BR0103406A - Processo de produção de frutose cristalina de elevada pureza utilizando xarope com baixo teor de frutose originária de sacarose, e produto obtido - Google Patents
Processo de produção de frutose cristalina de elevada pureza utilizando xarope com baixo teor de frutose originária de sacarose, e produto obtidoInfo
- Publication number
- BR0103406A BR0103406A BR0103406-5A BR0103406A BR0103406A BR 0103406 A BR0103406 A BR 0103406A BR 0103406 A BR0103406 A BR 0103406A BR 0103406 A BR0103406 A BR 0103406A
- Authority
- BR
- Brazil
- Prior art keywords
- fructose
- syrup
- sucrose
- crystalline
- glucose
- Prior art date
Links
- 229930091371 Fructose Natural products 0.000 title abstract 12
- 239000005715 Fructose Substances 0.000 title abstract 12
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title abstract 12
- 238000000034 method Methods 0.000 title abstract 6
- 229930006000 Sucrose Natural products 0.000 title abstract 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title abstract 3
- 239000005720 sucrose Substances 0.000 title abstract 3
- 235000021433 fructose syrup Nutrition 0.000 title abstract 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract 3
- 239000008103 glucose Substances 0.000 abstract 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 239000000126 substance Substances 0.000 abstract 2
- 239000006188 syrup Substances 0.000 abstract 2
- 235000020357 syrup Nutrition 0.000 abstract 2
- 240000000111 Saccharum officinarum Species 0.000 abstract 1
- 235000007201 Saccharum officinarum Nutrition 0.000 abstract 1
- 238000005903 acid hydrolysis reaction Methods 0.000 abstract 1
- 238000005119 centrifugation Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000013375 chromatographic separation Methods 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 235000013305 food Nutrition 0.000 abstract 1
- 235000003599 food sweetener Nutrition 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 235000015097 nutrients Nutrition 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 239000003765 sweetening agent Substances 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/002—Evaporating or boiling sugar juice
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/02—Crystallisation; Crystallising apparatus
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/04—Separating crystals from mother liquor
- C13B30/06—Separating crystals from mother liquor by centrifugal force
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B40/00—Drying sugar
- C13B40/002—Drying sugar or syrup in bulk
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Saccharide Compounds (AREA)
- Jellies, Jams, And Syrups (AREA)
- Seasonings (AREA)
Abstract
"PROCESSO DE PRODUçãO DE FRUTOSE CRISTALINA DE ELEVADA PUREZA UTILIZANDO XAROPE COM BAIXO TEOR DE FRUTOSE ORIGINáRIA DE SACAROSE, E PRODUTO OBTIDO". A invenção refere-se a um processo de produção de frutose cristalina com elevada pureza química, a partir de sacarose de cana-de-açúcar, que se apresenta sob a forma de partículas microcristalinas com morfologia bem definida, típica do sistema cristalino ortorrómbico, as quais exibem uma estreita distribuição de tamanhos com diâmetro efetivo médio na faixa de 250 a 350 mícrons. A invenção tem também por objeto a proteção do produto, frutose cristalina, fabricado pelo processo conforme a invenção. O referido processo consta de uma etapa de conversão química da sacarose em frutose e glicose por meio de uma hidrólise ácida; de uma segunda etapa na qual é efetuada uma separação cromatográfica entre a frutose e a glicose, e é preparado, como carga de alimentação de um cristalizador, um xarope rico em frutose com uma concentração mínima de 92% p/p de sólidos e com um teor de frutose compreendido entre 84 e 90% p/p, bs; e de uma terceira e última etapa que consiste na cristalização da frutose em meio hidro-alcoólico, na recuperação dos seus cristais por centrifugação do magma, e na lavagem e secagem dos mesmos. A frutose cristalina produzida pelo processo de acordo com a invenção possui um grau de pureza superior a 99,50% p/p, bs, e apresenta uma higroscopicidade e um tempo de dissolução que lhe conferem um ótimo desempenho em suas aplicações no setor de adoçantes nutritivos naturais, na indústria de alimentos. o processo conforme a invenção também produz um xarope aquoso rico em frutose, com uma concentração de sólidos compreendida entre cerca de 60 e cerca de 70% p/p, com um teor de frutose compreendido entre 74 e 80% p/p, bs, e com um teor de glicose compreendido entre 18 e 24% p/p, bs.