BR0109079A - Processo para a remoção destilativa de parte ou da totalidade de um derivado de azepina (iii) - Google Patents

Processo para a remoção destilativa de parte ou da totalidade de um derivado de azepina (iii)

Info

Publication number
BR0109079A
BR0109079A BR0109079-8A BR0109079A BR0109079A BR 0109079 A BR0109079 A BR 0109079A BR 0109079 A BR0109079 A BR 0109079A BR 0109079 A BR0109079 A BR 0109079A
Authority
BR
Brazil
Prior art keywords
iii
azepine
derivative
distilling
azepine derivative
Prior art date
Application number
BR0109079-8A
Other languages
English (en)
Inventor
Hermann Luyken
Frank Ohlbach
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of BR0109079A publication Critical patent/BR0109079A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/86—Separation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/04—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with only hydrogen atoms, halogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/12—Nitrogen atoms not forming part of a nitro radical
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/90—Particular type of heating

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

"PROCESSO PARA A REMOçãO DESTILATIVA DE PARTE OU DA TOTALIDADE DE UM DERIVADO DE AZEPINA (III)". A invenção refere-se a um método para a separação por destilação de uma porção de ou da totalidade de um derivado de azepina (III), que é selecionado do grupo consistindo de amino-hexilideno-imina, tetra-hidro-azepina, hexil-hexa-hidro-azepina e amino-hexil-hexa-hidro-azepina de uma mistura (II) contendo um derivado de azepina (III) e uma amina (I), caracterizado pelo fato de que a destilação é conduzida com uma máxima temperatura de fundo de 150<198>C.
BR0109079-8A 2000-03-08 2001-03-06 Processo para a remoção destilativa de parte ou da totalidade de um derivado de azepina (iii) BR0109079A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10010825A DE10010825A1 (de) 2000-03-08 2000-03-08 Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat
PCT/EP2001/002494 WO2001066514A1 (de) 2000-03-08 2001-03-06 Verfahren zur abtrennung eines azepin-derivats aus einer mischung enthaltend ein amin und ein azepin-derivat

Publications (1)

Publication Number Publication Date
BR0109079A true BR0109079A (pt) 2003-06-03

Family

ID=7633667

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0109079-8A BR0109079A (pt) 2000-03-08 2001-03-06 Processo para a remoção destilativa de parte ou da totalidade de um derivado de azepina (iii)

Country Status (14)

Country Link
US (1) US7147757B2 (pt)
EP (1) EP1261580B1 (pt)
JP (1) JP2003525925A (pt)
KR (1) KR20020091118A (pt)
CN (1) CN1234685C (pt)
AR (1) AR029486A1 (pt)
AU (1) AU2001256194A1 (pt)
BR (1) BR0109079A (pt)
CA (1) CA2402236C (pt)
DE (1) DE10010825A1 (pt)
IL (1) IL151358A0 (pt)
MX (1) MXPA02008168A (pt)
TW (1) TW574211B (pt)
WO (1) WO2001066514A1 (pt)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7060819B2 (en) * 2003-09-15 2006-06-13 Invista North America S.A.R.L. Process for producing hexamethylenediamine and aminocapronitrile from adiponitrile, wherein the hexamethylenediamine contains less than 100 ppm tetrahydroazepine
US7094528B2 (en) * 2004-06-30 2006-08-22 Kimberly-Clark Worldwide, Inc. Magnetic enzyme detection techniques
US7468119B2 (en) * 2004-09-10 2008-12-23 Invista North America S.A.R.L. Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
US7208632B2 (en) * 2004-09-10 2007-04-24 Invista North America S.A R.L. Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
FR2922207B1 (fr) * 2007-10-11 2009-12-04 Rhodia Operations Procede de purification d'hexamethylene diamine
US8884064B2 (en) 2010-12-29 2014-11-11 Basf Se Method of separating off magnetizable catalyst particles by means of magnetic filters
KR20130132513A (ko) 2010-12-29 2013-12-04 바스프 에스이 자기 필터들을 이용하여 자화가능한 촉매 입자들을 분리하는 방법
US10532257B2 (en) 2014-08-26 2020-01-14 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US9669270B2 (en) 2014-08-26 2017-06-06 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US12121782B2 (en) 2014-08-26 2024-10-22 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US11697050B2 (en) 2014-08-26 2023-07-11 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US11000742B2 (en) 2014-08-26 2021-05-11 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US12179072B2 (en) 2014-08-26 2024-12-31 Parsons Extreme Golf, Llc Golf club heads and methods to manufacture golf club heads
US11617925B2 (en) 2019-03-11 2023-04-04 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US12290725B2 (en) 2017-01-10 2025-05-06 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US11484756B2 (en) 2017-01-10 2022-11-01 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US11654338B2 (en) 2017-01-10 2023-05-23 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads
US11839798B2 (en) 2019-03-11 2023-12-12 Parsons Xtreme Golf, LLC Golf club heads and methods to manufacture golf club heads

