BR112012018953A2 - extração líquida / líquido - Google Patents
extração líquida / líquidoInfo
- Publication number
- BR112012018953A2 BR112012018953A2 BR112012018953A BR112012018953A BR112012018953A2 BR 112012018953 A2 BR112012018953 A2 BR 112012018953A2 BR 112012018953 A BR112012018953 A BR 112012018953A BR 112012018953 A BR112012018953 A BR 112012018953A BR 112012018953 A2 BR112012018953 A2 BR 112012018953A2
- Authority
- BR
- Brazil
- Prior art keywords
- liquid
- notably
- oils
- chosen
- vegetable
- Prior art date
Links
- 239000007788 liquid Substances 0.000 title abstract 12
- 238000000605 extraction Methods 0.000 title abstract 6
- 239000003921 oil Substances 0.000 abstract 4
- 235000019198 oils Nutrition 0.000 abstract 4
- 239000002904 solvent Substances 0.000 abstract 4
- 238000000034 method Methods 0.000 abstract 3
- 235000015112 vegetable and seed oil Nutrition 0.000 abstract 3
- 239000008158 vegetable oil Substances 0.000 abstract 3
- GETTZEONDQJALK-UHFFFAOYSA-N (trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=CC=C1 GETTZEONDQJALK-UHFFFAOYSA-N 0.000 abstract 2
- 235000014121 butter Nutrition 0.000 abstract 2
- ZQBFAOFFOQMSGJ-UHFFFAOYSA-N hexafluorobenzene Chemical compound FC1=C(F)C(F)=C(F)C(F)=C1F ZQBFAOFFOQMSGJ-UHFFFAOYSA-N 0.000 abstract 2
- 244000005700 microbiome Species 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000007670 refining Methods 0.000 abstract 2
- NUMQCACRALPSHD-UHFFFAOYSA-N tert-butyl ethyl ether Chemical compound CCOC(C)(C)C NUMQCACRALPSHD-UHFFFAOYSA-N 0.000 abstract 2
- JWUJQDFVADABEY-UHFFFAOYSA-N 2-methyltetrahydrofuran Chemical compound CC1CCCO1 JWUJQDFVADABEY-UHFFFAOYSA-N 0.000 abstract 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000003849 aromatic solvent Substances 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 238000004332 deodorization Methods 0.000 abstract 1
- AQEFLFZSWDEAIP-UHFFFAOYSA-N di-tert-butyl ether Chemical class CC(C)(C)OC(C)(C)C AQEFLFZSWDEAIP-UHFFFAOYSA-N 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 1
- 239000004519 grease Substances 0.000 abstract 1
- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 abstract 1
- 229940073561 hexamethyldisiloxane Drugs 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 abstract 1
- CZDYPVPMEAXLPK-UHFFFAOYSA-N tetramethylsilane Chemical compound C[Si](C)(C)C CZDYPVPMEAXLPK-UHFFFAOYSA-N 0.000 abstract 1
- 230000001131 transforming effect Effects 0.000 abstract 1
- 235000013311 vegetables Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P19/00—Drugs for skeletal disorders
- A61P19/02—Drugs for skeletal disorders for joint disorders, e.g. arthritis, arthrosis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
- C11C1/025—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by saponification and release of fatty acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Microbiology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Botany (AREA)
- Rheumatology (AREA)
- Physical Education & Sports Medicine (AREA)
- Orthopedic Medicine & Surgery (AREA)
- Immunology (AREA)
- Dermatology (AREA)
- Pain & Pain Management (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
- Medicines Containing Plant Substances (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
extração líquida / líquido. a invenção se refere a um processo de extração de uma fração insaponificável contida em um óleo vegetal, um óleo proveniente de um microrganismo ou uma manteiga vegetal ou em um corpoduto da indústria da refinação dos óleos vegetais, tal como as descargas de desodorização, compreendendo pelo menos: a) uma etapa de transformação dos ditos óleos, da dita manteiga ou do dito coproduto da indústria da refinação dos óleos vegetais ou dos óleos provenientes de microrganismo em solução hidroalcólica, notadamente via uma etapa escolhida dentre as hidroalcólica, na qual a fração graxa é separada da fração insaponificável por uma extração líquida / líquido, c) eventualmente uma etapa de purificação do insaponificável escolhida no grupo constituído pelas extrações líquidas / líquido, o dito processo compreendendo pelo