BR0016239A - Método para purificação de silìcio de qualidade metalúrgica - Google Patents

Método para purificação de silìcio de qualidade metalúrgica

Info

Publication number
BR0016239A
BR0016239A BR0016239-6A BR0016239A BR0016239A BR 0016239 A BR0016239 A BR 0016239A BR 0016239 A BR0016239 A BR 0016239A BR 0016239 A BR0016239 A BR 0016239A
Authority
BR
Brazil
Prior art keywords
silicon
purification
calcium
molten
metallurgical grade
Prior art date
Application number
BR0016239-6A
Other languages
English (en)
Other versions
BR0016239B1 (pt
Inventor
Bruno Ceccaroli
Kenneth Friestad
Original Assignee
Elkem Materials
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elkem Materials filed Critical Elkem Materials
Publication of BR0016239A publication Critical patent/BR0016239A/pt
Publication of BR0016239B1 publication Critical patent/BR0016239B1/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • C01B33/037Purification
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10FINORGANIC SEMICONDUCTOR DEVICES SENSITIVE TO INFRARED RADIATION, LIGHT, ELECTROMAGNETIC RADIATION OF SHORTER WAVELENGTH OR CORPUSCULAR RADIATION
    • H10F71/00Manufacture or treatment of devices covered by this subclass
    • H10F71/121The active layers comprising only Group IV materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00Energy generation through renewable energy sources
    • Y02E10/50Photovoltaic [PV] energy
    • Y02E10/547Monocrystalline silicon PV cells
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

"MéTODO PARA PURIFICAçãO DE SILìCIO DE QUALIDADE METALúRGICA". A invenção se refere a um método para purificação de silício de qualidade metalúrgica onde um composto contendo cálcio é adicionado ao silício em fusão antes ou depois do silício ser vazado do forno. O silício é vertido e solidificado a uma velocidade de resfriamento relativamente alta e o silício solidificado é triturado e submetido a um processo de purificação que consiste em duas etapas de lixiviação. Na primeira etapa de lixiviação, o silício é tratado com uma solução aquosa de FeC1~ 3~ ou FeC1~ 3~ e HCI que causa desintegração do silício e na segunda etapa de lixiviação o silício é tratado com uma solução aquosa de UF ou HF/HNO~ 3~. O composto contendo cálcio é adicionado ao silício em fusão em uma quantidade necessária para prover entre 0,3 e 0,95% em peso de cálcio no silício em fusão e a relação em peso entre AI e Fe no silício em fusão é regulada a entre 0,5 e 2,0,por adição de alumínio ao silício em fusão.
BRPI0016239-6A 1999-12-08 2000-11-08 método para purificação de silìcio de qualidade metalúrgica. BR0016239B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NO19996022A NO313132B1 (no) 1999-12-08 1999-12-08 Fremgangsmåte for rensing av silisium
PCT/NO2000/000374 WO2001042136A1 (en) 1999-12-08 2000-11-08 Refining of metallurgical grade silicon

Publications (2)

Publication Number Publication Date
BR0016239A true BR0016239A (pt) 2002-08-27
BR0016239B1 BR0016239B1 (pt) 2009-08-11

Family

ID=19904078

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0016239-6A BR0016239B1 (pt) 1999-12-08 2000-11-08 método para purificação de silìcio de qualidade metalúrgica.

Country Status (12)