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BR0103406-5A BR0103406A (pt) | 2001-08-15 | 2001-08-15 | Processo de produção de frutose cristalina de elevada pureza utilizando xarope com baixo teor de frutose originária de sacarose, e produto obtido |
| US10/486,516 US7150794B2 (en) | 2001-08-15 | 2002-05-17 | Process for the production of crystalline fructose of high purity utilizing fructose syrup having a low content of fructose made from sucrose and product obtained |
| EP02794717A EP1417354A1 (en) | 2001-08-15 | 2002-05-17 | Process for the production of crystalline fructose of high purity utilizing fructose syrup having a low content of fructose made from sucrose and product obtained |
| JP2003520866A JP2004537326A (ja) | 2001-08-15 | 2002-05-17 | スクロースから作られた少量のフルクトースを含むフルクトースシロップを用いて高純度の結晶質フルクトースを製造する方法及び製品 |
| PCT/BR2002/000071 WO2003016577A1 (en) | 2001-08-15 | 2002-05-17 | Process for the production of crystalline fructose of high purity utilizing fructose syrup having a low content of fructose made from sucrose and product obtained |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BR0103406-5A BR0103406A (pt) | 2001-08-15 | 2001-08-15 | Processo de produção de frutose cristalina de elevada pureza utilizando xarope com baixo teor de frutose originária de sacarose, e produto obtido |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR0103406A true BR0103406A (pt) | 2004-05-04 |
Family
ID=3947848
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR0103406-5A BR0103406A (pt) | 2001-08-15 | 2001-08-15 | Processo de produção de frutose cristalina de elevada pureza utilizando xarope com baixo teor de frutose originária de sacarose, e produto obtido |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US7150794B2 (pt) |
| EP (1) | EP1417354A1 (pt) |
| JP (1) | JP2004537326A (pt) |
| BR (1) | BR0103406A (pt) |
| WO (1) | WO2003016577A1 (pt) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI115919B (fi) * | 2002-06-27 | 2005-08-15 | Danisco Sweeteners Oy | Menetelmä kiteytysinhibiittoreiden poistamiseksi monosakkaridisokeriliuoksista |
| WO2006125286A1 (en) * | 2005-05-24 | 2006-11-30 | Getec Guanabara Química Industrial S.A. | Process for the production of pyrogen-free anhydrous crystalline dextrose of high purity from sucrose |
| US20070122892A1 (en) * | 2005-11-30 | 2007-05-31 | Christian Andersson | Process for producing succinic acid from sucrose |
| FR2912036B1 (fr) * | 2007-02-01 | 2009-10-02 | Nutritis | Sirops de sucres de fruits a haute teneur en fructose,et procede de preparation. |
| KR100967093B1 (ko) | 2008-04-01 | 2010-07-01 | 주식회사 신동방씨피 | 고순도 무수결정과당의 제조방법 |
| EP2292803B1 (en) * | 2009-07-07 | 2013-02-13 | DuPont Nutrition Biosciences ApS | Separation process |
| CN106220696B (zh) | 2011-03-07 | 2019-12-24 | 株式会社林原 | 含有2-O-α-D-葡萄糖基-L-抗坏血酸无水结晶的粉末的制造方法 |
| NL2006447C2 (en) * | 2011-03-22 | 2012-09-25 | Univ Wageningen | Process for the crystallisation of a water-soluble compound. |
| CA2882522C (en) * | 2012-08-20 | 2019-03-19 | Naturalia Ingredients S.R.L. | Method of producing a sugar product from fruit |
| JP6250946B2 (ja) * | 2012-12-26 | 2017-12-20 | 松谷化学工業株式会社 | 甘味料組成物およびその製造方法並びにその用途 |
| WO2014154676A1 (de) * | 2013-03-27 | 2014-10-02 | Annikki Gmbh | Verfahren zur isomerisierung von glucose |
| CN104600846B (zh) * | 2015-02-07 | 2016-09-14 | 国家电网公司 | 一种变电站通信自动化设备线监测系统 |
| US10266861B2 (en) * | 2015-12-14 | 2019-04-23 | E. I. Du Pont De Nemours And Company | Production and composition of fructose syrup |
| EP3561080B1 (fr) | 2018-04-23 | 2023-08-02 | Novasep Process Solutions | Procede de fabrication de fructose a partir de glucose |