menos uma etapa dentre as extrações líquidas / líquido da etapa b, as cristalizações da etapa c e as extrações líquidas / líquido da etapa c é feita, utilizando-se um primeiro sistema de solventes, compreendendo um teor em solvente escolhido dentre os solventes aromáticos fluorados, notadamente o trifluoro tolueno (btf) e o hexafluoro benzeno (bhf), os éteres terc-butila, notadamente o 2-etóxi -2-metil propano, ainda denominado éter-etil-terc-butila (etbe), os solventes compreendendo pelo menos um átomo de silício, notadamente o hexametil di-siloxano (hmds) e o tetrametil silano (tms), o metil- tetra-hidro furano (methf, e suas misturas de pleo menos 50% em volume em relação ao volume total do sistema de solventes, das frações obtidas pelo dito processo e composições compreendendo as ditas frações.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1050644A FR2955784B1 (fr) | 2010-01-29 | 2010-01-29 | Extraction liquide / liquide |
| FR1150682A FR2955785B1 (fr) | 2010-01-29 | 2011-01-28 | Extraction liquide / liquide |
| PCT/EP2011/051321 WO2011092329A2 (fr) | 2010-01-29 | 2011-01-31 | Extraction liquide / liquide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR112012018953A2 true BR112012018953A2 (pt) | 2016-04-12 |
Family
ID=42746079
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112012018953A BR112012018953A2 (pt) | 2010-01-29 | 2011-01-31 | extração líquida / líquido |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8957232B2 (pt) |
| EP (1) | EP2528583B1 (pt) |
| KR (1) | KR101899602B1 (pt) |
| CN (1) | CN102724958B (pt) |
| BR (1) | BR112012018953A2 (pt) |
| CA (2) | CA2989041C (pt) |
| ES (1) | ES2593453T3 (pt) |
| FR (2) | FR2955784B1 (pt) |
| PL (1) | PL2528583T3 (pt) |
| WO (1) | WO2011092329A2 (pt) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3006328B1 (fr) * | 2013-06-04 | 2015-06-05 | Saeml Valagro Carbone Renouvelable Poitou Charentes | Procedes d'extraction selective des insaponifiables de matieres premieres renouvelables par extraction liquide-liquide en presence d'un cosolvant |
| FR3006327B1 (fr) * | 2013-06-04 | 2015-06-05 | Saeml Valagro Carbone Renouvelable Poitou Charentes | Procedes d'extraction selective des insaponifiables de matieres premieres renouvelables par trituration reactive en presence d'un cosolvant |
| FR3006329B1 (fr) * | 2013-06-04 | 2015-06-05 | Saeml Valagro Carbone Renouvelable Poitou Charentes | Procedes d'extraction selective des insaponifiables de matieres premieres renouvelables par extraction solide-liquide en presence d'un cosolvant |
| KR101439898B1 (ko) * | 2013-08-12 | 2014-09-17 | 박승재 | 상황버섯을 이용한 고품질 코코넛오일의 제조방법 |
| CN107019207B (zh) * | 2016-02-02 | 2022-03-18 | 林岳辉 | 植物自体萃取营养份的方法及营养份 |
| CN109022141A (zh) * | 2018-09-30 | 2018-12-18 | 海南煊烨生物科技有限公司 | 一种提取微生物油脂的方法 |
| CN115181080B (zh) * | 2022-07-22 | 2023-08-22 | 扬州贝尔新环境科技有限公司 | 一种甲基叔丁基醚-四氢呋喃-乙醇-水共沸体系的分离工艺 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2530809A (en) | 1949-08-23 | 1950-11-21 | Pittsburgh Plate Glass Co | Fractionation of tall oil |
| US4324802A (en) * | 1979-12-18 | 1982-04-13 | L'oreal | Cosmetic oil and composition containing the same |
| FR2526805A1 (fr) | 1982-05-14 | 1983-11-18 | Exsymol Sa | Perfectionnement a l'obtention de composes insaponifiables a partir de substances naturelles et produits resultants |
| FR2678632B1 (fr) * | 1991-07-03 | 1994-09-02 | Pharmascience Lab | Procede de preparation de l'insaponifiable d'avocat permettant d'ameliorer sa teneur en l'une de ses fractions dite h. |
| US5403514A (en) * | 1991-10-07 | 1995-04-04 | Canon Kabushiki Kaisha | Solvent composition and water-repellent/oil-repellent composition using the same |
| JP3310773B2 (ja) * | 1994-04-28 | 2002-08-05 | ダイセル化学工業株式会社 | 脂肪族カルボン酸の抽出による分離方法 |
| DE19608463B4 (de) * | 1996-03-02 | 2008-08-14 | Sasol- Lurgi Technology Co.(Pty)Ltd. | Verfahren zum Extrahieren von Phenolen aus einem phenolhaltigen Abwasser mittels eines Lösungsmittel-Gemisches |
| FR2753200B1 (fr) | 1996-09-06 | 1998-12-04 | Fabre Pierre Dermo Cosmetique | Procede d'extraction de lipides provenant de la lecithine de soja, extrait lipidique obtenu et compositions dermato-cosmetiques le contenant |
