BR0112089A - Processo para a preparação de granulado de fenotiazina com propriedades aperfeiçoadas - Google Patents
Processo para a preparação de granulado de fenotiazina com propriedades aperfeiçoadasInfo
- Publication number
- BR0112089A BR0112089A BR0112089-1A BR0112089A BR0112089A BR 0112089 A BR0112089 A BR 0112089A BR 0112089 A BR0112089 A BR 0112089A BR 0112089 A BR0112089 A BR 0112089A
- Authority
- BR
- Brazil
- Prior art keywords
- phenothiazine
- liquid
- preparation
- improved properties
- range
- Prior art date
Links
- WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 title abstract 7
- 229950000688 phenothiazine Drugs 0.000 title abstract 7
- 239000008187 granular material Substances 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000007788 liquid Substances 0.000 abstract 4
- 239000002826 coolant Substances 0.000 abstract 1
- 238000009826 distribution Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000008188 pellet Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M135/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium
- C10M135/32—Heterocyclic sulfur, selenium or tellurium compounds
- C10M135/36—Heterocyclic sulfur, selenium or tellurium compounds the ring containing sulfur and carbon with nitrogen or oxygen
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/84—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms six-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,4
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/54—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with at least one nitrogen and one sulfur as the ring hetero atoms, e.g. sulthiame
- A61K31/5415—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with at least one nitrogen and one sulfur as the ring hetero atoms, e.g. sulthiame ortho- or peri-condensed with carbocyclic ring systems, e.g. phenothiazine, chlorpromazine, piroxicam
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
- C07B63/04—Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D279/00—Heterocyclic compounds containing six-membered rings having one nitrogen atom and one sulfur atom as the only ring hetero atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Plant Pathology (AREA)
- Epidemiology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicinal Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Nitrogen- Or Sulfur-Containing Heterocyclic Ring Compounds With Rings Of Six Or More Members (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Polymerisation Methods In General (AREA)
- Glanulating (AREA)
Abstract
"PROCESSO PARA A PREPARAçãO DE GRANULADO DE FENOTIAZINA COM PROPRIEDADES APERFEIçOADAS". Processo para a preparação de granulado de fenotiazina com estreita distribuição de tamanho de partícula, sendo que a fenotiazina com pureza de pelo menos 98% em forma líquida é prensada por um dispositivo dotado de perfurações e sobre a fenotiazina líquida é aplicada uma freq³ência e a fenotiazina líquida que passa pelas perfurações entra em um meio de resfriamento com uma temperatura na faixa de -196 até +120<198>C, de modo que as gotas de líquido de fenotiazina assim obtidas são levadas até uma temperatura inferior à temperatura de fusão e estas são eventualmente solidificadas em uma outra zona de pós-resfriamento. Frações de grão fino ou frações de grãos grossos eventualmente formadas podem ser eliminados a seguir por métodos adequados. A densidade aparente do granulado de fenotiazina obtido situa-se na faixa de 720 até 780 kg/m^ 3^.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10032137A DE10032137B4 (de) | 2000-07-01 | 2000-07-01 | Verfahren zur Herstellung von Phenothiazin-Granulat mit verbesserten Eigenschaften |