Country Link
US (1) US6861040B1 (pt)
EP (1) EP1254074B1 (pt)
JP (1) JP4035323B2 (pt)
CN (1) CN1231416C (pt)
AT (1) ATE277866T1 (pt)
AU (1) AU1560701A (pt)
BR (1) BR0016239B1 (pt)
CA (1) CA2393511C (pt)
DE (1) DE60014441T2 (pt)
ES (1) ES2223616T3 (pt)
NO (1) NO313132B1 (pt)
WO (1) WO2001042136A1 (pt)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4115432B2 (ja) * 2004-07-14 2008-07-09 シャープ株式会社 金属の精製方法
CN100579902C (zh) * 2007-07-06 2010-01-13 昆明理工大学 一种制备超冶金级硅的方法
ITMI20081085A1 (it) * 2008-06-16 2009-12-17 N E D Silicon S P A Metodo per la preparazione di silicio di grado metallurgico di elevata purezza.
WO2010148484A1 (en) * 2009-06-24 2010-12-29 The Governing Council Of The Universtiy Of Toronto Method of removal of impurities from silicon
DE102009034317A1 (de) 2009-07-23 2011-02-03 Q-Cells Se Verfahren zur Herstellung durchbruchsicherer p-Typ Solarzellen aus umg-Silizium
NO331026B1 (no) 2009-09-23 2011-09-12 Elkem Solar As Fremgangsmate for fremstilling av hoyrent silisium
DE102009046265A1 (de) * 2009-10-30 2011-05-19 Rheinisch-Westfälische Technische Hochschule Aachen Verfahren zur Aufarbeitung von Sägerückständen aus der Produktion von Silizium-Wafern
KR20130063501A (ko) 2010-05-20 2013-06-14 다우 코닝 코포레이션 알루미늄-규소 합금을 생성하기 위한 방법 및 시스템
CN102602935B (zh) * 2012-03-05 2014-03-12 矽明科技股份有限公司 一种高钙除磷的硅的清洗方法
TWI542544B (zh) 2012-06-25 2016-07-21 希利柯爾材料股份有限公司 純化矽之方法
EP2864252A1 (en) 2012-06-25 2015-04-29 Silicor Materials Inc. Method for purifying silicon
NO339608B1 (no) * 2013-09-09 2017-01-09 Elkem Solar As Multikrystallinske silisiumingoter, silisiummasterlegering, fremgangsmåte for å øke utbyttet av multikrystallinske silisiumingoter for solceller
WO2017096563A1 (zh) * 2015-12-09 2017-06-15 季国平 一种硅的工业提纯方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4200621A (en) * 1978-07-18 1980-04-29 Motorola, Inc. Sequential purification and crystal growth
IT1100218B (it) * 1978-11-09 1985-09-28 Montedison Spa Procedimento per la purificazione di silicio
US4312847A (en) * 1979-05-24 1982-01-26 Aluminum Company Of America Silicon purification system
DE2933164A1 (de) * 1979-08-16 1981-02-26 Consortium Elektrochem Ind Verfahren zum reinigen von rohsilicium
NO152551C (no) 1983-02-07 1985-10-16 Elkem As Fremgangsmaate til fremstilling av rent silisium.
US4612179A (en) * 1985-03-13 1986-09-16 Sri International Process for purification of solid silicon
US4798659A (en) * 1986-12-22 1989-01-17 Dow Corning Corporation Addition of calcium compounds to the carbothermic reduction of silica
RU2097320C1 (ru) 1993-11-01 1997-11-27 Институт металлургии Уральского отделения РАН Способ получения порошка кремния повышенной частоты

Also Published As

Publication number Publication date
CA2393511A1 (en) 2001-06-14
JP2003516295A (ja) 2003-05-13
WO2001042136A1 (en) 2001-06-14
JP4035323B2 (ja) 2008-01-23
ES2223616T3 (es) 2005-03-01
CN1409691A (zh) 2003-04-09
DE60014441D1 (de) 2004-11-04
AU1560701A (en) 2001-06-18
NO996022D0 (no) 1999-12-08
EP1254074A1 (en) 2002-11-06
NO313132B1 (no) 2002-08-19
NO996022L (no) 2001-06-11
CA2393511C (en) 2007-03-20
ATE277866T1 (de) 2004-10-15
EP1254074B1 (en) 2004-09-29
US6861040B1 (en) 2005-03-01
DE60014441T2 (de) 2005-01-20
BR0016239B1 (pt) 2009-08-11
CN1231416C (zh) 2005-12-14

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 08/11/2000, OBSERVADAS AS CONDICOES LEGAIS.

B25A Requested transfer of rights approved

Owner name: REC SOLAR NORWAY AS (NO)

B21A Patent or certificate of addition expired [chapter 21.1 patent gazette]

Free format text: PATENTE EXTINTA EM 08.11.2020