| FR2762512B1 (fr) | 1997-04-24 | 2000-10-13 | Pharmascience Lab | Compositions a base d'huile de lupin, notamment a base d'huile de lupin et d'huile de germe de ble et leur utilisation en cosmetologie, en pharmacie et en tant que complement alimentaire |
| EP1155104A2 (en) | 1999-02-10 | 2001-11-21 | Eastman Chemical Company | Corn fiber for the production of advanced chemicals and materials |
| FR2802547B1 (fr) | 1999-12-21 | 2002-03-01 | Archimex Pibs | Procede d'extraction et de fractionnement de matieres grasses par solvant, mettant en oeuvre au moins un hydrofluoroether |
| FR2803598B1 (fr) * | 2000-01-12 | 2002-04-26 | Pharmascience Lab | Procede d'extraction des insaponifiables des huiles vegetales au moyen de chloro-1-butane, composition comprenant ces insaponifiables |
| WO2001079400A2 (en) | 2000-04-14 | 2001-10-25 | Mars Incorporated | Extraction of sterols from cocoa hulls |
| US6497813B2 (en) * | 2001-01-19 | 2002-12-24 | Process Dynamics, Inc. | Solvent extraction refining of petroleum products |
| US6994875B2 (en) * | 2002-07-29 | 2006-02-07 | Laboratoires Expanscience | Process for obtaining a furan lipid-rich unsaponifiable material from avocado |
| MY130618A (en) | 2002-11-27 | 2007-07-31 | Malaysian Palm Oil Board | A method of extracting and isolating minor components from vegetable oil |
| US7776218B2 (en) * | 2003-12-19 | 2010-08-17 | Kfi Intellectual Properties L.L.C. | System for liquid extraction, and methods |
| JP4482627B2 (ja) * | 2004-01-28 | 2010-06-16 | 学校法人早稲田大学 | １，２，５−チアジアゾール化合物を含有してなる溶剤およびこの溶媒を用いた有機化合物の抽出方法 |
| US7038068B2 (en) * | 2004-03-16 | 2006-05-02 | Hitachi Global Storage Technologies Netherlands B.V. | Method for liquid/liquid extraction of molecular weight fractions of perfluorinated polyethers |
| WO2006009417A1 (es) | 2004-07-21 | 2006-01-26 | De La Llata Romero, Manuel | Obtenciòn de los lìpidos fijos totales de semillas de la familia sapotàcea para la preparaciòn de cosmèticos y composiciones farmacèuticas dermatològicas |
-
2010
- 2010-01-29 FR FR1050644A patent/FR2955784B1/fr not_active Expired - Fee Related
-
2011
- 2011-01-28 FR FR1150682A patent/FR2955785B1/fr active Active
- 2011-01-31 CN CN201180007378.9A patent/CN102724958B/zh active Active
- 2011-01-31 ES ES11701155.1T patent/ES2593453T3/es active Active
- 2011-01-31 WO PCT/EP2011/051321 patent/WO2011092329A2/fr not_active Ceased
- 2011-01-31 KR KR1020127020242A patent/KR101899602B1/ko active Active
- 2011-01-31 CA CA2989041A patent/CA2989041C/fr active Active
- 2011-01-31 EP EP11701155.1A patent/EP2528583B1/fr active Active
- 2011-01-31 US US13/575,402 patent/US8957232B2/en active Active
- 2011-01-31 BR BR112012018953A patent/BR112012018953A2/pt not_active Application Discontinuation
- 2011-01-31 PL PL11701155T patent/PL2528583T3/pl unknown
- 2011-01-31 CA CA2787773A patent/CA2787773C/fr active Active
Also Published As
| Publication number | Publication date |
|---|---|
| KR101899602B1 (ko) | 2018-09-17 |
| CA2989041A1 (fr) | 2011-08-04 |
| EP2528583A2 (fr) | 2012-12-05 |
| FR2955785A1 (fr) | 2011-08-05 |
| FR2955784B1 (fr) | 2014-02-14 |
| FR2955785B1 (fr) | 2014-02-07 |
| CA2989041C (fr) | 2020-08-25 |
| US20130035383A1 (en) | 2013-02-07 |
| EP2528583B1 (fr) | 2016-07-20 |
| CN102724958B (zh) | 2017-04-26 |
| PL2528583T3 (pl) | 2017-01-31 |
| FR2955784A1 (fr) | 2011-08-05 |
| CA2787773A1 (fr) | 2011-08-04 |
| US8957232B2 (en) | 2015-02-17 |
| WO2011092329A2 (fr) | 2011-08-04 |
| ES2593453T3 (es) | 2016-12-09 |
| CN102724958A (zh) | 2012-10-10 |
| CA2787773C (fr) | 2020-06-09 |
| WO2011092329A3 (fr) | 2012-02-23 |
| KR20120139690A (ko) | 2012-12-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B11A | Dismissal acc. art.33 of ipl - examination not requested within 36 months of filing | ||
| B11Y | Definitive dismissal - extension of time limit for request of examination expired [chapter 11.1.1 patent gazette] | ||
| B15K | Others concerning applications: alteration of classification |
Ipc: B01D 11/04 (2006.01), A23L 33/10 (2016.01), A23L 3 |