BE902182A - Procede de production de sulfate de potassium et produit ainsi obtenu. - Google Patents
Procede de production de sulfate de potassium et produit ainsi obtenu.Info
- Publication number
- BE902182A BE902182A BE0/214838A BE214838A BE902182A BE 902182 A BE902182 A BE 902182A BE 0/214838 A BE0/214838 A BE 0/214838A BE 214838 A BE214838 A BE 214838A BE 902182 A BE902182 A BE 902182A
- Authority
- BE
- Belgium
- Prior art keywords
- potassium sulfate
- product
- producing potassium
- potassium
- crystallize
- Prior art date
Links
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 title abstract 4
- 229910052939 potassium sulfate Inorganic materials 0.000 title abstract 3
- 235000011151 potassium sulphates Nutrition 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 239000001103 potassium chloride Substances 0.000 abstract 1
- 235000011164 potassium chloride Nutrition 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/02—Preparation of sulfates from alkali metal salts and sulfuric acid or bisulfates; Preparation of bisulfates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D9/00—Nitrates of sodium, potassium or alkali metals in general
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D1/00—Fertilisers containing potassium
- C05D1/02—Manufacture from potassium chloride or sulfate or double or mixed salts thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Procédé de préparation de sulfate de potassium, comprenant notamment la mise en réaction de chlorure de potassium et l'acide sulfurique dans une solution aqueuse recyclée suivant essentiellement le rapport stoechiométrique requis pour produire du sulfate de potassium, l'évaporation de pratiquement la totalité de l'acide chlorhydrique produit, le refroidissement de la solution ainsi obtenue de manière à cristalliser un sel de sulfate de potassium.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/602,036 US4588573A (en) | 1983-09-27 | 1984-04-19 | Method for the production of potassium sulfate using sulfuric acid and potassium chloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE902182A true BE902182A (fr) | 1985-07-31 |
Family
ID=24409716
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE0/214838A BE902182A (fr) | 1984-04-19 | 1985-04-12 | Procede de production de sulfate de potassium et produit ainsi obtenu. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4588573A (fr) |
| BE (1) | BE902182A (fr) |
| CA (1) | CA1217028A (fr) |
| DD (1) | DD232252A5 (fr) |
| DE (1) | DE3507802A1 (fr) |
| ES (1) | ES542414A0 (fr) |
| FR (1) | FR2563205A1 (fr) |
| JO (1) | JO1390B1 (fr) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6299663B1 (en) | 1996-04-19 | 2001-10-09 | Airborne Industrial Minerals Inc. | Granulation method and apparatus therefor |
| US6331193B1 (en) | 1998-04-17 | 2001-12-18 | Airborne Industrial Minerals Inc. | Wet granulation method generating sulfur granules |
| US6454979B1 (en) | 1998-04-17 | 2002-09-24 | Airborne Industrial Minerals Inc. | Wet granulation method for generating granules |
| US6132484A (en) * | 1998-04-17 | 2000-10-17 | Airborne Industrial Minerals Inc. | Wet granulation method for generating fertilizer granules |
| US6293985B1 (en) | 1998-04-17 | 2001-09-25 | Airborne Industrial Minerals | Fertilizer granulation method |
| US6315976B1 (en) | 1998-06-16 | 2001-11-13 | Aristos Capital Corporation | Method of producing potassium sulfate |
| US6692716B1 (en) | 1998-10-13 | 2004-02-17 | Airborne Industrial Minerals, Inc. | Method of formulating alkali earth salts |
| US6106796A (en) * | 1998-10-13 | 2000-08-22 | Airborne Technologies Inc. | Method of ammonium sulfate purification |
| WO2000067550A1 (fr) | 1999-05-05 | 2000-11-16 | Airborne Industrial Minerals Inc. | Procede de granulation de compost |
| US6334990B1 (en) | 1999-10-21 | 2002-01-01 | Airborne Industrial Minerals Inc. | Formulation of potassium sulfate, sodium carbonate and sodium bicarbonate from potash brine |
| US6375824B1 (en) | 2001-01-16 | 2002-04-23 | Airborne Industrial Minerals Inc. | Process for producing potassium hydroxide and potassium sulfate from sodium sulfate |
| US6676917B2 (en) | 2001-02-16 | 2004-01-13 | Cabello-Fuentes Jose | Process for the production of hydrochloric acid and neutralized sulfates |
| WO2003074424A1 (fr) * | 2002-03-07 | 2003-09-12 | Visweswara Rao Abburi | Procede cyclique pour produire continuellement du sulfate de potassium et sulfate de potassium produit par celui-ci |