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2208598A (en) * 1938-09-24 1940-07-23 Du Pont Aliphatic amino-nitriles and process of producing them
US2762835A (en) * 1953-03-12 1956-09-11 Celanese Corp Preparation of amino nitriles
GB1238351A (pt) 1968-01-17 1971-07-07
HU171166B (hu) * 1975-07-15 1977-11-28 Richter Gedeon Vegyeszet Sposob poluchenija novykh ehpoksi-androstanov
GB1490310A (en) * 1975-11-19 1977-11-02 Texaco Belgium Nv Sa Production of caprolactam
US5192399A (en) * 1991-01-30 1993-03-09 E. I. Du Pont De Nemours And Company Purification of aminonitriles or diamines
US5133838A (en) * 1991-02-28 1992-07-28 E. I. Du Pont De Nemours And Company Purification of 6-aminocapronitrile
DE4446893A1 (de) 1994-12-27 1996-07-04 Basf Ag Verfahren zur Herstellung von aliphatischen alpha,omega-Aminonitrilen
DE19500222A1 (de) * 1995-01-05 1996-07-11 Basf Ag Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
US5717090A (en) * 1995-01-05 1998-02-10 Basf Aktiengesellschaft Simultaneous preparation of caprolactam and hexamethylenediamine
DE19636766A1 (de) * 1996-09-10 1998-03-12 Basf Ag Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin
DE19646436A1 (de) 1996-11-11 1998-05-14 Basf Ag Verfahren zur Herstellung von aliphatischen, alpha,omega-Aminonitrilen
DE19636768A1 (de) 1996-09-10 1998-03-12 Basf Ag Für die Herstellung von aliphatischen alpha, omega-Aminonitrilen durch partielle Hydrierung von aliphatischen Dinitrilen geeignete Katalysatoren
DE19704614A1 (de) * 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin
DE19704620A1 (de) * 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronitril aus Mischungen, die 6-Aminocapronitril und ein Imin enthalten
DE19812427A1 (de) 1998-03-20 1999-09-23 Basf Ag Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat
DE19839338A1 (de) * 1998-08-28 2000-03-02 Basf Ag Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin
US5961788A (en) * 1998-10-09 1999-10-05 E. I. Du Pont De Nemours And Company Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine
JP2004516308A (ja) * 2000-12-23 2004-06-03 デグサ アクチエンゲゼルシャフト ニトリルおよびイミンの水素化により第一級および第二級アミンを製造する方法

Also Published As

Publication number Publication date
CA2402236A1 (en) 2001-09-13
CN1416418A (zh) 2003-05-07
JP2003525925A (ja) 2003-09-02
WO2001066514A1 (de) 2001-09-13
EP1261580A1 (de) 2002-12-04
TW574211B (en) 2004-02-01
US20030023083A1 (en) 2003-01-30
US7147757B2 (en) 2006-12-12
AR029486A1 (es) 2003-07-02
EP1261580B1 (de) 2014-11-19
CN1234685C (zh) 2006-01-04
MXPA02008168A (es) 2002-11-29
AU2001256194A1 (en) 2001-09-17
DE10010825A1 (de) 2001-09-13
IL151358A0 (en) 2003-04-10
CA2402236C (en) 2009-11-17
KR20020091118A (ko) 2002-12-05

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Legal Events

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B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

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B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE AO DESPACHO 8.6 DA RPI 2016 DE 25/08/2009