BR0214543A - Processo para isolar trimetilolpropano a partir de uma mistura de reação - Google Patents

Processo para isolar trimetilolpropano a partir de uma mistura de reação

Info

Publication number
BR0214543A
BR0214543A BR0214543-0A BR0214543A BR0214543A BR 0214543 A BR0214543 A BR 0214543A BR 0214543 A BR0214543 A BR 0214543A BR 0214543 A BR0214543 A BR 0214543A
Authority
BR
Brazil
Prior art keywords
trimethylolpropane
reaction mixture
isolating
column
mixture
Prior art date
Application number
BR0214543-0A
Other languages
English (en)
Other versions
BR0214543B1 (pt
Inventor
Tilman Sirch
Gerd Kaibel
Alexander Wartini
Matthias Dernbach
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7708393&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BR0214543(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Ag filed Critical Basf Ag
Publication of BR0214543A publication Critical patent/BR0214543A/pt
Publication of BR0214543B1 publication Critical patent/BR0214543B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/22—Trihydroxylic alcohols, e.g. glycerol

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Steroid Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

"PROCESSO PARA ISOLAR TRIMETILOLPROPANO A PARTIR DE UMA MISTURA DE REAçãO". O trimetilolpropano é isolado a partir de uma mistura de reação, obtida pela reação de n-butiraldeído com formaldeído na presença de uma base e hidrogenação opcional da mistura obtida. A mistura é destilada usando uma coluna de separação ou uma coluna de destilação com uma pré coluna ou uma coluna de destilação com uma pós coluna. O método é caracterizado por um custo de investimento e energia baixos e a formação reduzida de subprodutos de alta ebulição.
BRPI0214543-0A 2001-12-07 2002-12-06 processo para isolar trimetilolpropano a partir de uma mistura de reaÇço. BR0214543B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10160180A DE10160180A1 (de) 2001-12-07 2001-12-07 Verfahren zur Isolierung von Trimethylolpropan aus einem Reaktionsgemisch
PCT/EP2002/013882 WO2003048093A2 (de) 2001-12-07 2002-12-06 Verfahren zur isolierung von trimethylolpropan aus einem reaktionsgemisch

Publications (2)

Publication Number Publication Date
BR0214543A true BR0214543A (pt) 2004-11-03
BR0214543B1 BR0214543B1 (pt) 2013-04-16

Family

ID=7708393

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0214543-0A BR0214543B1 (pt) 2001-12-07 2002-12-06 processo para isolar trimetilolpropano a partir de uma mistura de reaÇço.

Country Status (12)

Country Link
US (1) US7112707B2 (pt)
EP (1) EP1456159B1 (pt)
JP (1) JP3923472B2 (pt)
KR (1) KR100884121B1 (pt)
CN (1) CN1257141C (pt)
AT (1) ATE334957T1 (pt)
AU (1) AU2002358636A1 (pt)
BR (1) BR0214543B1 (pt)
DE (2) DE10160180A1 (pt)
MX (1) MXPA04004920A (pt)
MY (1) MY128842A (pt)
WO (1) WO2003048093A2 (pt)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010066674A2 (de) * 2008-12-09 2010-06-17 Basf Se Verfahren zur herstellung von polymethylolen
MY153850A (en) * 2008-12-09 2015-03-31 Basf Se Method for purifying crude polymethylols
WO2010079187A1 (de) * 2009-01-12 2010-07-15 Basf Se Verfahren zur herstellung von polymethylolen
DE102010033844B4 (de) 2010-08-11 2013-01-03 Oxea Gmbh Verfahren zur Gewinnung von Di-Trimethylolpropan und mit Trimethylolpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung
DE102010042934A1 (de) * 2010-10-26 2012-04-26 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat
DE102010042936A1 (de) * 2010-10-26 2012-04-26 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat
KR101530102B1 (ko) * 2010-12-29 2015-06-18 주식회사 엘지화학 네오펜틸글리콜 정제를 위한 분리벽형 증류탑 및 이를 이용한 정제방법
ES2617733T3 (es) * 2012-09-28 2017-06-19 Dow Global Technologies Llc Procedimiento para la producción de ésteres de glicol de alta pureza
CN104853840A (zh) * 2013-01-16 2015-08-19 Lg化学株式会社 烷醇的制备装置
CN106861353A (zh) * 2015-12-14 2017-06-20 财团法人工业技术研究院 分离装置
KR102224268B1 (ko) * 2016-10-31 2021-03-08 주식회사 엘지화학 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
KR102224267B1 (ko) * 2016-10-31 2021-03-08 주식회사 엘지화학 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
KR102224243B1 (ko) * 2016-10-31 2021-03-08 주식회사 엘지화학 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
US10913700B2 (en) 2018-02-01 2021-02-09 Lg Chem, Ltd. Method for producing dimethylolbutanal and distillation apparatus for producing same
US20250115537A1 (en) 2022-01-19 2025-04-10 Exxonmobil Chemical Patents Inc. Compositions Containing Tri-Cyclopentadiene and Processes for Making Same
WO2025244981A1 (en) 2024-05-20 2025-11-27 ExxonMobil Technology and Engineering Company Processes for making exo-dicyclopentadiene and tricyclopentadiene

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2471134A (en) * 1946-07-17 1949-05-24 Standard Oil Dev Co Fractionation apparatus
DE3302525A1 (de) * 1983-01-26 1984-07-26 Basf Ag, 6700 Ludwigshafen Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes
DE3340791A1 (de) * 1983-11-11 1985-05-23 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von trimethylolalkanen aus alkanalen und formaldehyd
GB2303511A (en) * 1995-07-19 1997-02-19 Univ Manchester Compensating for backscattered light
US5767922A (en) * 1996-04-05 1998-06-16 Cornell Research Foundation, Inc. Apparatus and process for detecting scene breaks in a sequence of video frames
DE19653093A1 (de) * 1996-12-20 1998-06-25 Basf Ag Verfahren zur Herstellung von Polyalkoholen
JP4284477B2 (ja) * 1998-12-25 2009-06-24 三菱瓦斯化学株式会社 高純度トリメチロールプロパンの製造法
US6778697B1 (en) * 1999-02-05 2004-08-17 Samsung Electronics Co., Ltd. Color image processing method and apparatus thereof
US6389417B1 (en) * 1999-06-29 2002-05-14 Samsung Electronics Co., Ltd. Method and apparatus for searching a digital image
DE19963435A1 (de) * 1999-12-28 2001-07-05 Basf Ag Verfahren zur Reinigung von durch Hydrierung hergestelltem Trimethylolpropan durch kontinuierliche Destillation

Also Published As

Publication number Publication date
JP3923472B2 (ja) 2007-05-30
DE50207749D1 (de) 2006-09-14
ATE334957T1 (de) 2006-08-15
BR0214543B1 (pt) 2013-04-16
CN1257141C (zh) 2006-05-24
KR100884121B1 (ko) 2009-02-17
DE10160180A1 (de) 2003-06-18
AU2002358636A1 (en) 2003-06-17
WO2003048093A2 (de) 2003-06-12
US20040267055A1 (en) 2004-12-30
JP2005511674A (ja) 2005-04-28
MY128842A (en) 2007-02-28
EP1456159B1 (de) 2006-08-02
WO2003048093A3 (de) 2004-01-15
US7112707B2 (en) 2006-09-26
EP1456159A2 (de) 2004-09-15
CN1599707A (zh) 2005-03-23
MXPA04004920A (es) 2004-08-11
KR20050044718A (ko) 2005-05-12

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 16/04/2013, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 16A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2494 DE 23-10-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.