| EP3560570B1 (fr) * | 2018-04-23 | 2024-01-10 | Novasep Process Solutions | Procede de purification chromatographique de charges visqueuses |
| EP3560571B1 (fr) * | 2018-04-23 | 2023-12-13 | Novasep Process Solutions | Procede de purification de fructose |
| US11814691B2 (en) | 2018-07-30 | 2023-11-14 | Cargill, Incorporated | Semi-crystalline fructose in solid form and process for manufacturing the same |
| CN115058544A (zh) * | 2022-07-20 | 2022-09-16 | 北京斯坦励能源科技有限公司 | 一种以水果为原料制备结晶果糖的方法 |
| CN120054025B (zh) * | 2025-04-29 | 2025-07-08 | 山东福洋生物科技股份有限公司 | 一种果糖的结晶方法及其制备的结晶果糖 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3513023A (en) * | 1966-04-29 | 1970-05-19 | Boehringer Mannheim Gmbh | Process for the production of crystalline fructose |
| US3607392A (en) * | 1967-12-21 | 1971-09-21 | Boehringer Mannheim Gmbh | Process and apparatus for the recovery of crystalline fructose from methanolic solution |
| US3883365A (en) * | 1972-01-04 | 1975-05-13 | Suomen Sokeri Oy | PH adjustment in fructose crystallization for increased yield |
| JPS5239901B2 (pt) * | 1973-02-12 | 1977-10-07 | ||
| US4199374A (en) * | 1978-12-22 | 1980-04-22 | Chimicasa Gmbh | Process of preparing crystalline fructose from high fructose corn syrup |
| US4199373A (en) * | 1979-04-13 | 1980-04-22 | Chimicasa Gmbh | Process for the manufacture of crystalline fructose |
| US4405377A (en) * | 1982-02-10 | 1983-09-20 | Uop Inc. | Process for the separation of monosaccharides |
| US4517021A (en) * | 1983-10-28 | 1985-05-14 | A. E. Staley Manufacturing Company | Semi-crystalline fructose |
| US4643773A (en) * | 1984-03-09 | 1987-02-17 | A. E. Staley Manufacturing Company | Crystallization of fructose utilizing a mixture of alcohols |
| FR2582016B1 (fr) * | 1985-05-15 | 1987-09-18 | Roquette Freres | Procede et installation de production de fructose cristallise anhydre |
| US4888060A (en) * | 1985-06-21 | 1989-12-19 | A. E. Staley Manufacturing Company | Enrichment of fructose syrups |
| DE3528933A1 (de) * | 1985-08-13 | 1987-02-19 | Kernforschungsanlage Juelich | Fermentationsverfahren zur fructosegewinnung oder -anreicherung gegenueber glucose und dafuer brauchbare zymomonas mobilis mutanten |
| EP0613953B1 (en) | 1991-08-20 | 1999-02-03 | A.E. Staley Manufacturing Company | Fructose and dextrose containing liquid sweetener |
| US5656094A (en) * | 1987-02-02 | 1997-08-12 | A.E. Staley Manufacturing Company | Integrated process for producing crystalline fructose and a high-fructose, liquid phase sweetener |
| US5350456A (en) * | 1987-02-02 | 1994-09-27 | A. E. Staley Manufacturing Company | Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener |
| FI77693C (fi) * | 1987-06-03 | 1989-04-10 | Suomen Sokeri Oy | Foerfarande foer kristallisering av fruktos. |
| US5047088A (en) * | 1989-06-30 | 1991-09-10 | A. E. Staley Manufacturing Company | Method for crystallization of fructose |
-
2001
- 2001-08-15 BR BR0103406-5A patent/BR0103406A/pt not_active Application Discontinuation
-
2002
- 2002-05-17 US US10/486,516 patent/US7150794B2/en not_active Expired - Fee Related
- 2002-05-17 WO PCT/BR2002/000071 patent/WO2003016577A1/en not_active Ceased
- 2002-05-17 EP EP02794717A patent/EP1417354A1/en not_active Withdrawn
- 2002-05-17 JP JP2003520866A patent/JP2004537326A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US7150794B2 (en) | 2006-12-19 |
| JP2004537326A (ja) | 2004-12-16 |
| WO2003016577A1 (en) | 2003-02-27 |
| WO2003016577B1 (en) | 2003-08-07 |
| EP1417354A1 (en) | 2004-05-12 |
| US20040231662A1 (en) | 2004-11-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FBOS | Technical and formal requirements: other requirements |
Free format text: BASEADO NO ART. 216 1 DA LPI, APRESENTE COPIA AUTENTICADA DA PROCURACAO PARA QUE ESTA SEJA ACEITA. |
|
| B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: PEDIDO INDEFERIDO, DE ACORDO COM OS ARTIGOS 8O, 13 E 25 DA LPI 9.279/96. |
|
| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |
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| B15K | Others concerning applications: alteration of classification |
Ipc: C13B 30/00 (2011.01), C13B 20/14 (2011.01), C13B 3 |