| PCT/EP2001/002681 WO2002002543A1 (de) | 2000-07-01 | 2001-03-09 | Verfahren zur herstellung von phenothiazin-granulat mit verbesserten eigenschaften |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR0112089A true BR0112089A (pt) | 2003-05-06 |
| BR0112089B1 BR0112089B1 (pt) | 2012-05-29 |
Family
ID=7647511
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0112089-1A BR0112089B1 (pt) | 2000-07-01 | 2001-03-09 | processo para a preparação de granulado de fenotiazina com estreita distribuição de tamanho de partìcula, granulados de fenotiazina com estreita distribuição de tamanho de partìculas e uso dos mesmos. |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US6983612B2 (pt) |
| EP (1) | EP1299366B1 (pt) |
| JP (1) | JP2004502683A (pt) |
| BR (1) | BR0112089B1 (pt) |
| CZ (1) | CZ20024138A3 (pt) |
| DE (2) | DE10032137B4 (pt) |
| HU (1) | HUP0300707A2 (pt) |
| MX (1) | MX233652B (pt) |
| WO (1) | WO2002002543A1 (pt) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6284279B1 (en) | 1999-12-03 | 2001-09-04 | Avecia, Inc. | Phenothiazine in prill form and method for making the same |
| DE10032137B4 (de) * | 2000-07-01 | 2009-04-02 | Allessachemie Gmbh | Verfahren zur Herstellung von Phenothiazin-Granulat mit verbesserten Eigenschaften |
| US20060216319A1 (en) * | 2005-03-01 | 2006-09-28 | Chapple Andrew C | Bioactive chemicals with increased activity and methods for making same |
| JP2008188477A (ja) * | 2005-06-23 | 2008-08-21 | Seiko Kagaku Kk | 粒状化学物質の製造方法 |
| CN101234315B (zh) * | 2008-03-10 | 2013-01-09 | 泰兴市富安化工有限公司 | 中空颗粒状吩噻嗪物质及其制备方法 |
| DE102017211435A1 (de) * | 2017-07-05 | 2019-01-10 | Evonik Röhm Gmbh | Verfahren zum kontinuierlichen Lösen eines Feststoffes in einem Reaktionsmedium |
| CN112312983B (zh) * | 2018-05-31 | 2023-02-28 | 陶氏环球技术有限责任公司 | 用于聚合物溶液脱挥发的分配器和方法 |
Family Cites Families (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US749617A (en) * | 1904-01-12 | Road-making machine | ||
| US2415363A (en) * | 1947-02-04 | Refining of phenothiazine | ||
| US3160630A (en) * | 1964-12-08 | Amount of acetone in ccs | ||
| US3235453A (en) | 1962-01-09 | 1966-02-15 | Donald E Vierling | Phenothiazine composition and process for preparing same |
| US3169868A (en) | 1962-04-16 | 1965-02-16 | Eastman Kodak Co | Light sensitive photoresist composition |
| US3607993A (en) | 1969-05-20 | 1971-09-21 | Malcolm H Tuttle | Method of prilling |
| US3684607A (en) | 1970-03-24 | 1972-08-15 | Cecil Edward Morris | Manufacture of collapsible packaging tubes |
| US3686607A (en) * | 1971-02-05 | 1972-08-22 | Whitakercable Corp | High frequency shield for spark plug boot having suppression coil therein |
| US3912727A (en) | 1972-11-22 | 1975-10-14 | Grace W R & Co | Preparation of phenothiazines |
| GB1493612A (en) | 1974-07-06 | 1977-11-30 | Fisons Ltd | Prilling |
| US4021552A (en) | 1975-06-27 | 1977-05-03 | A. H. Robins Company, Incorporated | 10-[ω-(BENZOYLPIPERIDINYL)ALKYL]PHENOTHIAZINES |
| JPS5756306A (en) * | 1980-08-11 | 1982-04-03 | Mitsubishi Gas Chem Co Inc | Manufacture of sodium percarbonate with superior wear resistance |
| JPS5742511A (en) * | 1980-08-27 | 1982-03-10 | Mitsubishi Gas Chem Co Inc | Production of sodium percarbonate with improved wearability |
| DE3127750A1 (de) | 1981-07-14 | 1983-02-03 | Bayer Ag, 5090 Leverkusen | Stabilisatorhaltige reaktivkomponenten fuer pu-schaumstoffe, neue stabilisatoren und ein verfahren zur herstellung der stabilisatoren |
| JPS58124528A (ja) * | 1982-01-21 | 1983-07-25 | Ise Kagaku Kogyo Kk | 昇華性物質の球状化物、その製法及び製造装置 |
| JPS62183846A (ja) * | 1986-02-07 | 1987-08-12 | Toyo Eng Corp | 造粒方法 |
| US4785095A (en) | 1986-09-16 | 1988-11-15 | The Lubrizol Corporation | N-substituted thio alkyl phenothiazines |
| US4793783A (en) | 1987-01-20 | 1988-12-27 | The Dow Chemical Company | Apparatus for producing prills |
