间相沥青熔融纺丝方法
MX2022004597A (es) *	2019-10-17	2022-07-21	Tangold Inc	Fabricacion de fibras de carbono con altas propiedades mecanicas.
CN111830982A (zh) *	2020-07-16	2020-10-27	陕西理工大学	一种移动机器人编队与避障控制方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP0168639A2 (fr) *	1984-06-20	1986-01-22	Teijin Limited	Fibres de carbone ou de graphite à base de brai et procédé pour leur préparation
US4576811A (en) *	1983-11-03	1986-03-18	E. I. Du Pont De Nemours And Company	Process for adjusting the fiber structure of mesophase pitch fibers
US4859381A (en) *	1986-01-22	1989-08-22	Osaka Gas Company Limited	Process for preparing pitch-type carbon fibers

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH0781211B2 (ja) *	1983-11-10	1995-08-30	株式会社ペトカ	炭素繊維の製造方法
US4859382A (en) *	1986-01-22	1989-08-22	Osaka Gas Company Limited	Process for preparing carbon fibers elliptical in section

1990
- 1990-02-07 CA CA002009528A patent/CA2009528C/fr not_active Expired - Fee Related
- 1990-02-15 KR KR1019900001826A patent/KR0140867B1/ko not_active Expired - Fee Related
- 1990-02-15 JP JP2032608A patent/JP2897137B2/ja not_active Expired - Fee Related
- 1990-02-16 EP EP90103030A patent/EP0383339B1/fr not_active Expired - Lifetime
- 1990-02-16 DE DE69019193T patent/DE69019193T2/de not_active Expired - Fee Related
- 1990-02-16 ES ES90103030T patent/ES2072324T3/es not_active Expired - Lifetime
- 1990-02-16 AU AU49844/90A patent/AU626176B2/en not_active Ceased

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4576811A (en) *	1983-11-03	1986-03-18	E. I. Du Pont De Nemours And Company	Process for adjusting the fiber structure of mesophase pitch fibers
EP0168639A2 (fr) *	1984-06-20	1986-01-22	Teijin Limited	Fibres de carbone ou de graphite à base de brai et procédé pour leur préparation
US4859381A (en) *	1986-01-22	1989-08-22	Osaka Gas Company Limited	Process for preparing pitch-type carbon fibers

Also Published As

Publication number	Publication date
KR0140867B1 (ko)	1998-07-01
DE69019193D1 (de)	1995-06-14
CA2009528A1 (fr)	1990-08-16
EP0383339A2 (fr)	1990-08-22
AU4984490A (en)	1990-08-23
EP0383339A3 (fr)	1991-08-28
DE69019193T2 (de)	1995-10-12
ES2072324T3 (es)	1995-07-16
JPH02242918A (ja)	1990-09-27
CA2009528C (fr)	2001-01-09
JP2897137B2 (ja)	1999-05-31
KR900013119A (ko)	1990-09-03
EP0383339B1 (fr)	1995-05-10

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CN1064091C (zh)	2001-04-04	可纺丝溶液的离心纺丝法及制成的纤维制品和该制品用途
EP0166388B1 (fr)	1991-11-21	Procédé pour la production de fibres de carbone du type brai
CN1039040C (zh)	1998-07-08	一种用于把纤维素溶液纺制成丝的喷丝板
JPH11512492A (ja)	1999-10-26	中空ポリマファイバを紡糸する装置および方法
GB2180499A (en)	1987-04-01	Apparatus for cooling and conditioning melt-spun material
KR960007714B1 (ko)	1996-06-08	초고 모듈러스와 높은 인장강도가 균형을 이룬 탄소섬유 및 이의 제조방법
EP0031707A2 (fr)	1981-07-08	Procédé de fabrication de fibres de carbone
AU626176B2 (en)	1992-07-23	Improved pitch carbon fiber spinning process
US5437927A (en)	1995-08-01	Pitch carbon fiber spinning process
US5536486A (en)	1996-07-16	Carbon fibers and non-woven fabrics
JPH06294014A (ja)	1994-10-21	導電性繊維の製造方法
US5202072A (en)	1993-04-13	Pitch carbon fiber spinning process
US5169584A (en)	1992-12-08	Method of making small diameter high strength carbon fibers
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JP3427844B2 (ja)	2003-07-22	高熱伝導度炭素繊維
JPH0133572B2 (fr)	1989-07-13
GB2150924A (en)	1985-07-10	Carbon fibres
JP2894880B2 (ja)	1999-05-24	ピッチ系炭素繊維紡糸用口金
EP0387829A2 (fr)	1990-09-19	Fibres de carbone et non-tissés
JP2551979B2 (ja)	1996-11-06	ピッチの溶融紡糸方法
JP2711918B2 (ja)	1998-02-10	ピッチ系炭素繊維
JP2665118B2 (ja)	1997-10-22	細径ピッチ系炭素繊維の製造方法ならびに紡糸ノズル
JPH01306614A (ja)	1989-12-11	ポリエーテルイミド繊維の製造方法
JPH0319913A (ja)	1991-01-29	ポリエーテルケトン繊維の製造法
JP2744552B2 (ja)	1998-04-28	紡糸口金パック