| EP2188211A1 (fr) * | 2007-07-25 | 2010-05-26 | F.P.C. Enterprise (2008) LTD | Procédé chimique de production de chlorure d'hydrogène et de fertilisants de sulfate de potassium composés sans chlorure ou d'autres sulfates métalliques |
| CA2737825A1 (fr) * | 2011-04-20 | 2012-10-20 | Carbon Solutions Incorporated | Conversion de gaz corrosif en engrais a base de sulfate ou de phosphate |
| CN103387243A (zh) * | 2012-05-12 | 2013-11-13 | 甘肃麦格理钾肥有限责任公司 | 盐酸母液法生产硫酸钾氨的方法 |
| JOP20170077B1 (ar) * | 2016-09-13 | 2021-08-17 | Veolia Water Tech Inc | طريقة لإنتاج كبريتات البوتاسيوم من كلوريد البوتاسيوم و حمض كبريتيك |
| CA2968257C (fr) * | 2017-05-24 | 2022-05-24 | Inotel Inc. | Fertilisant au potassium et magnesium |
| KR102378525B1 (ko) * | 2017-06-13 | 2022-03-23 | 재단법인 포항산업과학연구원 | 황산 칼륨의 제조 방법 |
| PL422437A1 (pl) * | 2017-08-02 | 2019-02-11 | Alwernia Spółka Akcyjna | Sposób otrzymywania kwaśnej soli siarczanu potasu o niskiej zawartości chlorków i kwasu solnego spożywczej jakości |
| CN111807386B (zh) * | 2020-07-24 | 2023-04-07 | 华融化学股份有限公司 | 一种试剂级硫酸钾的制备方法 |
| IT202000018238A1 (it) | 2020-07-28 | 2022-01-28 | Edale S R L | Processo di produzione di concimi a base di solfato di potassio |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB435772A (en) * | 1934-03-27 | 1935-09-27 | Henry Elhanan Zvi Raczkowski | Improvements in and relating to the production of syngenite and to the production ofpotassium sulphate from potassium chloride |
| FR787713A (fr) * | 1934-05-02 | 1935-09-27 | Ici Ltd | Perfectionnements à la fabrication du sulfate de potassium |
| US2689041A (en) * | 1952-03-18 | 1954-09-14 | Int Minerals & Chem Corp | Beneficiation of ores containing potassium chloride and magnesium sulfate |
| US2788257A (en) * | 1954-11-19 | 1957-04-09 | Minerals & Chemicals Corp | Crystallization process for recovering sylvite from sylvinite ore |
| FR1310550A (fr) * | 1961-09-12 | 1962-11-30 | Montedison Spa | Procédé pour la production de sulfate de potassium à partir de kaïnite |
| ES295016A1 (es) * | 1963-01-15 | 1964-07-01 | Montedison Spa | Un procedimiento para recuperar sulfato potasico de las aguas madres finales de elaboraciën de los minerales potasicos |
| US3402018A (en) * | 1967-02-14 | 1968-09-17 | Grace W R & Co | Removal of potassium and sodium sulfate from brines and bitterns |
| DE1902738B2 (de) * | 1969-01-21 | 1977-02-10 | Kali Und Salz Ag, 3500 Kassel | Verfahren zur herstellung von kaliumsulfat und/oder syngenit |
| SU558855A1 (ru) * | 1973-12-04 | 1977-05-25 | Предприятие П/Я А-7125 | Способ получени двойной соли сульфата кали -кальци |
| US3998935A (en) * | 1975-01-30 | 1976-12-21 | Pennzoil Company | Manufacture of potassium sulfate |
| SU806605A1 (ru) * | 1975-10-08 | 1981-02-23 | Всесоюзный Научно-Исследовательскийи Проектный Институт Галургии | Способ извлечени хлористогоКАли |
| US4045543A (en) * | 1975-11-12 | 1977-08-30 | Pennzoil Company | Production of potassium sulfate and hydrogen chloride |
| US4215100A (en) * | 1978-05-18 | 1980-07-29 | Antonova Nina V | Method of producing potassium sulfate |
| DE2950404C2 (de) * | 1978-12-25 | 1984-05-30 | Asahi Kasei Kogyo K.K., Osaka | Verfahren zur Herstellung von Kaliumsulfat |
| GB2068918B (en) * | 1980-01-09 | 1984-06-20 | Lozano J A F | Potassium sulphate and potassium sodium sulphate production |
-
1984
- 1984-04-19 US US06/602,036 patent/US4588573A/en not_active Expired - Fee Related
-
1985
- 1985-02-20 CA CA000474736A patent/CA1217028A/fr not_active Expired
- 1985-03-05 DE DE19853507802 patent/DE3507802A1/de not_active Withdrawn
- 1985-03-28 JO JO19851390A patent/JO1390B1/en active
- 1985-04-01 DD DD85274701A patent/DD232252A5/de unknown
- 1985-04-12 BE BE0/214838A patent/BE902182A/fr not_active IP Right Cessation
- 1985-04-17 FR FR8505793A patent/FR2563205A1/fr not_active Withdrawn
- 1985-04-19 ES ES542414A patent/ES542414A0/es active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JO1390B1 (en) | 1986-11-30 |
| CA1217028A (fr) | 1987-01-27 |
| US4588573A (en) | 1986-05-13 |
| DE3507802A1 (de) | 1985-10-31 |
| DD232252A5 (de) | 1986-01-22 |
| FR2563205A1 (fr) | 1985-10-25 |
| ES8603346A1 (es) | 1985-12-16 |
| ES542414A0 (es) | 1985-12-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RE | Patent lapsed |
Owner name: PRODECO INC. Effective date: 19880430 |