| DE3701738A1 (de) | 1987-01-22 | 1988-08-04 | Bayer Ag | Neue stabilisatoren und deren verwendung zur herstellung stabilisierter polyamide und kautschukmaterialien |
| US5024774A (en) | 1987-06-09 | 1991-06-18 | The Lubrizol Corporation | Nitrogen containing anti-oxidant compositions |
| US5006284A (en) | 1989-06-14 | 1991-04-09 | Ciba-Geigy Corporation | Granules of alkyl esters containing hydroxyphenyl groups |
| FR2652084B1 (fr) | 1989-09-21 | 1991-10-31 | Rhone Poulenc Sante | Nouveaux derives de la phenothiazine, leur preparation et les compositions pharmaceutiques qui les contiennent. |
| DE4022648C2 (de) * | 1990-07-17 | 1994-01-27 | Nukem Gmbh | Verfahren und Vorrichtung zur Herstellung von kugelförmigen Teilchen aus flüssiger Phase |
| IT1244742B (it) | 1991-02-14 | 1994-08-08 | Zambon Spa | Processo per la funzionalizzazione diretta e regioselettiva in posizione 2 della fenotiazina |
| JPH05309252A (ja) * | 1992-05-08 | 1993-11-22 | Osaka Yogyo Kk | 真球度の高い球状粒子の製造方法 |
| DE4338212C2 (de) | 1993-11-10 | 1996-01-18 | Nukem Gmbh | Verfahren und Vorrichtung zur Herstellung von aus Kunststoff bestehenden Partikeln |
| NL9400618A (nl) | 1994-04-18 | 1995-12-01 | Goudsche Machinefabriek Bv | Inrichting voor het koelen en verwerken van een gesmolten produkt tot een granulaatprodukt. |
| US5451337A (en) | 1994-05-31 | 1995-09-19 | The Procter & Gamble Co. | Dye transfer inhibition system containing a peroxidase/accelerator system |
| NL1007904C2 (nl) * | 1997-12-24 | 1999-06-25 | Goudsche Machinefabriek Bv | Werkwijze en inrichting voor het vormen van granulaat uit een smelt van chemische producten. |
| US6284279B1 (en) * | 1999-12-03 | 2001-09-04 | Avecia, Inc. | Phenothiazine in prill form and method for making the same |
| DE10032137B4 (de) * | 2000-07-01 | 2009-04-02 | Allessachemie Gmbh | Verfahren zur Herstellung von Phenothiazin-Granulat mit verbesserten Eigenschaften |
-
2000
- 2000-07-01 DE DE10032137A patent/DE10032137B4/de not_active Expired - Lifetime
-
2001
- 2001-03-09 CZ CZ20024138A patent/CZ20024138A3/cs unknown
- 2001-03-09 US US10/312,019 patent/US6983612B2/en not_active Expired - Lifetime
- 2001-03-09 BR BRPI0112089-1A patent/BR0112089B1/pt not_active IP Right Cessation
- 2001-03-09 EP EP01915324A patent/EP1299366B1/de not_active Expired - Lifetime
- 2001-03-09 DE DE50109706T patent/DE50109706D1/de not_active Expired - Lifetime
- 2001-03-09 JP JP2002507797A patent/JP2004502683A/ja active Pending
- 2001-03-09 HU HU0300707A patent/HUP0300707A2/hu unknown
- 2001-03-09 WO PCT/EP2001/002681 patent/WO2002002543A1/de not_active Ceased
- 2001-03-09 MX MXPA03000077 patent/MX233652B/es active IP Right Grant
-
2006
- 2006-01-03 US US11/324,746 patent/US20060166841A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| HUP0300707A2 (en) | 2003-07-28 |
| EP1299366B1 (de) | 2006-05-03 |
| US6983612B2 (en) | 2006-01-10 |
| JP2004502683A (ja) | 2004-01-29 |
| WO2002002543A1 (de) | 2002-01-10 |
| DE10032137A1 (de) | 2001-08-23 |
| BR0112089B1 (pt) | 2012-05-29 |
| US20060166841A1 (en) | 2006-07-27 |
| DE10032137B4 (de) | 2009-04-02 |
| MX233652B (es) | 2006-01-10 |
| MXPA03000077A (es) | 2003-07-14 |
| DE50109706D1 (de) | 2006-06-08 |
| EP1299366A1 (de) | 2003-04-09 |
| CZ20024138A3 (cs) | 2003-04-16 |
| US20040094749A1 (en) | 2004-05-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B15K | Others concerning applications: alteration of classification |
Free format text: PARA:INT.CI. B01J 2/18, C07D 279/20, C09K 15/30 Ipc: B01J 2/18 (2011.01), C07D 279/20 (2011.01), C09K 1 |
|
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 29/05/2012, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B21A | Patent or certificate of addition expired [chapter 21.1 patent gazette] |
Free format text: PATENTE EXTINTA EM 29.05.2022 |