BE902193A - PROCESS FOR PRODUCING SINTERABLE LITHIUM ORTHOSILICATE (LI4SIO4) POWDER AND USE THEREOF. - Google Patents
PROCESS FOR PRODUCING SINTERABLE LITHIUM ORTHOSILICATE (LI4SIO4) POWDER AND USE THEREOF.Info
- Publication number
- BE902193A BE902193A BE1/11237A BE1011237A BE902193A BE 902193 A BE902193 A BE 902193A BE 1/11237 A BE1/11237 A BE 1/11237A BE 1011237 A BE1011237 A BE 1011237A BE 902193 A BE902193 A BE 902193A
- Authority
- BE
- Belgium
- Prior art keywords
- li4sio4
- powder
- lithium orthosilicate
- sinterable lithium
- suspension
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- YTZVWGRNMGHDJE-UHFFFAOYSA-N tetralithium;silicate Chemical compound [Li+].[Li+].[Li+].[Li+].[O-][Si]([O-])([O-])[O-] YTZVWGRNMGHDJE-UHFFFAOYSA-N 0.000 title 1
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 abstract 3
- 239000000725 suspension Substances 0.000 abstract 2
- 229910021486 amorphous silicon dioxide Inorganic materials 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 238000001694 spray drying Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B4/00—Hydrogen isotopes; Inorganic compounds thereof prepared by isotope exchange, e.g. NH3 + D2 → NH2D + HD
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/32—Alkali metal silicates
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21B—FUSION REACTORS
- G21B1/00—Thermonuclear fusion reactors
- G21B1/11—Details
- G21B1/13—First wall; Blanket; Divertor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E30/00—Energy generation of nuclear origin
- Y02E30/10—Nuclear fusion reactors
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- High Energy & Nuclear Physics (AREA)
- Plasma & Fusion (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Silicon Compounds (AREA)
Abstract
Procédé caractérisé par les étapes opérationnelles suivantes: a) préparer une solution aqueuse d'hydroxyde de lithium, b) introduire du SiO 2 amorphe dans la solution de l'étape a), avec formation d'une suspension et addition de H2O2 à cette dernière, c) sécher par atomisation la suspension de l'étape b) en un résidu sec pulvérulent, et d) chauffer le résidu sec de l'étape c), pour réaction et calcination, à une température de l'ordre de 500 à 1000 C.Process characterized by the following operational steps: a) preparing an aqueous solution of lithium hydroxide, b) introducing amorphous SiO 2 into the solution of step a), with the formation of a suspension and addition of H2O2 to the latter , c) spray-drying the suspension from step b) into a dry pulverulent residue, and d) heating the dry residue from step c), for reaction and calcination, at a temperature of the order of 500 to 1000 vs.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19843415326 DE3415326A1 (en) | 1984-04-25 | 1984-04-25 | METHOD FOR PRODUCING SINTERABLE POWDER FROM LITHIUM ORTHOSILICATE LI (DOWN ARROW) 4 (DOWN ARROW) SIO (DOWN ARROW) 4 (DOWN ARROW) AND THE USE THEREOF |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE902193A true BE902193A (en) | 1985-07-31 |
Family
ID=6234301
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE1/11237A BE902193A (en) | 1984-04-25 | 1985-04-15 | PROCESS FOR PRODUCING SINTERABLE LITHIUM ORTHOSILICATE (LI4SIO4) POWDER AND USE THEREOF. |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE902193A (en) |
| DE (1) | DE3415326A1 (en) |
| FR (1) | FR2568866B1 (en) |
| GB (1) | GB2159806B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6387845B1 (en) * | 1999-03-23 | 2002-05-14 | Kabushiki Kaisha Toshiba | Carbon dioxide gas absorbent containing lithium silicate |
| CN103159222B (en) * | 2011-12-09 | 2014-10-01 | 核工业西南物理研究院 | A kind of method for compacting lithium orthosilicate pellets for tritium propagation |
| CN111018557B (en) * | 2019-12-26 | 2022-04-29 | 广州赛隆增材制造有限责任公司 | A kind of preparation method of lithium orthosilicate spherical shell for tritium breeding |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1792078A1 (en) * | 1962-07-13 | 1971-10-14 | Exxon Research Engineering Co | Process for the preparation of lithium silicate and lithium sodium silicate solutions |
| FR1546127A (en) * | 1966-11-30 | 1968-11-15 | Henkel & Cie Gmbh | Process for preparing lithium silicate solutions |
| US3932140A (en) * | 1973-04-30 | 1976-01-13 | E. I. Du Pont De Nemours & Co. | Forming highly absorbent, low bulk density sodium silicate by contacting with H2 O2 and heating to about 45° to 60°C |
| US4011302A (en) * | 1975-06-26 | 1977-03-08 | E. I. Du Pont De Nemours And Company | Process for preparing highly absorbent, low bulk density sodium silicate |
| DE3121919A1 (en) * | 1980-06-24 | 1982-04-29 | Steirische Magnesit-Industrie AG, 1130 Wien | HYDROTHERMAL DIRECT SYNTHESIS OF ALKALISILICATES |
-
1984
- 1984-04-25 DE DE19843415326 patent/DE3415326A1/en active Granted
-
1985
- 1985-04-09 FR FR8505318A patent/FR2568866B1/en not_active Expired
- 1985-04-12 GB GB08509432A patent/GB2159806B/en not_active Expired
- 1985-04-15 BE BE1/11237A patent/BE902193A/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE3415326C2 (en) | 1988-10-06 |
| FR2568866A1 (en) | 1986-02-14 |
| GB8509432D0 (en) | 1985-06-19 |
| GB2159806A (en) | 1985-12-11 |
| DE3415326A1 (en) | 1985-10-31 |
| GB2159806B (en) | 1988-02-24 |
| FR2568866B1 (en) | 1987-01-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RE | Patent lapsed |
Owner name: KERNFORSCHUNGSZENTRUM KARLSRUHE G.M.B.H. Effective date: 19880430 |